IP Library Granted Patent US 11,551,932
Granted Patent B2
US 11,551,932 · App. 16/905,506 · Granted Jan 10, 2023

Photonuclear transmutation doping in gallium-based semiconductor materials

Inventors: Jae Wan Kwon (Columbia, MO); Quang Nguyen (Columbia, MO)
Assignee: The Curators of the University of Missouri
H01L21/261H01L21/0254H01L21/02614
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Quick Facts
Patent No.
US 11,551,932
App. No.
16/905,506
Granted
Jan 10, 2023
Kind
B2
Abstract

The present invention relates to various high quality n-type and p-type doped gallium-based semiconductor materials, electronic components incorporating these materials, and processes of producing these materials. In particular, The present invention relates processes to achieve high quality, uniform doping of a whole wafer or a thin layer of gallium-based semiconductor materials for various applications such as a vertical power transistor or diode.

Claims (21)

1. A process for producing a doped gallium-based semiconductor material comprising:

irradiating a gallium-based semiconductor workpiece with gamma rays in a photonuclear reaction to effect transmuting at least a portion of Ga in the workpiece to Zn and/or Ge to produce the doped gallium-based semiconductor material,

wherein the gallium-based semiconductor workpiece comprises at least one other component selected from group consisting of N, O, Sb, In, and combinations thereof.

2. The process of claim 1 , wherein Ga is transmuted to Zn.

3. The process of claim 1 , wherein 69 Ga is transmuted to 68 Zn and/or 71 Ga is transmuted to 70 Zn.

4. The process of claim 1 , wherein the gamma rays have an incident photon energy that is 7.5 MeV or more.

5. The process of claim 1 , wherein the gamma rays have an incident photon energy that is 20.5 MeV or less.

6. The process of claim 2 , wherein the gamma rays have an incident photon energy that is in the range of from 7.5 MeV to 10 MeV.

7. The process of claim 1 , wherein the doped gallium-based semiconductor material is a p-type doped gallium-based semiconductor material.

8. The process of claim 1 , wherein Ga is transmuted to Ge.

9. The process of claim 8 , wherein the gamma rays have an incident photon energy that is 9.5 MeV or more.

10. The process of claim 8 , wherein the gamma rays have an incident photon energy that is in the range of from 9.5 MeV to 50 MeV.

11. The process of claim 1 , wherein the doped gallium-based semiconductor material is a n-type doped gallium-based semiconductor material.

12. The process of claim 1 , further comprising shielding a first region of the gallium-based semiconductor workpiece with a high-Z material during irradiation to selectively dope a second region of the workpiece that is unshielded.

13. The process of claim 12 , wherein the high-Z material comprises at least one component selected from the group consisting of Pb, W, Bi, Sn, Sb, Fe, Pt, Ta, a composite thereof, and metal foam thereof.

14. The process of claim 1 , wherein the gallium-based semiconductor workpiece comprises GaN.

15. The process of claim 1 , further comprising annealing the doped gallium-based semiconductor material.

16. The process of claim 1 , wherein the doped gallium-based semiconductor material is not radioactive after irradiation.

17. A process for producing a doped gallium-based semiconductor material comprising:

irradiating a gallium-based semiconductor workpiece with gamma rays in a photonuclear reaction to effect transmuting at least a portion of Ga in the workpiece to Zn and/or Ge to produce the doped gallium-based semiconductor material,

wherein the gallium-based semiconductor workpiece comprises gallium oxide.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jan 12, 2024
From: UNIVERSITY OF MISSOURI-COLUMBIA
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 066286/0631 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNOR: LORENZEN, LISA PREVIOUSLY RECORDED ON REEL 053405 FRAME 0169. ASSIGNOR(S) HEREBY CONFIRMS THE REMOVAL OF ASSIGNOR: LORENZEN, LISA WHO IS NOT AN ASSIGNOR, RATHER SIGNED ACCEPTANCE OF THE ASSIGNMENT OF BEHALF OF THE ASSIGNEE. Recorded Sep 3, 2020
From: KWON, JAE WAN; NGUYEN, QUANG
To: THE CURATORS OF THE UNIVERSITY OF MISSOURI
Reel/Frame 053682/0441 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2020
From: KWON, JAE WAN; NGUYEN, QUANG; LORENZEN, LISA
To: THE CURATORS OF THE UNIVERSITY OF MISSOURI
Reel/Frame 053405/0169 →
Continuity (2)
Provisional Application 62863010 · Jun 18, 2019
Related Publication 20200402802A1 · Dec 24, 2020