IP Library Granted Patent US 11,390,826
Granted Patent B2
US 11,390,826 · App. 16/894,729 · Granted Jul 19, 2022

Grease composition, machine component, and starter overrunning clutch

Inventors: Yoshinori Fukushima (Kariya, JP); Koji Sakakibara (Kariya, JP); Youichi Hasegawa (Kariya, JP); Makoto Mori (Kariya, JP); Yuji Masamura (Hadano, JP)
Assignees: DENSO CORPORATION; DUPONT TORAY SPECIALTY MATERIALS KABUSHIKI KAISHA
C10M169/06C10M107/50C10M117/02C10M135/18C10M137/10C10M141/10C10M169/00F16D7/02F16D41/067C10M2207/1265C10M2207/1276C10M2207/1285C10M2219/068C10M2223/045C10M2223/061C10M2229/045C10M2229/0415C10M2229/0425C10M2229/0515C10N2010/02C10N2010/04C10N2030/06C10N2030/08C10N2040/04C10N2050/10
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Quick Facts
Patent No.
US 11,390,826
App. No.
16/894,729
Granted
Jul 19, 2022
Kind
B2
Abstract

A silicone grease composition having high friction characteristics and wear characteristics is disclosed. The silicone grease composition is provided by adding a zinc salt (B) containing, at a mass ratio from 1:99 to 99:1, a zinc dialkyldithiophosphate (B1) and a zinc dialkyldithiocarbamate (B2) as an extreme-pressure additive to a silicone oil (A). A method for transmitting torque of a clutch or a torque limiter mechanism is also disclosed.

Claims (16)

1. A method for increasing the friction of a lubricating part of an overrunning clutch, the overrunning clutch having a clutch cam chamber formed from an outer clutch and an inner clutch, the method comprising enclosing a grease composition in the clutch cam chamber, wherein the grease composition comprises:

a silicone oil (A);

a zinc salt (B) containing, at a mass ratio from 1:99 to 40:60, a zinc dialkyldithiophosphate (B1) and a zinc dialkyldithiocarbamate (B2); and

a thickener (C);

wherein a content of the silicone oil (A) is in a range of not less than 50 mass % and not greater than 95 mass % relative to the entire grease composition;

wherein the silicone oil (A) is a methylphenyl silicone, where the phenyl group content is from 3 to 10 mol % relative to all organic groups;

wherein a content of the zinc salt (B) is not less than 5 mass % and not greater than 30 mass % relative to the entire grease composition;

wherein the zinc dialkyldithiophosphate (B1) is bis(2-ethylhexyl)zinc dithiophosphate and the zinc dialkyldithiocarbamate (B2) is zinc dimethyldithiocarbamate;

wherein the thickener (C) is a lithium complex soap that is a 4:1 mixture of lithium (12-hydroxystearate) and dilithium azelate salt;

wherein a coefficient of friction (COF) of the lubricating part is increased to at least 0.160 relative to the lubricating part without the grease composition, where the COF is measured in accordance with a barbell plate test; and

wherein the barbell plate test includes an opposite material with a barbell shape that is brought into contact with a plate surface, and the plate is rotated while applying a load in this state so as to slide the surface of the opposite material and the plate surface with continuous contact therebetween, where the opposite material is a Fe—Cr alloy steel formed from two discs 13 mm in diameter and 2 mm thick and a shaft connecting the central portions of these two discs, a portion of the opposite material which is in sliding contact with the plate surface is the peripheral edge portion of the discs, where the barbell-type test piece is formed from SCr415 steel and the plate-type test piece is formed from SUJ2 steel, where a state of cylindrical line contact is assumed so as to achieve a stable state of contact with little one-sided contact even under relatively low surface pressure conditions, where the test conditions are: 800N load, 1015 MPa surface pressure, 0.388 m/s sliding rate, 15 s test time, and −30° C. test temperature, and wherein the COF is measured by measuring the torque in the sliding direction with a load cell.

2. The method according to claim 1 , wherein the zinc salt (B) contains the zinc dialkyldithiophosphate (B1) and the zinc dialkyldithiocarbamate (B2) at a mass ratio from 2:98 to 40:60.

3. The method according to claim 1 , wherein the silicone oil (A) is of the general formula

Me 3 SiO(Me 2 SiO) l (R 2 R 3 SiO) m SiMe 3

where Me is a methyl group, R 2 is a methyl group or a phenyl group, R 3 is a phenyl group, l is 0 or a positive integer, and m is a positive integer.

4. The method according to claim 1 , wherein the grease composition further comprises a partial ester (D) of a polyhydric alcohol.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE 2ND ASSIGNEE'S FULL NAME IS "DOW CORNING TORAY CO., LTD." PREVIOUSLY RECORDED AT REEL: 059286 FRAME: 0375. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Mar 21, 2022
From: FUKUSHIMA, YOSHINORI; SAKAKIBARA, KOJI; HASEGAWA, YOUICHI; MORI, MAKOTO; MASAMURA, YUJI
To: DENSO CORPORATION; DOW CORNING TORAY CO., LTD.
Reel/Frame 059452/0707 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 16, 2022
From: FUKUSHIMA, YOSHINORI; SAKAKIBARA, KOJI; HASEGAWA, YOUICHI; MORI, MAKOTO; MASAMURA, YUJI
To: DENSO CORPORATION; DOW CORNING TORAY
Reel/Frame 059286/0375 →
CHANGE OF NAME Recorded Mar 16, 2022
From: DOW CORNING TORAY CO., LTD.
To: DUPONT TORAY SPECIALTY MATERIALS KABUSHIKI KAISHA
Reel/Frame 059370/0602 →
Priority Claims (1)
JP 2016-047996 · Mar 11, 2016 · national
Continuity (2)
Continuation 16082713
Related Publication 20200299607A1 · Sep 24, 2020