IP Library Granted Patent US 12,110,312
Granted Patent B2
US 12,110,312 · App. 16/908,401 · Granted Oct 8, 2024

Integrated continuous manufacturing of therapeutic protein drug substances

Inventors: Konstantin Konstantinov (Bridgewater, NJ); Rahul Godawat (Bridgewater, NJ); Veena Warikoo (Bridgewater, NJ); Sujit Jain (Bridgewater, NJ)
Assignee: Genzyme Corporation
C07K1/22B01D15/1807B01D15/1864B01D15/1871B01D15/327B01D15/34B01D15/362B01D15/363B01D15/3809B01D15/3814B01D15/422C07K1/16C07K1/18C07K1/36C07K16/00C12M23/52C12M47/10C12M47/12C12N9/00C12N9/2402C12N9/2465C12P21/00C12P21/005C12Y302/01022C12Y302/01045C07K2317/14
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Quick Facts
Patent No.
US 12,110,312
App. No.
16/908,401
Granted
Oct 8, 2024
Kind
B2
Abstract

Provided herein are integrated continuous biomanufacturing processes for producing a therapeutic protein drug substance. Also provided are systems that are capable of continuously producing a therapeutic protein drug substance.

Claims (21)

1. A process for manufacturing a recombinant therapeutic protein drug substance, the process comprising:

(a) introducing one or both of liquid culture medium or nutrients into a cell culture disposed in a perfusion bioreactor, wherein cells in the cell culture secrete a recombinant therapeutic protein;

(b) monitoring cell density in the cell culture disposed in the perfusion bioreactor;

(c) continuously flowing the cell culture from the perfusion bioreactor into a cell retention system;

(d) continuously removing a liquid comprising the recombinant therapeutic protein that is substantially free of cells from the cell retention system;

(e) feeding the liquid into a first multi-column chromatography system (MCCS);

(f) capturing the recombinant therapeutic protein in the liquid using the first MCCS; and

(g) purifying and polishing the recombinant therapeutic protein using a second MCCS, wherein the purifying is performed using a resin in the second MCCS that is different in chemical structure compared to the resin in the second MCCS used to perform the polishing.

2. The process of claim 1 , wherein the use of the first MCCS involves column switching.

3. The process of claim 1 , wherein the first MCCS utilizes at least two chromatography columns.

4. The process of claim 1 , wherein the first MCCS utilizes at least one chromatography column and at least one chromatographic membrane.

5. The process of claim 1 , wherein the first MCCS is a periodic counter current chromatography system (PCCS).

6. The process of claim 5 , wherein the PCCS comprises a four-column PCCS.

7. The process of claim 1 , wherein the capturing is performed using affinity chromatography, cation exchange chromatography, anion exchange chromatography, or molecular sieve chromatography.

8. The process of claim 7 , wherein the affinity chromatography is performed with a capture mechanism selected from the group consisting of: protein A-binding capture mechanism, substrate-binding capture mechanism, antibody- or antibody fragment-binding capture mechanism, aptamer-binding capture mechanism, and cofactor-binding capture mechanism.

9. The process of claim 1 , further comprising formulating the recombinant therapeutic protein drug substance into a pharmaceutical composition.

10. The process of claim 1 , wherein the process is performed over a continuous period of at least about 10 days.

11. The process of claim 1 , wherein the process is performed for a continuous period of at least about 30 days.

12. The process of claim 1 , wherein the cell retention system filters the cell culture.

13. The process of claim 1 , wherein the cell retention system is an alternating tangential flow system.

14. The process of claim 1 , wherein the process further comprises performing viral inactivation on the liquid.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2020
From: KONSTANTINOV, KONSTANTIN; GODAWAT, RAHUL; WARIKOO, VEENA; JAIN, SUJIT
To: GENZYME CORPORATION
Reel/Frame 053509/0024 →
Continuity (6)
Continuation 15493523 · Apr 21, 2017
Continuation 14645138 · Mar 11, 2015
Continuation 14195481 · Mar 3, 2014
Provisional Application 61856390 · Jul 19, 2013
Provisional Application 61775060 · Mar 8, 2013
Related Publication 20200317726A1 · Oct 8, 2020