IP Library Granted Patent US 10,815,229
Granted Patent B1
US 10,815,229 · App. 16/821,294 · Granted Oct 27, 2020

Benzenesulfonamide compounds and their use as therapeutic agents

Inventors: Kristen Nicole Burford (Burnaby, CA); Sultan Chowdhury (Burnaby, CA); Christoph Martin Dehnhardt (Burnaby, CA); Thilo Focken (Burnaby, CA); Michael Edward Grimwood (Burnaby, CA); Syed Abid Hasan (Burnaby, CA)
Assignee: Xenon Pharmaceuticals Inc.
C07D451/06C07D213/76C07D237/20C07D239/69C07D261/16C07D277/52C07D285/08C07D401/12C07D403/12C07D413/12C07D417/12C07D417/14C07D493/10
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Quick Facts
Patent No.
US 10,815,229
App. No.
16/821,294
Granted
Oct 27, 2020
Kind
B1
Abstract

This invention is directed to benzenesulfonamide compounds, as stereoisomers, enantiomers, tautomers thereof or mixtures thereof; or pharmaceutically acceptable salts, solvates or prodrugs thereof, for the treatment of diseases or conditions associated with voltage-gated sodium channels, such as epilepsy.

Claims (79)

1. A compound of the following formula:

wherein:

R 1 is an optionally substituted phenyl or optionally substituted pyridyl;

R 2 is an optionally substituted thiazolyl, an optionally substituted thiadiazolyl, an optionally substituted isothiazolyl, or an optionally substituted pyridinyl;

R 3 is —O— or —N(R 13 )—;

R 4 , R 5 , and R 13 are each independently selected from hydrogen, alkyl, and haloalkyl;

each R 6 is independently selected from hydrogen, halo, alkyl, and haloalkyl;

R 7 is halo;

each R 8 is independently selected from hydrogen, alkyl, and haloalkyl;

m is 1 or 2; and

n is 1 or 2;

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

2. The compound of claim 1 , wherein:

R 1 is phenyl or pyridyl, each optionally substituted with halo or alkyl;

R 2 is thiazolyl, thiadiazolyl, isothiazolyl, or pyridinyl, each optionally substituted with halo or alkyl;

R 3 is —O— or —N(R 13 )—;

R 4 and R 5 are each hydrogen;

R 13 is hydrogen, alkyl, or haloalkyl;

each R 6 is independently selected from hydrogen, halo, alkyl, and haloalkyl;

R 7 is halo;

R 8 is hydrogen;

m is 1; and

n is 1 or 2;

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

3. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-5-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

4. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-5-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

5. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-5-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

6. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

7. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

8. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

9. The compound of claim 1 , which is (S)-2,6-difluoro-3-methyl-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

10. The compound of claim 1 , which is (S)-2,6-difluoro-3-methyl-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

11. The compound of claim 1 , which is (S)-2,6-difluoro-3-methyl-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

12. The compound of claim 1 , which is (S)-4-((1-benzyl-3-methylpyrrolidin-3-yl)oxy)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

13. The compound of claim 1 , which is (S)-4-((1-benzyl-3-methylpyrrolidin-3-yl)oxy)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

14. The compound of claim 1 , which is (S)-4-((1-benzyl-3-methylpyrrolidin-3-yl)oxy)-2,6-difluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

15. The compound of claim 1 , which is (S)-3-chloro-2,6-difluoro-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

16. The compound of claim 1 , which is (S)-3-chloro-2,6-difluoro-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

17. The compound of claim 1 , which is (S)-3-chloro-2,6-difluoro-4-(methyl(1-((6-methylpyridin-2-yl)methyl)pyrrolidin-3-yl)amino)-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

18. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-N-(isothiazol-3-yl)-5-methylbenzenesulfonamide, represented by the formula:

.

19. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-N-(isothiazol-3-yl)-5-methylbenzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

20. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-N-(isothiazol-3-yl)-5-methylbenzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

21. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(isothiazol-3-yl)-3-methylbenzenesulfonamide, represented by the formula:

22. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(isothiazol-3-yl)-3-methylbenzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

23. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(isothiazol-3-yl)-3-methylbenzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof;

or a pharmaceutically acceptable salt or solvate thereof.

24. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(6-fluoropyridin-2-yl)-3-methylbenzenesulfonamide, represented by the formula:

25. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(6-fluoropyridin-2-yl)-3-methylbenzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

26. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2,6-difluoro-N-(6-fluoropyridin-2-yl)-3-methylbenzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof; or a pharmaceutically acceptable salt or solvate thereof.

27. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

28. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

or a pharmaceutically acceptable salt thereof.

29. The compound of claim 1 , which is (S)-4-((1-benzylpyrrolidin-3-yl)(methyl)amino)-2-fluoro-3-methyl-N-(thiazol-4-yl)benzenesulfonamide, represented by the formula:

as an individual stereoisomer, enantiomer or tautomer thereof or a mixture thereof; or a pharmaceutically acceptable salt or solvate thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 18, 2020
From: ANDREZ, JEAN-CHRISTOPHE; BURFORD, KRISTEN NICOLE; CHOWDHURY, SULTAN; COHEN, CHARLES JAY; DEHNHARDT, CHRISTOPH MARTIN; DEVITA, ROBERT JOSEPH; EMPFIELD, JAMES ROY; FOCKEN, THILO; GRIMWOOD, MICHAEL EDWARD; HASAN, SYED ABID; JOHNSON, JAMES PHILIP, JR.; ZENOVA, ALLA YUREVNA
To: XENON PHARMACEUTICALS INC.
Reel/Frame 052144/0637 →
Continuity (4)
Continuation 16289212 · Feb 28, 2019
Continuation 15600490 · May 19, 2017
Provisional Application 62432152 · Dec 9, 2016
Provisional Application 62339773 · May 20, 2016