IP Library Granted Patent US 11,205,778
Granted Patent B2
US 11,205,778 · App. 16/900,556 · Granted Dec 21, 2021

Conductive polymer emulsion

Inventors: Gao Liu (Piedmont, CA); Tianyue Zheng (Albany, CA)
Assignee: The Regents of the University of California
H01M4/622C08F220/1804C08F220/1818C08J3/07H01B1/20H01M4/386H01M4/387H01M4/625H01M10/0525
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Quick Facts
Patent No.
US 11,205,778
App. No.
16/900,556
Granted
Dec 21, 2021
Kind
B2
Abstract

The present invention provides for an emulsion comprising solid particles of a single composition, or a mixture thereof, comprising a polymer comprising one monomer of an aryl methacrylate, or a mixture thereof, co-polymerized with a monomer of an alkyl methacrylate, or a mixture thereof; wherein Ar is an aryl group and R is an alkyl group, and n:m has a ratio of from about 0:100 to about 100:0.

Claims (31)

1. An emulsion comprising solid particles of a polymer, or a mixture thereof, comprising one monomer of

or a mixture thereof, co-polymerized with a monomer of

or a mixture thereof; wherein Ar is an aryl group and R is any C 2 -C 10 alkyl group, and n:m has a ratio of from 0:100 to 100:0; wherein the polymer comprises at least one monomer of

co-polymerized with at least one monomer of

and Ar is a polycyclic aryl group.

2. The emulsion of claim 1 , wherein the emulsion is aqueous.

3. The emulsion of claim 1 , wherein Ar is any polycyclic aryl group with two, three or four aryl rings.

4. The emulsion of claim 3 , wherein Ar is

5. The emulsion of claim 1 , wherein R is any C 2 -C 5 alkyl group.

6. The emulsion of claim 5 , wherein R is an ethyl, propyl, isopropyl, butyl, s-butyl, isobutyl, or t-butyl group.

7. The emulsion of claim 1 , wherein the solid particles having an average particle size of about 10 nm to about 500 nm.

8. The emulsion of claim 7 , wherein the solid particles having an average particle size of about 50 nm to about 200 nm.

9. The emulsion of claim 7 , wherein the solid particles having an average particle size of about 80 nm to about 500 nm.

10. The emulsion of claim 1 , wherein n:m has a ratio of from 0:100 to about 1:1.

11. The emulsion of claim 1 , wherein the solid particles form at least about 10 weight percent.

12. The emulsion of claim 11 , wherein the solid particles form at least about 20 weight percent.

13. The emulsion of claim 1 , wherein the Ar

monomer is polymerized from naphthalene methacrylate, anthracene methacrylate, pyrene methacrylate, 1-naphthalenemethyl methacrylate, 9-anthracenemethyl methacrylate, or 1-pyrenemethyl methacrylate.

14. A method for making an electrode for use in a lithium ion battery comprising the steps of:

a) forming an emulsion comprising solid particles of a polymer, or a mixture thereof, comprising one monomer of

or a mixture thereof, co-polymerized with a monomer of

or a mixture thereof; wherein Ar is an aryl group and R is any C 2 -C 10 alkyl group, and n:m has a ratio of from 0:100 to 100:0; wherein the polymer comprises at least one monomer of

co-polymerized with at least one monomer of

b) to this solution adding micro or nanoparticles of at least one element selected from the group consisting of: silicon, Sn, and graphite to form a slurry;

c) mixing the slurry to form a homogenous mixture;

d) depositing a thin film of said thus obtained mixture over top of a substrate; and

e) drying the resulting composite to form said silicon electrode.

15. A lithium ion battery having a silicon electrode incorporating solid particles of a polymer, or a mixture thereof, comprising one monomer of

or a mixture thereof, co-polymerized with a monomer of

or a mixture thereof; wherein Ar is an aryl group and R is any C 2 -C 10 alkyl group, and n:m has a ratio of from 0:100 to 100:0; wherein the polymer comprises at least one monomer of

co-polymerized with at least one monomer of

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 16, 2020
From: UNIVERSITY OF CALIF-LAWRENC BERKELEY LAB
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 054666/0257 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 12, 2020
From: LIU, GAO; ZHENG, TIANYUE
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 052932/0401 →
Continuity (2)
Provisional Application 62860725 · Jun 12, 2019
Related Publication 20200395614A1 · Dec 17, 2020