IP Library › Granted Patent US 11,185,791
Granted Patent B2
US 11,185,791 · App. 16/935,696 · Granted Nov 30, 2021

Rotary evaporator capable of accurately quantifying concentrated liquid and/or distillate

Inventor: Shuyao Wen (Beijing, CN)
Assignee: Beijing Normal University
B01D3/085B01D1/0023B01D3/42B01D5/006B01L3/0289B01L2200/0605
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Quick Facts
Patent No.
US 11,185,791
App. No.
16/935,696
Granted
Nov 30, 2021
Kind
B2
Abstract

The present invention provides a rotary evaporator capable of accurately quantifying concentrated liquid and/or distillate. A distillation flask is improved into a structure having a liquid discharge opening formed at the bottom, and/or a spherical collecting flask is improved into a structure having a liquid release opening formed at the bottom. Concentrated liquid and/or distillate can be discharged without dismounting the distillation flask and/or the collecting flask. In addition, fine metering scale tubes and quantitative capacity increase units are disposed at the liquid discharge opening and/or the liquid release opening, there is a valve on the top and another valve on the bottom of each tube, so that the constant subtle changes of the amount of concentrated liquid and/or distillate can be observed, and an accurate amount of concentrated liquid and/or distillate can be discharged.

Claims (24)

1. A rotary evaporator capable of quantifying a concentrated liquid, comprising a support frame, a distillation flask and a condenser dismountably fixed on the support frame, and a concentrated liquid quantification assembly,

wherein the distillation flask is configured to be heated through a heating assembly, and a bottom of the condenser is connected with a collecting flask;

wherein a distillation flask liquid discharge opening is at a bottom portion of the distillation flask, and the distillation flask liquid discharge opening is connected with the concentrated liquid quantification assembly for quantifying the concentrated liquid;

wherein the concentrated liquid quantification assembly includes a quantitative tube with quantitative scale lines, a first liquid discharge valve and a second liquid discharge valve, liquid discharge of the concentrated liquid and sealing of the distillation flask are controllable through the second liquid discharge valve disposed at a bottom of the quantitative tube;

wherein the first liquid discharge valve is disposed at the distillation flask liquid discharge opening, and is configured to control discharge of the concentrated liquid and sealing of the distillation flask; and

wherein the heating assembly is an electric heating belt disposed at an outer wall of the distillation flask.

2. The rotary evaporator according to claim 1 , wherein a tail end of the concentrated liquid quantification assembly away from the distillation flask liquid discharge opening is connected with one of a plurality of first containers in a sealed way through glass ground openings and a clamp, and the plurality of first containers are configured to increase capacity in liquid discharge of the concentrated liquid.

3. The rotary evaporator of claim 2 , wherein the plurality of first containers comprise containers with different capacities, and are configured to be selected and replaced according to the capacity of the concentrated liquid.

4. The rotary evaporator according to claim 1 , wherein a temperature controller sensor probe is further disposed between the electric heating belt and the distillation flask.

5. The rotary evaporator according to claim 1 , wherein the quantitative tube includes a spherical expansion portion at a lower part.

6. A rotary evaporator capable of quantifying concentrated liquid and distillate, comprising a support frame, a distillation flask and a condenser dismountably fixed on the support frame, and at least one of a concentrated liquid quantification assembly and a distillate quantification assembly,

wherein the distillation flask is heated through a heating assembly, and a bottom of the condenser is connected with a collecting flask;

wherein a distillation flask liquid discharge opening is at bottom portion of the distillation flask, and the distillation flask liquid discharge opening is connected with the concentrated liquid quantification assembly for quantifying the concentrated liquid;

wherein the concentrated liquid quantification assembly includes a quantitative tube with quantitative scale lines, a first liquid discharge valve and a second liquid discharge valve, liquid discharge of the concentrated liquid and sealing of the distillation flask are controllable through the second liquid discharge valve disposed at a bottom of the quantitative tube;

wherein the first liquid discharge valve is disposed at the distillation flask liquid discharge opening, and is configured to control discharge of the concentrated liquid and sealing of the distillation flask;

wherein the heating assembly is an electric heating belt disposed at an outer wall of the distillation flask;

wherein a collecting flask liquid release opening is at a bottom of the collecting flask, and the collecting flask liquid release opening is connected with the distillate quantification assembly for measuring the distillate;

wherein the distillate quantification assembly includes a metering tube with metering scale lines, a first liquid release valve and a second liquid release valve, liquid discharge of the distillate and sealing are controllable through the second liquid release valve disposed at a bottom of the metering tube; and

wherein the first liquid release valve is disposed at the collecting flask liquid release opening, and is configured to control distillate discharge and sealing.

7. The rotary evaporator according to claim 6 , wherein a tail end of the concentrated liquid quantification assembly away from the distillation flask liquid discharge opening is connected with a first container in a sealed way through glass ground openings and a clamp, and the first container is configured to increase capacity in liquid discharge of the concentrated liquid.

8. The rotary evaporator according to claim 6 , where

a tail end of the distillate quantification assembly away from the collecting flask liquid discharge opening is connected with a second container in a sealed way through glass ground openings and a clamp, and the second container is configured to increase capacity in liquid discharge of the distillate.

9. The rotary evaporator according to claim 6 , wherein the quantitative tube includes a spherical expansion portion at a lower part.

10. The rotary evaporator according to claim 6 , wherein the metering tube includes a spherical expansion portion at a lower part.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 22, 2020
From: WEN, SHUYAO
To: BEIJING NORMAL UNIVERSITY
Reel/Frame 053281/0091 →
Priority Claims (2)
CN 201810061892.4 · Jan 23, 2018 · national
CN 201810061916.6 · Jan 23, 2018 · national
Continuity (2)
Continuation PCTCN2018121938 · Dec 19, 2018
Related Publication 20200346132A1 · Nov 5, 2020