Passively pumped, polycrystalline ceramic high and ultra-high vacuum chambers
A sealed, passively pumped, polycrystalline ceramic vacuum chamber and method for fabricating the chamber are disclosed. The body of the vacuum chamber is made from a polycrystalline ceramic, for example, alumina. The vacuum chamber includes one or more windows made from a transparent ceramic, for example, sapphire, to accommodate optical access, while remaining amorphous-glass free to minimize or eliminate helium permeation. The vacuum chamber components are joined via laser welding or furnace brazing and the completed chamber is bakeable at temperatures up to 400° C. The vacuum chamber can operate at high or ultra-high vacuum pressures for an extended period through the use of one or more getter-based pumps. The vacuum chamber may include one or more atomic sources depending upon the application.
1. A sealed, passively pumped vacuum chamber comprising:
a body formed of a polycrystalline ceramic, the body including at least one window recess; and
at least one window, each of the at least one windows formed of a transparent ceramic, each of the at least one windows located in a corresponding one of the at least one window recesses.
2. The sealed, passively pumped vacuum chamber of claim 1 , wherein the polycrystalline ceramic used to form the body includes one of an oxide-based ceramic, a nitride-based ceramic, and a carbide-based ceramic.
3. The sealed, passively pumped vacuum chamber of claim 1 , wherein the polycrystalline ceramic used to form the body includes 80-99.8% alumina.
4. The sealed, passively pumped vacuum chamber of claim 1 , wherein a bottom of each of the at least one window recesses forms a slight angle with respect to a corresponding face of the body, the slight angle adapted to reduce optical reflections.
5. The sealed, passively pumped vacuum chamber of claim 1 , wherein the transparent ceramic used to form each of the at least one windows includes one of sapphire, aluminum oxynitride, yttrium oxide, and yttria-alumina garnet.
6. The sealed, passively pumped vacuum chamber of claim 1 , wherein each of the at least one windows includes an anti-reflection coating.
7. The sealed, passively pumped vacuum chamber of claim 1 , further comprising:
at least one filler metal ring, each of the at least one filler metal rings located between a corresponding one of the at least one window recesses and a corresponding one of the at least one windows;
or
at least one window frame, each of the at least one window frames located around a perimeter of a corresponding one of the at least one windows; and
at least one recess frame, each of the at least one recess frames located in a corresponding one of the at least one window recesses, each of the at least one recess frames facing a corresponding one of the at least one window frames.
8. The sealed, passively pumped vacuum chamber of claim 1 , further comprising at least one getter-based pump.
9. The sealed, passively pumped vacuum chamber of claim 8 , wherein each of the at least one getter-based pumps includes an alloy containing one or more of zirconium, aluminum, titanium, vanadium, and iron.
10. The sealed, passively pumped vacuum chamber of claim 8 ,
wherein the body further includes at least one port;
wherein each of the at least one getter-based pumps includes a corresponding tube body, each corresponding tube body being located in a corresponding one of the at least one ports.
11. The sealed, passively pumped vacuum chamber of claim 8 , wherein each of the at least one getter-based pumps is located adjacent to an inner surface of the body.
12. The sealed, passively pumped vacuum chamber of claim 8 , wherein each of the at least one getter-based pumps is adapted to be activated by at least one of electrical feedthroughs, induction, and light.
13. The sealed, passively pumped vacuum chamber of claim 1 ,
further comprising a pump out tube, the pump out tube adapted to be coupled to an external vacuum pumping system, the pump out tube adapted to be sealed;
wherein the body further includes a port; and
wherein the pump out tube is located in the port.
14. The sealed, passively pumped vacuum chamber of claim 13 , wherein the pump out tube includes an oxygen-free high thermal conductivity (OFHC) copper tube or a nickel tube.
15. The sealed, passively pumped vacuum chamber of claim 13 , wherein the pump out tube further includes a titanium or polycrystalline ceramic sleeve, the titanium or polycrystalline ceramic sleeve located around the exterior of a portion of the pump out tube.
16. The sealed, passively pumped vacuum chamber of claim 1 ,
further comprising a lid;
wherein the body further includes a port; and
wherein the lid is solder sealed to the port.
17. The sealed, passively pumped vacuum chamber of claim 1 ,
further comprising at least one atomic source;
wherein the body further includes at least one port; and
wherein each of the at least one atomic sources includes a corresponding tube body, each corresponding tube body being located in a corresponding one of the at least one ports.
18. The sealed, passively pumped vacuum chamber of claim 17 , wherein each of the at least one atomic sources includes one of aluminum (Al), argon (Ar), calcium (Ca), cesium (Cs), chromium (Cr), dysprosium (Dy), erbium (Er), francium (Fr), helium (He), indium (In), lithium (Li), magnesium (Mg), mercury (Hg), neon (Ne), potassium (K), rubidium (Rb), sodium (Na), strontium (Sr), xenon (Xe), ytterbium (Yb), diiodine (I 2 ), and disodium (Na 2 ).
19. The sealed, passively pumped vacuum chamber of claim 17 , wherein each of the at least one atomic sources is adapted to be activated by at least one of electrical feedthroughs, induction, and light.
20. The sealed, passively pumped vacuum chamber of claim 1 , further comprising:
at least one of a getter-based pump and an atomic source;
a high-temperature cofired ceramic (HTCC), each of the at least one getter-based pump and atomic source being located adjacent the HTCC, each of the at least one getter-based pump and atomic source being activated by metalized current paths within the HTCC; and
a tube body, the HTCC being located in the tube body;
wherein the body further includes a port; and
wherein the tube body is located in the port.