IP Library Granted Patent US 11,421,359
Granted Patent B2
US 11,421,359 · App. 16/880,015 · Granted Aug 23, 2022

Polyamide nanofiber nonwovens

Inventors: Wai-shing Yung (Pensacola, FL); Scott E. Osborn (Pensacola, FL); Chris E. Schwier (Pensacola, FL); Vikram Gopal (The Woodlands, TX); Albert Ortega (Pensacola, FL)
Assignee: Ascend Performance Materials Operations LLC
D04H1/4334D04H1/43838D04H1/552D04H1/56D04H1/565D04H3/016D04H3/16B82Y40/00
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Quick Facts
Patent No.
US 11,421,359
App. No.
16/880,015
Granted
Aug 23, 2022
Kind
B2
Abstract

A nanofiber nonwoven product is disclosed which comprises a polyamide with a relative viscosity from 2 to 330, spun into nanofibers with an average diameter of less than 1000 nanometers (1 micron). In general, the inventive products are prepared by: (a) providing a polyamide composition, wherein the polyamide has a relative viscosity from 2 to 330; (b) melt spinning the polyamide composition into a plurality of nanofibers having an average fiber diameter of less than 1 micron, followed by (c) forming the nanofibers into the product.

Claims (18)

1. A nanofiber nonwoven product comprising polyamide nanofibers and at least one additive, wherein the polyamide of the nanofibers comprises a nylon, nylon copolymer, nylon terpolymer, nylon blend, nylon derivative, or combinations thereof, wherein the at least one additive comprises an oil, a wax, a solvent, a stabilizer, a delusterant, an antioxidant, a colorant, a pigment, a dye, or combinations thereof wherein the polyamide of the nanofibers have a relative viscosity from 10 to 330, and wherein the nanofibers have an average diameter from 100 to 950 nanometers.

2. The nanofiber nonwoven product according to claim 1 , wherein the nanofiber nonwoven product comprised staple nanofibers.

3. The nanofiber nonwoven product according to claim 1 , wherein the nanofiber nonwoven product comprises continuous nanofibers.

4. The nanofiber nonwoven product according to claim 1 , wherein the melt point of the nanofiber nonwoven product is between 223° C. and 390° C.

5. The nanofiber nonwoven product according to claim 1 , wherein the product has an Air Permeability Value of less than 600 CFM/ft 2 .

6. The nanofiber nonwoven product according to claim 1 , wherein the polyamide nanofibers further comprise at least one of a polyolefin, a polyacetal, a polyester, a cellulose ether, a cellulose ester, a polyalkylene sulfide, a polyarylene oxide, a polysulfone, and combinations thereof.

7. The nanofiber nonwoven product according to claim 1 , wherein the polyamide nanofibers further comprise at least one of polyethylene, a polybutylene terephthalate, a polypropylene, a poly(vinylchloride), a polymethylmethacrylate, a polystyrene, a poly(vinylidene fluoride), a poly(vinylidene chloride), a polyvinyl alcohol, or combinations thereof.

8. The nanofiber nonwoven product according to claim 1 , wherein the polyamide nanofiber comprises Nylon 6, Nylon 66, Nylon 6,10, or combinations thereof.

9. The nanofiber nonwoven product according to claim 1 , wherein the polyamide nanofiber comprises at least 0.1 wt. % Nylon 6, Nylon 66, Nylon 61, Nylon 6T, or combinations thereof.

10. The nanofiber nonwoven product according to claim 1 , wherein from 1 to 20% of the nanofibers have a fiber diameter of greater than 700 nanometers.

11. The nanofiber nonwoven product according to claim 1 , wherein all additives are present in a total amount from 0.01 to 49 wt. %, based on the total weight of the nanofiber nonwoven product.

12. The nanofiber nonwoven product according to claim 1 , wherein the additive comprises a zinc compound.

13. The nanofiber nonwoven product according to claim 1 , wherein the additive comprises zinc oxide.

14. The nanofiber nonwoven product according to claim 1 , wherein the additive comprises a copper compound.

15. The nanofiber nonwoven product according to claim 1 , wherein the nanofiber nonwoven product has a TDI from 20 to 400 ppm and an ODI from 1 to 200 ppm.

16. The nanofiber nonwoven product according to claim 1 , wherein the nanofiber nonwoven product comprises less than 5000 ppm solvent.

17. The nanofiber nonwoven product according to claim 1 , wherein the nanofiber nonwoven product has a filtration efficiency from 1 to 99.999%.

18. A nanofiber nonwoven product comprising polyamide nanofibers, wherein the polyamide of the nanofibers comprises a non-nylon polyamide, wherein the polyamide of the nanofibers have a relative viscosity from 4 to 330, and wherein the nanofibers have an average diameter from 100 to 950 nanometers.

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Dec 23, 2025
From: WILMINGTON SAVINGS FUND SOCIETY, FSB
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 074050/0090 →
SECURITY INTEREST Recorded Dec 23, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 074056/0183 →
SECURITY INTEREST Recorded Dec 19, 2025
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 074007/0183 →
SECURITY INTEREST Recorded Apr 10, 2025
From: BANK OF AMERICA, N.A.
To: WILMINGTON SAVINGS FUND SOCIETY, FSB
Reel/Frame 070811/0705 →
SECURITY INTEREST Recorded Dec 8, 2022
From: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
To: WELLS FARGO CAPITAL FINANCE, LLC
Reel/Frame 062094/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2020
From: YUNG, WAI-SHING; OSBORN, SCOTT E.; SCHWIER, CHRIS E.; GOPAL, VIKRAM; ORTEGA, ALBERT
To: ASCEND PERFORMANCE MATERIALS OPERATIONS LLC
Reel/Frame 052950/0058 →
Continuity (4)
Continuation 16003528 · Jun 8, 2018
Provisional Application 62516867 · Jun 8, 2017
Provisional Application 62518769 · Jun 13, 2017
Related Publication 20200283937A1 · Sep 10, 2020