IP Library Granted Patent US 11,319,477
Granted Patent B2
US 11,319,477 · App. 16/655,119 · Granted May 3, 2022

Breaker additives for extended delay in removal of oil-based filter cakes

Inventors: Catherine Martin Santos (Houston, TX); William Walter Shumway (Spring, TX); Jay Paul Deville (Spring, TX)
Assignee: Halliburton Energy Services, Inc.
C09K8/52C09K8/035C09K2208/26
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Quick Facts
Patent No.
US 11,319,477
App. No.
16/655,119
Granted
May 3, 2022
Kind
B2
Abstract

The present disclosure provides methods, compositions, and systems directed to filter cake removal embodying a delayed breaker fluid for oil-based drill-in fluids. A wellbore treatment method comprising: introducing a delayed breaker fluid into a wellbore, wherein the delayed breaker fluid comprises an aqueous base fluid, an acid precursor, and a carbodiimide; and contacting a filter cake in the wellbore with the delayed breaker fluid such that the filter cake is at least partially degraded by acid released from the acid precursor.

Claims (23)

1. A wellbore treatment method comprising:

introducing a delayed breaker fluid into a wellbore, wherein the delayed breaker fluid comprises an aqueous base fluid, an acid precursor, and a carbodiimide, wherein the carbodiimide is present in an amount of about 1 to about 3 pounds per barrel of the delayed breaker fluid; and

contacting an oil-based filter cake in the wellbore with the delayed breaker fluid such that the oil-based filter cake is at least partially degraded by acid released from the acid precursor.

2. The method of claim 1 , wherein the delayed breaker fluid further comprises a wetting-agent.

3. The method of claim 2 , wherein the wetting-agent comprises a surfactant.

4. The method of claim 2 , wherein the wetting-agent is present in an amount of about 0.02% to about 4% by volume of the delayed breaker fluid.

5. The method of claim 1 , wherein the delayed breaker fluid is essentially free of polymeric viscosifiers.

6. The method of claim 1 , wherein the carbodiimide comprises at least one carbodiimide selected from the group consisting of a carbodiimide monomer, a polycarbodiimide, and combinations thereof.

7. The method of claim 1 , wherein the carbodiimide comprises at least one carbodiimide monomer selected from the group consisting of dialkyl-,diaryl-, diallyl-carbodiimides, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDCI), N,N′-dicyclohexylcarbodiimide (DCC), N,N′-diisopropylcarbodiimide (DIC), and bis(2,6-diisopropylphenyl)carbodiimide, and combinations thereof.

8. The method of claim 1 , wherein the aqueous base fluid comprises at least one fluid selected from the group consisting of fresh water, saltwater, seawater, and combinations thereof.

9. The method of claim 1 , wherein the aqueous base fluid is present in an amount of about 50% to about 99% by volume of the delayed breaker fluid.

10. The method of claim 1 , wherein the acid precursor is present in an amount of about 5% to about 25% by volume of the delayed breaker fluid.

11. The method of claim 1 , wherein the acid precursor comprises an ester-based acid precursor.

12. A wellbore treatment method comprising:

introducing a delayed breaker fluid into a wellbore, wherein the delayed breaker fluid comprises a brine; an ester-based breaker; a carbodiimide, wherein the carbodiimide is present in an amount of about 1 to about 3 pounds per barrel of the delayed breaker fluid; and a wetting agent;

contacting an oil-based filter cake in the wellbore with the delayed breaker fluid; and

degrading the oil-based filter cake with acid released from the ester-based breaker.

13. The method of claim 12 , wherein the delayed breaker fluid is essentially free of polymeric viscosifiers.

14. The method of claim 12 , wherein the ester-based breaker is present in an amount of about 5% to about 25% by volume of the delayed breaker fluid.

15. The method of claim 12 , wherein the carbodiimide comprises at least one carbodiimide selected from the group consisting of a carbodiimide monomer, a polycarbodiimide, and combinations thereof.

16. The method of claim 12 , wherein the carbodiimide comprises at least one carbodiimide monomer selected from the group consisting of dialkyl-,diaryl-, diallyl-carbodiimides, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide (EDCI), N,N′-dicyclohexylcarbodiimide (DCC), N,N′-diisopropylcarbodiimide (DIC), and bis(2,6-diisopropylphenyl)carbodiimide, and combinations thereof.

17. The method of claim 12 , wherein the wetting-agent is present in an amount of about 0.02% to about 4% by volume of the delayed breaker fluid.

18. The method of claim 12 , wherein the aqueous base fluid is present in an amount of about 50% to about 99% by volume of the delayed breaker fluid.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2019
From: SANTOS, CATHERINE MARTIN; SHUMWAY, WILLIAM WALTER; DEVILLE, JAY PAUL
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 050956/0402 →
Continuity (1)
Related Publication 20210115320A1 · Apr 22, 2021
Cited By (1)
US 12,466,988