IP Library Granted Patent US 11,794,208
Granted Patent B2
US 11,794,208 · App. 16/932,855 · Granted Oct 24, 2023

Fluidized-bed coating method and fluidized-bed coating apparatus

Inventors: Makoto Furuki (Kanagawa, JP); Susumu Yoshino (Kanagawa, JP); Hiroshi Saegusa (Kanagawa, JP); Satoshi Yoshida (Kanagawa, JP)
Assignee: FUJIFILM Business Innovation Corp.
B05D1/24B05C3/04B05C3/09B05C11/045B05C19/02B05D1/20B05D3/0218B05D3/0254C08K3/36C09D5/031C09D5/033C09D125/06C09D133/12
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Quick Facts
Patent No.
US 11,794,208
App. No.
16/932,855
Granted
Oct 24, 2023
Kind
B2
Abstract

A fluidized-bed coating method includes: immersing at least part of a workpiece in a powder coating material contained in a fluidized-bed vessel while air is introduced from a bottom of the fluidized-bed vessel at an average air flow rate of 5 mm/min or higher and 20 mm/min or lower per unit area of the bottom so that a floating ratio of the powder coating material is 5% or higher and 20% or lower, the workpiece having a temperature higher than or equal to a softening temperature of the powder coating material and lower than or equal to a melting temperature of the powder coating material; taking the workpiece out of the powder coating material; and heating the powder coating material attached to the workpiece.

Claims (16)

1. A fluidized-bed coating method comprising:

immersing at least part of a workpiece in a powder coating material contained in a fluidized-bed vessel while air is introduced from a bottom of the fluidized-bed vessel at an average air flow rate of 5 mm/min or higher and 20 mm/min or lower per unit area of the bottom so that a floating ratio of the powder coating material is 5% or higher and 20% or lower;

taking the workpiece out of the powder coating material; and

heating the powder coating material attached to the workpiece,

wherein when the at least part of the workpiece is immersed in the powder coating material, a surface temperature of an immersed portion of the workpiece decreases by at least 5° C. from a preheating temperature due to conveyance before the immersion and heat conduction to contact particles of the powder coating material during the immersion, and is then maintained in a range of from a softening temperature of the powder coating material to a melting temperature of the powder coating material for at least 5 seconds after the immersion,

wherein the softening temperature of the powder coating material is a glass transition temperature of the powder coating material and is in a range of 45° C. to 70° C., and the melting temperature of the powder coating material is in a range of 80° C. to 180° C.,

wherein the powder coating material has a volume average particle diameter D50v of 5 μm or more and 20 μm or less,

wherein the workpiece is preheated to the preheating temperature before the conveyance and the immersion, and the preheating temperature is set in a range of from a temperature 20° C. higher than the softening temperature of the powder coating material to a temperature 5° C. higher than the melting temperature of the powder coating material.

2. The fluidized-bed coating method according to claim 1 , wherein an immersion time for the at least part of the workpiece is 5 seconds or longer and 10 seconds or shorter.

3. The fluidized-bed coating method according to claim 1 , wherein the powder coating material has an aerated flowability energy AE of 5 mJ or higher and lower than 100 mJ, where the AE is measured with a powder rheometer using a vessel having a cross-sectional area with Ø 50 mm under conditions of a rotary blade tip speed of 100 mm/sec, a rotary blade helix angle of −5°, and an air flow rate of 20 ml/min.

4. The fluidized-bed coating method according to claim 1 , wherein the powder coating material has a volume particle size distribution index GSDv of 1.15 or higher and 1.40 or lower.

5. The fluidized-bed coating method according to claim 4 , wherein the powder coating material has a volume particle size distribution index GSDv of 1.15 or higher and 1.25 or lower.

6. The fluidized-bed coating method according to claim 1 , wherein the floating ratio is 10% or higher and 20% or lower.

7. The fluidized-bed coating method according to claim 1 , wherein the powder coating material includes powder particles and an external additive on the powder particles.

8. The fluidized-bed coating method according to claim 7 , wherein the external additive is a hydrophobic external additive.

9. The fluidized-bed coating method according to claim 7 , wherein the external additive has a volume average particle diameter of 5 nm or more and 30 rim or less.

Assignments (2)
CHANGE OF NAME Recorded May 13, 2021
From: FUJI XEROX CO., LTD.
To: FUJIFILM BUSINESS INNOVATION CORP.
Reel/Frame 056222/0855 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2020
From: FURUKI, MAKOTO; YOSHINO, SUSUMU; SAEGUSA, HIROSHI; YOSHIDA, SATOSHI
To: FUJI XEROX CO., LTD.
Reel/Frame 053322/0876 →
Priority Claims (1)
JP 2020-058594 · Mar 27, 2020 · national
Continuity (1)
Related Publication 20210299699A1 · Sep 30, 2021