IP Library › Granted Patent US 11,316,171
Granted Patent B2
US 11,316,171 · App. 16/675,538 · Granted Apr 26, 2022

Conductive, anti-corrosive magnesium titanium oxide material

Inventors: Lei Cheng (Sunnyvale, CA); Jonathan Mailoa (Cambridge, MA); Soo Kim (Cambridge, MA); Mordechai Kornbluth (Brighton, MA); Dawei Zhang (La Jolla, CA); Nathan Craig (Santa Clara, CA)
Assignee: ROBERT BOSCH GMBH
H01M8/0228H01M8/0206H01M8/0217
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Quick Facts
Patent No.
US 11,316,171
App. No.
16/675,538
Granted
Apr 26, 2022
Kind
B2
Abstract

A fuel cell bipolar plate (BPP) includes a metal substrate having a bulk portion and a surface portion comprising an anticorrosive, conductive material having oxygen vacancies and a formula (I): MgTi 2 O 5-δ   (I), where δ is any number between 0 and 3 optionally including a fractional part denoting the oxygen vacancies, the material having an electronic conductivity of about 2-10 S/m at room temperature in an ambient environment.

Claims (29)

1. A fuel cell bipolar plate comprising:

a metal substrate having:

a bulk portion; and

a surface portion comprising an anticorrosive, conductive, non-stoichiometric material having oxygen vacancies and a formula (I):

MgTi 2 O 5-δ   (I),

where δ is a number between 0 and 3 including a fractional part denoting the oxygen vacancies, the non-stoichiometric material having an electronic conductivity of about 2-10 S/m at room temperature in an ambient environment.

2. The bipolar plate of claim 1 , wherein a static corrosion current density of the bipolar plate is less than about 1 μA cm −2 at pH of 2 at a temperature of about 0 to 80° C.

3. The bipolar plate of claim 1 , wherein an Mg/Ti ratio of the material is a number in a range between 0.3 to 0.6.

4. The bipolar plate of claim 1 , wherein the material has an activation energy of about 0.13 eV in a temperature range between 25° C. to 80° C.

5. The bipolar plate of claim 1 , wherein the material has a crystalline structure.

6. The bipolar plate of claim 5 , wherein the structure includes at least one Ti atom with five bonds to oxygen atoms.

7. A proton-exchange-membrane fuel cell bipolar plate comprising:

a metal substrate having a bulk portion and a surface portion either one of which includes an anticorrosive, conductive non-stoichiometric material having oxygen vacancies and a formula (I):

MgTi 2 O 5-δ   (I),

where δ is a number between 0 and 3 including a fractional part and denoting oxygen vacancies,

the non-stoichiometric material having a nominal chemical composition of about 33 mol % MgO and 66 mol % of a mixture of TiO and TiO 2 .

8. The bipolar plate of claim 7 , wherein an Mg/Ti ratio is a number in a range between 0.3 to 0.6.

9. The bipolar plate of claim 7 , wherein a static corrosion current density of the bipolar plate is less than about 1 μA cm −2 at pH of 2 at a temperature of about 0 to 80° C.

10. The bipolar plate of claim 7 , wherein the material has an activation energy of about 0.13 eV in a temperature range between 25° C. to 80° C.

11. The bipolar plate of claim 7 , wherein the bulk portion comprises the material.

12. A fuel cell comprising:

a bipolar plate having a metal substrate including a bulk portion and a surface portion comprising an anticorrosive, conductive material having oxygen vacancies and a formula (I):

MgTi 2 O 5-δ   (I),

where

δ is any number between 0 and 3 including the fractional part denoting the oxygen vacancies,

the material having an electronic conductivity of about 2-10 S/m at room temperature in ambient environment.

13. The fuel cell of claim 12 , wherein static corrosion current density of the bipolar plate is less than about 1 μA cm −2 at pH of 2 at a temperature of about 0 to 80° C.

14. The fuel cell of claim 12 , wherein an Mg/Ti ratio of the material is a number in a range between 0.3 to 0.6.

15. The fuel cell of claim 12 , wherein the fuel cell is an anion exchange membrane fuel cell (AEMFC).

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2019
From: CHENG, LEI; MAILOA, JONATHAN; KIM, SOO; KORNBLUTH, MORDECHAI; ZHANG, DAWEI; CRAIG, NATHAN
To: ROBERT BOSCH GMBH
Reel/Frame 050932/0163 →
Continuity (1)
Related Publication 20210135252A1 · May 6, 2021