Method of acquiring sample for evaluation of SiC single crystal
A method of acquiring a sample for evaluation of a SiC single crystal, comprising: a step of cutting a SiC ingot in a radial direction at a thickness position, which is located in a range from a curved surface which forms a distal end surface in a crystal growth direction to a seed crystal, to obtain a head member which includes the curved surface, wherein the SiC ingot used in the step is a SiC ingot in which SiC thereof is crystal-grown from a seed crystal along a c axis direction; and a step of polishing a silicon surface of the head member to obtain a sample for evaluation.
1. A method of acquiring a sample for evaluation of a SiC single crystal, comprising:
a step of cutting a SiC ingot in a radial direction at a thickness position, which is located in a range from a curved surface which forms a distal end surface in a crystal growth direction to a seed crystal, to obtain a dome head member which includes the curved surface, wherein the SiC ingot used in the step is a SiC ingot in which SiC thereof is crystal-grown from the seed crystal along a c axis direction, and wherein the SiC ingot used in the step comprises the dome head member and a truncated cone portion; and
a step of polishing a silicon surface of the dome head member to obtain a sample for evaluation.
2. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 1 ,
wherein the thickness position is located closer to a position, where a diameter of the SiC ingot starts to be reduced in the crystal growth direction, on the seed crystal side of the position.
3. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 1 ,
wherein distance from the distal end of the curved surface to the thickness position in a crystal growth direction is included in a length range of 1% or more and 30% or less with respect to a total length of the SiC single crystal which is a length between the distal end of the curved surface and the seed crystal.
4. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 3 ,
wherein the distance from the distal end of the curved surface to the thickness position in a crystal growth direction is included in a length range of 1% or more and 10% or less with respect to the total length of the SiC single crystal.
5. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 3 ,
wherein the distance from the distal end of the curved surface to the thickness position in a crystal growth direction is included in a length range of 1% or more and 5% or less with respect to the total length of the SiC single crystal.
6. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 3 ,
wherein the distance from the distal end of the curved surface to the thickness position in a crystal growth direction is included in a length range of 1% or more and 3% or less with respect to the total length of the SiC single crystal.
7. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 1 , further comprising:
a step of grinding a portion including the distal end of the curved surface to form a flat surface.
8. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 1 , further comprising:
a step of loading the sample for evaluation on a sample supporting member including a supporting surface having a shape of the curved surface.
9. The method of acquiring a sample for evaluation of a SiC single crystal according to claim 1 ,
wherein the dome head member includes the silicon surface and the curved surface, wherein the silicon surface is a flat surface.