IP Library Granted Patent US 11,374,180
Granted Patent B2
US 11,374,180 · App. 16/861,655 · Granted Jun 28, 2022

Organic electroluminescent materials and devices

Inventors: Chuanjun Xia (Lawrenceville, NJ); Bin Ma (Plainsboro, NJ); David Zenan Li (Princeton, NJ); Bert Alleyne (Newtown, PA); Alan Deangelis (Pennington, NJ); James Fiordeliso (Yardley, PA); Vadim Adamovich (Yardley, PA)
Assignee: UNIVERSAL DISPLAY CORPORATION
H01L51/0085C07F15/0033
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Quick Facts
Patent No.
US 11,374,180
App. No.
16/861,655
Granted
Jun 28, 2022
Kind
B2
Abstract

Compounds are provided that comprise a ligand having a 5-substituted 2-phenylquinoline. In particular, the 2-phenylquinoline may be substituted with a cycloalkyl containing group at the 5-position. These compounds may be used in organic light emitting devices, in particular as red emitters in the emissive layer of such devices, to provide devices having improved properties.

Claims (46)

1. A compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent mono, di, tri, or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R B is selected from the group consisting of partially fluorinated alkyl having at least 2 carbon atoms and silyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

2. The compound of claim 1 , wherein A is phenyl.

3. The compound of claim 1 , wherein M is Ir.

4. The compound of claim 1 , wherein the compound has the formula:

wherein L′ is an ancillary ligand; and

wherein m is 1, 2, or 3.

5. The compound of claim 4 , wherein L′ is a monoanionic bidentate ligand.

6. The compound of claim 4 , wherein L′ is

and wherein each of R 1 , R 2 , and R 3 is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl.

7. The compound of claim 4 , wherein the compound has the formula:

wherein each R 1 , R 2 , R 3 , R 5 , R 6 and R 7 is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl; and

wherein m is 1, 2, or 3.

8. The compound of claim 7 , wherein each of R 1 and R 3 is a branched alkyl with branching at a position further than the α position to the carbonyl group.

9. The compound of claim 7 , wherein each of R 5 , R 6 and R 7 is independently selected from methyl and hydrogen, and at least one of R 5 , R 6 and R 7 is methyl.

10. The compound of claim 7 , wherein each of R 5 and R 7 is methyl, and R 6 is hydrogen.

11. The compound of claim 7 , wherein each of R 5 and R 6 is methyl, and R 7 is hydrogen.

12. The compound of claim 7 , wherein each of R 5 , R 6 and R 7 is methyl.

13. The compound of claim 1 , wherein R B is a partially fluorinated alkyl group having at least 4 carbon atoms.

14. The compound of claim 1 , wherein R B is a partially fluorinated alkyl group having at least 3 carbon atoms.

15. The compound of claim 1 , wherein the compound is selected from

16. The compound of claim 1 , wherein R B is silyl.

17. A first device comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent mono, di, tri, or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R B is selected from the group consisting of partially fluorinated alkyl having at least 2 carbon atoms and silyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

18. The first device of claim 17 , wherein the compound is selected from the group consisting of:

19. A consumer product comprising an organic light emitting device, comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound comprising a ligand L having the formula:

wherein A is a 5-membered or 6-membered carbocyclic or heterocyclic ring;

wherein R A can represent mono, di, tri, or tetra substitutions;

wherein each of R A is independently a hydrogen or a substituent selected from the group consisting of deuterium, alkyl, silyl, alkoxy, amino, alkenyl, alkynyl, arylkyl, aryl and heteroaryl;

wherein R B is selected from the group consisting of partially fluorinated alkyl having at least 2 carbon atoms and silyl; and

wherein the ligand L is coordinated to a metal M having an atomic number greater than 40.

20. The consumer product of claim 19 , wherein the consumer product is one of a flat panel display, a computer monitor, a television, a billboard, a light for interior or exterior illumination and/or signaling, a heads up display, a fully transparent display, a flexible display, a laser printer, a telephone, a cell phone, a personal digital assistant (PDA), a laptop computer, a digital camera, a camcorder, a viewfinder, a vehicle, a wall, theater or stadium screen, and a sign.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 8, 2020
From: XIA, CHUANJUN; MA, BIN; LI, DAVID ZENAN; ALLEYNE, BERT; FIORDELISO, JAMES; ADAMOVICH, VADIM; DEANGELIS, ALAN
To: UNIVERSAL DISPLAY CORPORATION
Reel/Frame 052608/0672 →
Continuity (4)
Continuation 15989854 · May 25, 2018
Continuation 13932546 · Jul 1, 2013
Continuation In Part 13006016 · Jan 13, 2011
Related Publication 20200259107A1 · Aug 13, 2020
Cited By (1)
US 12,622,128