IP Library Granted Patent US 11,925,879
Granted Patent B2
US 11,925,879 · App. 16/894,679 · Granted Mar 12, 2024

Systems and methods for separating radium from lead, bismuth, and thorium

Inventor: Matthew J. O'Hara (Richland, WA)
Assignee: Battelle Memorial Institute
B01D15/203B01D15/1871B01J20/103B01J20/261B01J20/28004B01J20/28016B01J20/283B01J20/285B01J20/3425B01J20/3433B01J20/3475C01G21/003C01G29/003C22B3/42C22B26/20G21G1/001B01J2220/52B01J2220/603
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,925,879
App. No.
16/894,679
Granted
Mar 12, 2024
Kind
B2
Abstract

Methods for separating Ra from Pb, Bi, and Th are provided, the methods can include: providing a first mixture comprising Ra, Pb, Bi, and/or Th; providing a system that can include: a first vessel housing a first media; a second vessel in fluid communication with the first vessel, the second vessel housing a second media; and a third vessel in fluid communication with the second vessel, the third vessel housing a third media; and exposing the first mixture to the first media within the first vessel then, through the fluid communication, exposing the first remainder to the second media in the second vessel, then, through fluid communication, exposing the next remainder to the third media in the third vessel, the exposing separating the Th and Bi from the Ra and Pb, and the Ra from the Pb. Methods for separating Ra from being associated with a media are also provided. The methods can include: exposing the Ra and media to a chelating agent to form a mixture comprising the Ra complexed with the chelating agent.

Claims (11)

1. A method for separating Ra from Pb, Bi, and Th, the method comprising:

providing a first mixture comprising Ra, Pb, Bi, and Th;

providing a system comprising:

a first vessel housing a first media; and

a second vessel in fluid communication with the first vessel, the second vessel housing a second media;

exposing the first mixture to the first media within the first vessel to separate the Th and Bi from the Ra and Pb and form a second mixture comprising the Ra and Pb; then, through the fluid communication, exposing the second mixture to the second media in the second vessel to associate the Pb with the second media and form a third mixture comprising the Ra.

2. The method of claim 1 wherein the Th and Bi are associated with the first media in the first vessel.

3. The method of claim 2 further comprising exposing the first media and Th and Bi to a strong HCl solution to elute the Th and Bi from the first media.

4. The method of claim 2 further comprising drying down the eluant of Th and Bi for storage and/or reuse.

5. The method of claim 1 further comprising exposing the third mixture to a third media to associate the Ra of the third mixture with the third media.

6. The method of claim 5 further comprising exposing the third media associated with the Ra to a chelating solution to remove the Ra.

Assignments (2)
CONFIRMATORY LICENSE Recorded Oct 19, 2020
From: BATTELLE MEMORIAL INSTITUTE, PACIFIC NORTHWEST DIVISION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 054094/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 7, 2020
From: O'HARA, MATTHEW J.
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 054002/0950 →
Continuity (2)
Provisional Application 62857681 · Jun 5, 2019
Related Publication 20210024365A1 · Jan 28, 2021