IP Library Granted Patent US 11,795,829
Granted Patent B2
US 11,795,829 · App. 16/906,298 · Granted Oct 24, 2023

Reactive thermal barrier coating

Inventors: Brian T. Hazel (Avon, CT); Elisa M. Zaleski (Manchester, CT); Kaylan M. Wessels (West Hartford, CT)
Assignee: RTX Corporation
F01D5/282B32B15/04B32B18/00C23C4/11C23C4/134C23C4/18C23C14/06C23C14/08C23C14/081C23C14/082C23C14/083C23C14/086C23C14/088C23C14/22C23C14/28C23C14/30C23C14/34C23C14/3492C23C16/40C23C16/405C23C16/409C23C16/45525C23C28/04C23C28/042C23C28/30C23C28/3215C23C28/345C23C28/3455C23C30/00C23C30/005F01D5/28F01D5/284F01D5/288F01D25/005F01D25/08C04B2237/34C04B2237/343C04B2237/348Y10T428/1259Y10T428/12597Y10T428/12611Y10T428/12618Y10T428/2495Y10T428/24967Y10T428/265
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Quick Facts
Patent No.
US 11,795,829
App. No.
16/906,298
Granted
Oct 24, 2023
Kind
B2
Abstract

A calcium-magnesium-alumino-silicate (CMAS)-reactive thermal barrier coating includes a ceramic coating and a CMAS-reactive overlay coating, wherein the CMAS-reactive overlay coating conforms to a surface of the ceramic coating and comprises a compound that forms a stable high melting point crystalline precipitate when reacted with molten CMAS at a rate that is competitive with CMAS infiltration kinetics into the thermal barrier coating. The ceramic coating phase is stable with the CMAS-reactive overlay coating.

Claims (11)

1. A calcium-magnesium-alumino-silicate (CMAS)-reactive thermal barrier coating comprising:

a ceramic coating comprising a plurality of featherlike columnar grains separated by vertically-oriented gaps open to an outer surface, wherein the ceramic coating comprises a fully stabilized zirconate or hafnate structure; and

a CMAS-reactive overlay coating forming a conformal layer with uniform surface coverage on surfaces of the featherlike grains extending into the vertically-oriented gaps, wherein the vertically-oriented gaps remain open to the outer surface, and wherein the CMAS-reactive overlay coating comprises a compound selected from a group consisting of a pure rare earth oxide and a mixed rare earth oxide that forms a crystalline precipitate when reacted with molten CMAS at a rate substantially equal to or greater than a rate at which the molten CMAS infiltrates through the thermal barrier coating;

wherein the ceramic coating is phase stable with the CMAS-reactive overlay coating.

2. The CMAS-reactive thermal barrier coating of claim 1 , wherein the ceramic coating comprises gadolinium zirconate.

3. The CMAS-reactive thermal barrier coating of claim 1 , wherein the ceramic coating comprises yttrium zirconate.

4. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay is deposited in pores open to the vertically-oriented gaps.

5. The CMAS-reactive thermal barrier coating of claim 4 , wherein the thickness of the CMAS-reactive overlay ranges from 10 to 500 nanometers.

6. The CMAS-reactive thermal barrier coating of claim 4 , wherein the CMAS-reactive overlay extends into the vertically-oriented gaps to a depth of at least one-third of a thickness of the ceramic coating from the outer surface of the ceramic coating.

7. The CMAS-reactive thermal barrier coating of claim 6 , wherein the CMAS-reactive overlay extends into the vertically-oriented gaps to a depth of at least one-half of a thickness of the ceramic coating from an outer surface of the ceramic coating.

8. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay has a material composition that will react with molten CMAS to form an oxy-apatite phase.

Assignments (2)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064402/0837 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2021
From: HAZEL, BRIAN T.; ZALESKI, ELISA M.; WESSELS, KAYLAN M.
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054856/0457 →
Continuity (2)
Provisional Application 62864624 · Jun 21, 2019
Related Publication 20200400028A1 · Dec 24, 2020
Cited By (1)
US 12,196,109