IP Library Granted Patent US 11,028,019
Granted Patent B2
US 11,028,019 · App. 16/655,325 · Granted Jun 8, 2021

Boron carbide composite

Inventors: Jeffrey P Youngblood (West Lafayette, IN); Erich Weaver (West Lafayette, IN); Rodney W. Trice (West Lafayette, IN); Andres Diaz-Cano (West Lafayette, IN); Andrew Schlup (West Lafayette, IN)
Assignee: Purdue Research Foundation
C04B35/563B28B1/24B28B11/243C04B35/6261C04B35/6264C04B35/64C04B2235/3225C04B2235/3821C04B2235/3847C04B2235/6022C04B2235/656C04B2235/668
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Quick Facts
Patent No.
US 11,028,019
App. No.
16/655,325
Granted
Jun 8, 2021
Kind
B2
Abstract

The present disclosure relates to boron carbide (B 4 C) composite material and the method of making and using the boron carbide (B 4 C) composite.

Claims (11)

1. A composite material comprising a sintered product of a mixture comprising 70-95 wt. % of boron carbide (B 4 C), 2-15 wt. % of tungsten carbide-cobalt (WC—Co), and 3-15 wt. % of yttrium oxide (Y 2 O 3 ), wherein said boron carbide, tungsten carbide-cobalt (WC—Co), and yttrium oxide are substantially uniformly distributed in the sintered product, wherein the sintered product has a relative density of 90-99%.

2. The composite material of claim 1 , wherein the mixture comprises 70-90 wt. % of boron carbide (B 4 C), 5-15 wt. % of tungsten carbide-cobalt (WC—Co), and 5-15 wt. % of yttrium oxide (Y 2 O 3 ).

3. The composite material of claim 1 , wherein the sintered product has a relative density of 97-99%.

4. The composite material of claim 1 , wherein the sintered product is obtained under substantially pressureless condition at a temperature range of 1600-2600° C.

5. The composite material of claim 1 , wherein said boron carbide is first attrition milled with tungsten carbide in ethanol to provide attrition milled mixture of boron carbide and tungsten carbide-cobalt (WC—Co), wherein said boron carbide after attrition milled is substantially free of boron oxide (B 2 O 3 ).

6. A method of preparing the composite material of claim 1 , comprising:

attrition milling boron carbide and tungsten carbide in ethanol to provide an attrition milled powder comprising boron carbide and tungsten carbide-cobalt (WC—Co), wherein said boron carbide after the attrition milling is substantially free of boron oxide (B 2 O 3 );

preparing an aqueous suspension comprising the attrition milled boron carbide and tungsten carbide-cobalt (WC—Co) powder, and yttrium oxide powder;

injecting mold said suspension and making it a dried mixture; and

sintering the dried mixture at a temperature range of 1600-2600° C. to provide the composite material.

7. The method of claim 6 , wherein the sintering is carried out at substantially pressureless condition.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 18, 2022
From: PURDUE UNIVERSITY
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 059657/0220 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 11, 2019
From: YOUNGBLOOD, JEFFREY PAUL; TRICE, RODNEY WAYNE; WEAVER, ERICH; DIAZ-CANO, ANDRES; SCHLUP, ANDREW
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 051242/0178 →
Continuity (2)
Provisional Application 62772659 · Nov 29, 2018
Related Publication 20200172441A1 · Jun 4, 2020