IP Library Granted Patent US 10,881,982
Granted Patent B2
US 10,881,982 · App. 16/659,698 · Granted Jan 5, 2021

Method and apparatus for extracting botanical oils

Inventor: C. Russell Thomas (Boulder, CO)
Assignee: Natural Extraction Systems, LLC
B01D11/02B01D1/14B01D3/343B01D11/023B01D11/028B01D11/0288B01D11/0296C11B1/10C11B9/027B01D2011/007
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Quick Facts
Patent No.
US 10,881,982
App. No.
16/659,698
Granted
Jan 5, 2021
Kind
B2
Abstract

An apparatus for extracting an oil from plant material includes an extraction chamber for plant material. The plant material is exposed to a heated gas stream with a temperature sufficient to volatilize on oil from the plant material. The gas stream is rapidly cooled to liquefy the oil into entrained droplets. The oil is collected with a collection solvent.

Claims (94)

1. A system for extracting oil from plant material, comprising:

a gas moving device operable to propel a gas stream through the system;

a heater in fluid communication with the gas moving device such that the heater is operable to heat the gas stream and produce a heated gas stream;

an extraction chamber configured to receive a plant material, in which the extraction chamber is in fluid communication with both the gas moving device and the heater such that the heated gas stream is directed through plant material disposed in the extraction chamber to vaporize oil from the plant material and produce an oil vapor;

a collection chamber in fluid communication with the extraction chamber such that the gas stream flows from the extraction chamber to the collection chamber, in which the collection chamber is configured to cool the gas stream to condense the oil vapor and produce a condensed oil; and

a liquid collector in fluid communication with the collection chamber such that at least some of the condensed oil is directed from the collection chamber to the liquid collector,

wherein the system is configured such that the gas moving device propels the gas stream through each of the heater, the extraction chamber, and the collection chamber; and

the system is configured to simultaneously vaporize oil from the plant material and condense oil vapor.

2. The system of claim 1 , further comprising:

a plant material hopper in communication with the extraction chamber such that the system is configured to automatically feed plant material from the plant material hopper into the extraction chamber; and

a spent plant material deposit area in communication with the extraction chamber such that the system is configured to convey plant material from the extraction chamber into the spent plant material deposit area,

in which the gas moving device is a blower;

the system comprises a substantially closed loop defined by the path of the gas stream; and

the system is configured such that the gas stream circulates through each of the blower, the extraction chamber, and the collection chamber.

3. The system of claim 1 , further comprising:

a plant material hopper in communication with the extraction chamber such that the system is configured to automatically feed plant material from the plant material hopper into the extraction chamber; and

a spent plant material deposit area in communication with the extraction chamber such that the system is configured to convey plant material from the extraction chamber into the spent plant material deposit area,

in which the system is configured to both automatically feed plant material into the extraction chamber and then convey the plant material from the extraction chamber in a total amount of time that is greater than 15 seconds and less than 75 seconds.

4. The system of claim 1 , in which the system is configured such that the gas stream enters the collection chamber within 5 seconds after the gas stream exits the extraction chamber.

5. The system of claim 1 , further comprising a plant material hopper in communication with the extraction chamber such that the system is configured to automatically feed plant material from the plant material hopper into the extraction chamber.

6. The system of claim 1 , further comprising a spent plant material deposit area in communication with the extraction chamber such that the system is configured to automatically convey plant material from the extraction chamber into the spent plant material deposit area, in which the spent plant material deposit area is both in fluid communication with the gas moving device and separated from the external atmosphere.

7. The system of claim 1 , further comprising a spent plant material deposit area in communication with the extraction chamber such that the system is configured to automatically convey plant material from the extraction chamber into the spent plant material deposit area.

8. The system of claim 1 , in which:

the system comprises a substantially closed loop defined by the path of the gas stream;

the gas moving device is a blower; and

the system is configured such that the gas stream circulates through each of the blower, the extraction chamber, and the collection chamber.

9. The system of claim 1 , further comprising a cyclone, in which:

the system comprises a substantially closed loop defined by the path of the gas stream;

the substantially closed loop comprises the cyclone;

the cyclone is configured to separate particles or droplets from the gas stream; and

the system is configured such that the gas stream circulates through each of the blower, the extraction chamber, the cyclone, and the collection chamber.

10. The system of claim 1 , in which:

the system comprises a substantially closed loop defined by the path of the gas stream; and

the system is configured such that the gas stream circulates through each of the gas moving device, the extraction chamber, and the collection chamber.

11. The system of claim 1 , in which:

the system comprises a substantially closed loop defined by the path of the gas stream, and

the system is configured such that the gas stream circulates through both the extraction chamber and the collection chamber.

12. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber and configured to spray a collection solvent into the collection chamber, in which: (a) the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil, and (b) the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector;

a solvent reservoir in fluid communication with the collection solvent sprayer, in which (a) the solvent reservoir is configured to contain the collection solvent to be sprayed by the collection solvent sprayer, and (b) the solvent reservoir is configured to receive collection solvent from the liquid collector;

a liquid pump configured to pump collection solvent from the liquid collector to the solvent reservoir;

a secondary distillation system operable to boil the collection solvent to generally separate at least a portion of the collection solvent from at least a portion of the dissolved oil; and

a vacuum pump configured to create at least a partial vacuum in the secondary distillation system to reduce the boiling point of the collection solvent.

13. The system of claim 1 , further comprising:

a collection solvent sprayer;

a solvent reservoir; and

a secondary distillation system,

in which:

the collection solvent sprayer is configured to spray a collection solvent from the solvent reservoir into the collection chamber;

the solvent reservoir is configured to contain the collection solvent to be sprayed by the collection solvent sprayer;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil;

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector;

the secondary distillation system is in fluid communication with the liquid collector such that the system is operable to direct at least a portion of the collection solvent and at least a portion of the dissolved oil from the liquid collector to the secondary distillation system; and

the secondary distillation system is operable to boil the collection solvent to generally separate at least a portion of the collection solvent from at least a portion of the dissolved oil.

14. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber;

a solvent reservoir in fluid communication with the collection solvent sprayer;

a secondary distillation system operable to boil a collection solvent; and

a vacuum pump in fluid communication with the secondary distillation system,

in which the collection solvent sprayer is configured to spray the collection solvent from the solvent reservoir into the collection chamber;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil;

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector;

the secondary distillation system is configured to generally separate at least a portion of the collection solvent from at least a portion of the dissolved oil; and

the vacuum pump is operable to reduce the boiling point of the collection solvent by creating at least a partial vacuum in the secondary distillation system.

15. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber;

a solvent reservoir in fluid communication with the collection solvent sprayer; and

a secondary distillation system operable to boil a collection solvent, in which the collection solvent sprayer is configured to spray the collection solvent from the solvent reservoir into the collection chamber;

the solvent reservoir is configured to contain collection solvent to be sprayed by the collection solvent sprayer;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil;

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector; and

the secondary distillation system is configured to generally separate at least a portion of the collection solvent from at least a portion of the dissolved oil.

16. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber; and

a solvent reservoir in fluid communication with the collection solvent sprayer,

in which:

the collection solvent sprayer is configured to spray a collection solvent from the solvent reservoir into the collection chamber;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil;

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector; and

the liquid collector is in fluid communication with the solvent reservoir such that the system comprises a substantially closed loop defined by the path of the collection solvent.

17. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber; and

a solvent reservoir in fluid communication with the collection solvent sprayer, in which the collection solvent sprayer is configured to spray a collection solvent from the solvent reservoir into the collection chamber;

the solvent reservoir is configured to contain collection solvent to be sprayed by the collection solvent sprayer;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil;

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector; and

the system is configured to direct collection solvent from the liquid collector to the solvent reservoir.

18. The system of claim 1 , further comprising:

a collection solvent sprayer in fluid communication with the collection chamber; and

a solvent reservoir in fluid communication with the collection solvent sprayer,

in which:

the collection solvent sprayer is configured to spray a collection solvent from the solvent reservoir into the collection chamber;

the collection solvent is a liquid capable of dissolving at least a portion of the oil vapor such that either the condensed oil is a dissolved oil or the condensed oil becomes a dissolved oil; and

the system is configured such that at least some of the collection solvent that the collection solvent sprayer sprays into the collection chamber and at least some of the dissolved oil that is dissolved in the collection solvent are directed from the collection chamber to the liquid collector.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2020
From: THOMAS, C. RUSSELL
To: NATURAL EXTRACTION SYSTEMS, LLC
Reel/Frame 052800/0830 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 26, 2020
From: THOMAS, C. RUSSELL
To: NATURAL EXTRACTION SYSTEMS, LLC
Reel/Frame 052751/0418 →
Continuity (5)
Continuation 16184574 · Nov 8, 2018
Division 15090143 · Apr 4, 2016
Continuation PCTIB2014002383 · Oct 6, 2014
Provisional Application 61886908 · Oct 4, 2013
Related Publication 20200129882A1 · Apr 30, 2020
Cited By (4)
US 12,297,181 US 12,420,214 US 12,544,390 US 12,606,535