IP Library Granted Patent US 11,117,112
Granted Patent B2
US 11,117,112 · App. 16/833,446 · Granted Sep 14, 2021

Pressure-based control of fluidized bed reactor

Inventors: Kahl Brown (Moses Lake, WA); Matthew J. Miller (Moses Lake, WA); Benjamin Center (Moses Lake, WA); Gerald A. Zeininger (Long Beach, CA); Stein Julsrud (Moses Lake, WA)
Assignee: REC Silicon Inc
B01J8/1809B01J2208/00539B01J2219/002B01J2219/0022B01J2219/00164
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Quick Facts
Patent No.
US 11,117,112
App. No.
16/833,446
Granted
Sep 14, 2021
Kind
B2
Abstract

A method of controlling particle additions to a fluidized bed reactor includes measuring pressure fluctuations inside the fluidized bed reactor over a selected time period, determining a pressure parameter indicative of amplitudes of the pressure fluctuations, comparing the pressure parameter to a specified threshold, and controlling particle additions to the fluidized bed reactor when the pressure parameter deviates from the specified threshold.

Claims (40)

1. A method, comprising:

through a pressure tap, measuring pressure fluctuations inside a fluidized bed reactor over a selected time period at a location of the pressure tap along an axis of the fluidized bed reactor;

determining a pressure parameter indicative of amplitudes of the pressure fluctuations measured at the location of the pressure tap;

comparing the pressure parameter to a specified threshold; and

controlling particle additions to the fluidized bed reactor when the pressure parameter deviates from the specified threshold.

2. The method of claim 1 , wherein the pressure tap is at or below a location where gas is injected into the fluidized bed reactor.

3. The method of claim 1 , wherein the pressure tap is at or below a location where gas bubbles form in a fluidized bed of the fluidized bed reactor.

4. The method of claim 1 , wherein determining the pressure parameter further comprises determining a difference between a maximum pressure and a minimum pressure over the selected time period.

5. The method of claim 4 , wherein determining the pressure parameter further comprises determining a moving average of the difference between the maximum pressure and the minimum pressure of the selected time period and at least one earlier time period.

6. The method of claim 1 , wherein determining the pressure parameter further comprises determining a moving average of maximum pressure amplitudes based on the selected time period and at least one earlier time period.

7. The method of claim 1 , wherein determining the pressure parameter further comprises determining a standard deviation of the pressure over the selected time period.

8. The method of claim 1 , wherein determining the pressure parameter further comprises determining a standard deviation of pressure maximums over the selected time period, determining a standard deviation of pressure minimums over the selected time period, determining a pressure variance over the selected time period, or any combination thereof.

9. The method of claim 1 , further comprising:

determining a difference between the pressure parameter and the specified threshold; and

wherein controlling particle additions further comprises determining a rate at which to add particles to the fluidized bed reactor based at least in part on the difference between the pressure parameter and the specified threshold.

10. The method of claim 1 , wherein controlling particle additions further comprises increasing a rate at which particles are added to the fluidized bed reactor when the pressure parameter is below the specified threshold and decreasing the rate at which particles are added to the fluidized bed reactor when the pressure parameter is above the specified threshold.

11. The method of claim 1 , further comprising pyrolizing silicon-bearing gas in the fluidized bed reactor to produce polysilicon particles.

12. A method, comprising:

through a pressure tap, measuring pressure fluctuations inside a fluidized bed reactor over a selected time period at a location of the pressure tap along an axis of the fluidized bed reactor;

determining a pressure parameter indicative of amplitudes of pressure fluctuations measured at the location of the pressure tap;

comparing the pressure parameter to a pressure parameter set point;

determining a rate at which to add particles to the fluidized bed reactor based at least in part on the comparison of the pressure parameter and the pressure parameter set point; and

transmitting control signals to a particle supply system to supply particles to the fluidized bed reactor at the determined rate.

13. The method of claim 12 , wherein determining the pressure parameter further comprises determining a difference between a maximum pressure and a minimum pressure over the selected time period.

14. The method of claim 13 , wherein determining the pressure parameter further comprises determining a moving average of the difference between the maximum pressure and the minimum pressure of the selected time period and at least one earlier time period.

15. The method of claim 12 , wherein determining the pressure parameter further comprises determining a moving average of maximum pressure amplitudes based on the selected time period and at least one earlier time period.

16. The method of claim 12 , wherein determining the pressure parameter further comprises determining a standard deviation of a pressure over the selected time period, determining a standard deviation of pressure maximums over the selected time period, determining a standard deviation of pressure minimums over the selected time period, determining a variance of a pressure over the selected time period, or any combination thereof.

17. A system, comprising:

a reactor vessel;

a pressure sensor configured to sense a pressure inside the reactor vessel through a pressure tap located along an axis of the reactor vessel;

a particle supply system in fluid communication with the reactor vessel;

and a controller configured to:

receive data of the pressure in the reactor vessel measured at the location of the pressure tap from the pressure sensor over a selected time period;

determine a pressure parameter indicative of amplitudes of pressure fluctuations at the location of the pressure tap over the selected time period based at least in part on the data of the pressure in the reactor vessel measured at the location of the pressure tap;

compare the pressure parameter to a pressure parameter set point;

determine a rate at which to add particles to the reactor vessel based at least in part on the comparison of the pressure parameter and the pressure parameter set point; and

transmit control signals to the particle supply system to supply particles to the reactor vessel at the determined rate.

18. The system of claim 17 , wherein determining the pressure parameter further comprises determining a difference between a maximum pressure and a minimum pressure over a selected time period associated with gas bubbles emerging from an at least partially fluidized particle bed in the reactor vessel.

19. The system of claim 18 , wherein determining the pressure parameter further comprises determining a moving average of the difference between the maximum pressure and the minimum pressure of the selected time period and at least one earlier time period.

20. The system of claim 17 , wherein determining the pressure parameter further comprises determining an average maximum pressure in the reactor vessel over the selected time period, determining a standard deviation of the pressure over the selected time period, determining a variance of a pressure over the selected time period, or any combination thereof.

Assignments (2)
SECURITY INTEREST Recorded Jan 24, 2025
From: REC SILICON INC; REC ADVANCED SILICON MATERIALS LLC
To: HANWHA INTERNATIONAL LLC, AS LENDER
Reel/Frame 070002/0600 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2020
From: BROWN, KAHL; MILLER, MATTHEW J.; CENTER, BENJAMIN; ZEININGER, GERALD A.; JULSRUD, STEIN
To: REC SILICON INC
Reel/Frame 053322/0614 →
Continuity (2)
Provisional Application 62825729 · Mar 28, 2019
Related Publication 20200306712A1 · Oct 1, 2020
Cited By (1)
US 12,558,661