IP Library Granted Patent US 11,376,534
Granted Patent B2
US 11,376,534 · App. 16/864,769 · Granted Jul 5, 2022

Polyamide nanofiber nonwovens for filters

Inventors: Wai-Shing Yung (Pensacola, FL); Scott E. Osborn (Pensacola, FL); Chris E. Schwier (Pensacola, FL); Vikram Gopal (The Woodlands, TX); Albert Ortega (Pensacola, FL); Joseph L. Menner (Pinehurst, TX)
Assignee: Ascend Performance Materials Operations LLC
B01D39/163A62B23/02B32B5/022B32B5/26B01D2239/025B01D2239/0442B01D2239/0618B01D2239/0622B01D2239/0654B01D2239/1233B01D2239/1258B32B2262/0261B32B2535/00
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,376,534
App. No.
16/864,769
Granted
Jul 5, 2022
Kind
B2
Abstract

A filter comprising a nanofiber nonwoven product is disclosed which comprises a polyamide with a relative viscosity from 2 to 330, spun into nanofibers with an average diameter of less than 1000 nanometers (1 micron). In general, the inventive products are prepared by: (a) providing a polyamide composition, wherein the polyamide has a relative viscosity from 2 to 330; (b) melt spinning the polyamide composition into a plurality of nanofibers having an average fiber diameter of less than 1 micron, followed by (c) forming the nanofibers into the product.

Claims (21)

1. A filter product comprising one or more layers of a nanofiber nonwoven product, comprising polyamide nanofibers, wherein the polyamide of the nanofibers comprises at least one of N6, N66, N6T/66, N612, N6/66, N6I/66, N66/6I/6T, N11, N12, or combinations thereof, wherein “N” means Nylon, wherein the polyamide of the nanofibers have a relative viscosity from 4 to 330, and wherein the nanofibers have an average diameter from 100 to 950 nanometers.

2. The filter product according to claim 1 , wherein the melt point of the nanofiber nonwoven product is 225° C. or greater.

3. The filter product according to claim 1 , wherein no more than 20% of the nanofibers have a diameter of greater than 700 nanometers.

4. The filter product according to claim 1 , wherein the polyamide of the nanofibers comprises nylon 66 or nylon 6/66.

5. The filter product according to claim 1 , wherein the nanofiber nonwoven product has an Air Permeability Value of less than 600 CFM/ft 2 .

6. The filter product according to claim 1 , wherein the nanofiber nonwoven product has a basis weight of 150 GSM or less.

7. The filter product according to claim 1 , wherein the nanofiber nonwoven product has a TDI of at least 20 ppm and an ODI of at least 1 ppm.

8. The filter product according to claim 1 , wherein the nanofiber nonwoven product is free of solvent.

9. The filter product according to claim 1 , further comprising a scrim layer and/or support layer.

10. The filter product according to claim 1 , wherein the filter is an air filter, an oil filter, a bag filter, a liquid filter, or a breathing filter.

11. The filter product according to claim 1 , comprising three or more layers of a nanofiber nonwoven product.

12. The filter product according to claim 1 , wherein the nanofiber nonwoven product comprises from 1 wppm to 30,000 wppm of zinc and less than or equal to 1 wt. % of a phosphorus compound.

13. A breathing filter product comprising:

a support layer; and

one or more layers of a nanofiber nonwoven product disposed on the support layer, wherein the nanofiber nonwoven product comprises polyamide nanofibers, wherein the nanofibers have an average diameter from 100 to 950 nanometers, and wherein the nanofiber nonwoven product has a TDI of at least 20 ppm and an ODI of at least 1 ppm.

14. The breathing filter according to claim 13 , wherein the polyamide of the nanofibers comprises at least one of N6, N66, N6T/66, N612, N6/66, N6I/66, N66/6I/6T, N11, N12, or combinations thereof, wherein “N” means Nylon.

15. The breathing filter according to claim 13 , wherein the polyamide of the nanofibers have a relative viscosity from 4 to 330.

16. The breathing filter according to claim 13 , wherein the nanofibers have an average diameter from 300 to 700 nanometers.

17. The breathing filter according to claim 13 , wherein the pressure drop of the nanofiber nonwoven product is from 0.5 to 10 mm H 2 O.

18. The breathing filter according to claim 13 , wherein the nanofiber nonwoven product is free of solvent.

19. The breathing filter according to claim 13 , wherein the nanofiber nonwoven product comprises from 1 wppm to 30,000 wppm of zinc and less than or equal to 1 wt. % of a phosphorus compound.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Dec 23, 2025
From: WILMINGTON SAVINGS FUND SOCIETY, FSB
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 074050/0090 →
SECURITY INTEREST Recorded Dec 23, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 074056/0183 →
SECURITY INTEREST Recorded Dec 19, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 074007/0183 →
SECURITY INTEREST Recorded Apr 10, 2025
From: BANK OF AMERICA, N.A.
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 070811/0705 →
SECURITY INTEREST Recorded Dec 8, 2022
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC
Reel/Frame 062094/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 19, 2020
From: YUNG, WAI-SHING; OSBORN, SCOTT E.; SCHWIER, CHRIS E.; GOPAL, VIKRAM; ORTEGA, ALBERT; MENNER, JOSEPH L.
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 054098/0891 →
Continuity (5)
Continuation In Part 16003528 · Jun 8, 2018
Provisional Application 62841485 · May 1, 2019
Provisional Application 62516867 · Jun 8, 2017
Provisional Application 62518769 · Jun 13, 2017
Related Publication 20200254371A1 · Aug 13, 2020
Cited By (4)
US 12,491,458 US 12,492,292 US 12,534,834 US 12,539,479