IP Library Granted Patent US 11,661,401
Granted Patent B2
US 11,661,401 · App. 16/905,884 · Granted May 30, 2023

2,5-disubstituted 3-methyl pyrazines and 2,5,6-trisubstituted 3-methyl pyrazines as allosteric SHP2 inhibitors

Inventors: Elena S. Koltun (Redwood City, CA); Kevin Mellem (Redwood City, CA); Adrian Gill (Redwood City, CA); Gert Kiss (Redwood City, CA); Christopher Semko (Redwood City, CA); Naing Aay (Redwood City, CA); Andreas Buckl (Redwood City, CA); Ashutosh Jogalekar (Redwood City, CA); Walter Won (Redwood City, CA)
Assignee: REVOLUTION MEDICINES, INC.
C07D241/20A61P35/02A61P35/04C07D241/18C07D401/04C07D403/04C07D403/12C07D477/26C07D487/04
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Quick Facts
Patent No.
US 11,661,401
App. No.
16/905,884
Granted
May 30, 2023
Kind
B2
Abstract

The present disclosure is directed to inhibitors of SHP2, such as pyrazine compounds, and their use in the treatment of disease associated with SHP2 modulation, such as Noonan Syndrome, Leopard Syndrome, juvenile myelomonocytic leukemias, neuroblastoma, melanoma, acute myeloid leukemia and cancers of the breast, lung and colon. Also disclosed are pharmaceutical compositions comprising the same.

Claims (25)

1. A compound of Formula I-W:

or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein:

A is aryl;

Y 1 is —C(═CH 2 )—;

Y 2 is —NR a ; wherein the bond on the left side of Y 2 , as drawn, is bound to the pyrazine ring and the bond on the right side of the Y 2 moiety, as drawn, is bound to R 3 ;

R 1 is independently, at each occurrence, —H, -D, —C 1 -C 6 alkyl, —C 2 -C 6 alkenyl, —C 4 -C 8 cycloalkenyl, —C 2 -C 6 alkynyl, —C 3 -C 8 cycloalkyl, —OH, —OR 6 , halogen, —NO 2 , —CN, —NR 5 R 6 , —SR 5 , —S(O) 2 NR 5 R 6 , —S(O) 2 R 5 , —NR 5 S(O) 2 NR 5 R 6 , —NR 5 S(O) 2 R 6 , —S(O)NR 5 R 6 , —S(O)R 5 , —NR 5 S(O)NR 5 R 6 , —NR 5 S(O)R 6 , —C(O)R 5 , —CO 2 R 5 , —C(O)NR 5 R 6 , —NR 5 C(O)R 6 , monocyclic or polycyclic heterocyclyl, spiroheterocyclyl, heteroaryl, or oxo, wherein each alkyl, alkenyl, cycloalkenyl, alkynyl, cycloalkyl, heterocyclyl, spiroheterocyclyl, or heteroaryl is optionally substituted with one or more —OH, —NO 2 , oxo, —CN, —R 5 , —OR 5 , —NR 5 R 6 , —SR 5 , —S(O) 2 NR 5 R 6 , —S(O) 2 R 5 , —NR 5 S(O) 2 NR 5 R 6 , —NR 5 S(O) 2 R 6 , —S(O)NR 5 R 6 , —S(O)R 5 , —NR 5 S(O)NR 5 R 6 , —NR 5 S(O)R 6 , heterocycle, aryl, or heteroaryl;

R 2 is —C 1 -C 6 alkyl;

R b is independently, at each occurrence, —H, -D, —OH, —C 1 -C 6 alkyl, —C 3 -C 8 cycloalkyl, —C 2 -C 6 alkenyl, —(CH 2 ) n -aryl, heterocyclyl containing 1-5 heteroatoms selected from the group consisting of N, S, P, and O, or heteroaryl containing 1-5 heteroatoms selected from the group consisting of N, S, P, and O; wherein each alkyl, cycloalkyl, alkenyl, heterocycle, heteroaryl, or —(CH 2 ) n -aryl is optionally substituted with one or more —OH, halogen, —NO 2 , oxo, —CN, —R 5 , —OR 5 , —NR 5 R 6 , —SR 5 , —S(O) 2 NR 5 R 6 , —S(O) 2 R 5 , —NR 5 S(O) 2 NR 5 R 6 , —NR 5 S(O) 2 R 6 , —S(O)NR 5 R 6 , —S(O)R 5 , —NR 5 S(O)NR 5 R 6 , —NR 5 S(O)R 6 , —C(O)NR 5 R 6 , —NR 5 C(O)R 6 , heterocycle, aryl, heteroaryl, —(CH 2 ) n OH, —C 1 -C 6 alkyl, —CF 3 , —CHF 2 , or —CH 2 F;

R 3 combines with R a to form a 3- to 12-membered monocyclic or polycyclic heterocycle or a 5- to 12-membered spiroheterocycle, wherein each heterocycle or spiroheterocycle is optionally substituted with one or more —C 1 -C 6 alkyl, halogen, —OH, —OR b , —NH 2 , —NHR b , heteroaryl, heterocyclyl, —(CH 2 ) n NH 2 , —(CH 2 ) n OH, —COOR b , —CONHR b , —CONH(CH 2 ) n COOR b , —NHCOOR b , —CF 3 , —CHF 2 , —CH 2 F, or ═O;

R 4 is —H;

R 5 is independently —H, -D, —C 1 -C 6 alkyl, —C 2 -C 6 alkenyl, —C 4 -C 8 cycloalkenyl, —C 2 -C 6 alkynyl, —C 3 -C 8 cycloalkyl, a monocyclic or polycyclic 3- to 12-membered heterocycle, —OR 7 , —SR 7 , —NR 7 R 8 , —NO 2 , —CF 3 , or —CN;

R 6 is independently —H, -D, —C 1 -C 6 alkyl, —C 2 -C 6 alkenyl, —C 4 -C 8 cycloalkenyl, —C 2 -C 6 alkynyl, —C 3 -C 8 cycloalkyl, a monocyclic or polycyclic 3- to 12-membered heterocycle, —OR 7 , —SR 7 , halogen, —NR 7 R 8 , —NO 2 , —CF 3 , or —CN;

R 7 and R 8 are independently, at each occurrence, —H, -D, —C 1 -C 6 alkyl, —C 2 -C 6 alkenyl, —C 4 -C 8 cycloalkenyl, —C 2 -C 6 alkynyl, —C 3 -C 8 cycloalkyl, —OR b , or a monocyclic or polycyclic 3- to 12-membered heterocycle, wherein each alkyl, alkenyl, cycloalkenyl, alkynyl, cycloalkyl, or heterocycle is optionally substituted with one or more —OH, —SH, —NH 2 , —NO 2 , or —CN;

and

n is independently, at each occurrence, 0, 1, 2, 3, 4, 5, 6, 7, 8, 9, or 10.

2. The compound of claim 1 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein R 3 and R a together with the atoms to which they are attached combine to form a 5- to 12-membered spiroheterocycle, which is optionally substituted with —C 1 -C 6 alkyl, —OH, —NH 2 , heteroaryl, heterocyclyl, —(CH 2 ) n NH 2 , —COOR b , —CONHR b , —CONH(CH 2 ) n COOR b , —NHCOOR b , —CF 3 , —CHF 2 , or —CH 2 F.

3. The compound of claim 2 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein 5- to 12-membered spiroheterocycle comprises piperidinyl.

4. The compound of claim 3 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein 5- to 12-membered spiroheterocycle comprises an oxygen.

5. The compound of claim 1 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein R 3 and R a together with the atom to which they are attached combine to form a 3- to 12-membered monocyclic heterocycle, which is optionally substituted with —C 1 -C 6 alkyl, —OH, —NH 2 , heteroaryl, heterocyclyl, —(CH 2 ) n NH 2 , —COOR b , —CONHR b , —CONH(CH 2 ) n COOR b , —NHCOOR b , —CF 3 , —CHF 2 , or —CH 2 F.

6. The compound of claim 1 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, wherein R 3 and R a together with the atoms to which they are attached combine to form a 3- to 12-membered polycyclic heterocycle, which is optionally substituted with —C 1 -C 6 alkyl, —OH, —NH 2 , heteroaryl, heterocyclyl, —(CH 2 ) n NH 2 , —COOR b , —CONHR b , —CONH(CH 2 ) n COOR b , —NHCOOR b , —CF 3 , —CHF 2 , or —CH 2 F.

7. The compound of claim 1 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, where the compound is

8. The compound of claim 1 , wherein R 1 is independently, at each occurrence, —C 1 -C 6 alkyl, halogen, or —NR 5 R 6 .

9. The compound of claim 1 , wherein R 1 is independently selected from methyl, fluoro, chloro, and —NH 2 .

10. The compound of claim 1 , wherein n is 1 or 2.

11. A pharmaceutical composition comprising a compound claim 1 , or a pharmaceutically acceptable salt, solvate, hydrate, or tautomer thereof, and a pharmaceutically acceptable carrier.

Assignments (2)
SECURITY INTEREST Recorded Jun 25, 2025
From: REVOLUTION MEDICINES, INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS AGENT
Reel/Frame 071721/0025 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2022
From: KOLTUN, ELENA S.; MELLEM, KEVIN; GILL, ADRIAN; KISS, GERT; SEMKO, CHRISTOPHER; AAY, NAING; BUCKL, ANDREAS; JOGALEKAR, ASHUTOSH; WON, WALTER
To: REVOLUTION MEDICINES, INC.
Reel/Frame 061737/0219 →
Continuity (6)
Continuation 16694588 · Nov 25, 2019
Continuation 16228324 · Dec 20, 2018
Continuation PCTUS2017041577 · Jul 11, 2017
Provisional Application 62449523 · Jan 23, 2017
Provisional Application 62361249 · Jul 12, 2016
Related Publication 20210101870A1 · Apr 8, 2021