IP Library Granted Patent US 11,236,320
Granted Patent B2
US 11,236,320 · App. 16/737,292 · Granted Feb 1, 2022

Enzymatic production of hexoses

Inventors: Daniel Joseph Wichelecki (Charlottesville, VA); Edwin O. Rogers (Charlottesville, VA)
Assignee: BONUMOSE, INC.
C12N9/90C12N9/1051C12N9/16C12N9/92C12P19/02C12P19/14C12P19/18C12P19/24C12Y204/01001C12Y301/03011C12Y503/01009C12Y504/02002
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Quick Facts
Patent No.
US 11,236,320
App. No.
16/737,292
Granted
Feb 1, 2022
Kind
B2
Abstract

Disclosed herein are methods of producing hexoses from saccharides by enzymatic processes. The methods utilize fructose 6-phosphate and at least one enzymatic step to convert it to a hexose.

Claims (17)

1. An enzymatic process for preparing fructose from sucrose, the process comprising the steps of:

(i) a step of converting sucrose to glucose 1-phosphate (G1P) using a sucrose phosphorylase;

(ii) a step of converting G1P to glucose 6-phosphate (G6P), wherein the step is catalyzed by a phosphoglucomutase (PGM)

(iii) a step of converting G6P to fructose 6-phosphate (F6P), wherein the step is catalyzed by a phosphoglucoisomerase (PGI)

(iv) a step of converting F6P to fructose catalyzed by a fructose 6-phosphate phosphatase (F6PP), wherein the process is conducted without adenosine triphosphate (ATP) as a source of phosphate.

2. The process of claim 1 , wherein the process steps are conducted under at least one of the following process conditions:

at a temperature ranging from about 37° C. to about 85° C.,

at a pH ranging from about 5.0 to about 9.0, or

for about 0.5 hours to about 48 hours.

3. The process of claim 1 , wherein the process steps are conducted under at least one of the following process conditions:

without nicotinamide adenosine dinucleotide,

at a phosphate concentration from about 0.1 mM to about 150 mM,

where phosphate is recycled, or

where step (iv) involves an energetically favorable chemical reaction.

4. The process of claim 3 , wherein phosphate is recycled, and the phosphate produced by F6PP dephosphorylation of F6P is used in the process step of converting sucrose to G1P.

5. The process of claim 3 , wherein the step of converting F6P to fructose is an energetically favorable, irreversible phosphatase reaction.

6. The process of claim 1 , wherein the process steps are conducted in a single reaction vessel.

Assignments (3)
SECURITY INTEREST Recorded Nov 8, 2022
From: BONUMOSE, INC.
To: X-CALIBER RURAL CAPITAL, LLC
Reel/Frame 061691/0474 →
CHANGE OF NAME Recorded Nov 1, 2021
From: BONUMOSE LLC
To: BONUMOSE, INC.
Reel/Frame 058598/0501 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2020
From: WICHELECKI, DANIEL JOSEPH; ROGERS, EDWIN O.
To: BONUMOSE LLC
Reel/Frame 051452/0173 →
Continuity (7)
Division 16542560 · Aug 16, 2019
Continuation PCTUS2018022185 · Mar 13, 2018
Provisional Application 62482148 · Apr 5, 2017
Provisional Application 62480798 · Apr 3, 2017
Provisional Application 62470620 · Mar 13, 2017
Provisional Application 62470605 · Mar 13, 2017
Related Publication 20200131499A1 · Apr 30, 2020