IP Library Granted Patent US 11,717,792
Granted Patent B2
US 11,717,792 · App. 16/939,761 · Granted Aug 8, 2023

Materials and methods for photothermal membrane distillation

Inventors: Young-Shin Jun (St. Louis, MO); Srikanth Singamaneni (St. Louis, MO); Xuanhao Wu (St. Louis, MO); Qisheng Jiang (St. Louis, MO)
Assignee: Washington University
B01D67/0093B01D61/364B01D69/02B01D69/144B01D71/34C02F1/447B01D2325/38
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Quick Facts
Patent No.
US 11,717,792
App. No.
16/939,761
Granted
Aug 8, 2023
Kind
B2
Abstract

A photothermal distillation membrane comprising a tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS) fluoro-silanized, polydopamine (PDA) coated, polyvinylidene fluoride (PVDF) membrane is disclosed, as well as a process for synthesizing a FTCS-PDA-PVDF membrane. A tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS) fluoro-silanized, polydopamine (PDA) containing bacterial nanocellulose (BNC) aerogel membrane is also disclosed, as well as a process for synthesizing a FTCS-PDA/BNC aerogel membrane.

Claims (23)

1. A photothermal membrane comprising tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS) and a polydopamine (PDA) coated, polyvinylidene fluoride (PVDF) membrane.

2. The photothermal membrane of claim 1 , wherein the photothermal membrane is hydrophobic.

3. The photothermal membrane of claim 1 , wherein the photothermal membrane has a solar efficiency of at least about 10%.

4. The photothermal membrane of claim 1 , wherein the photothermal membrane has a permeate flux of at least about 0.40 kg m −2 h −1 .

5. A process for synthesizing a photothermal membrane according to claim 1 , the process comprising:

coating a polyvinylidene fluoride (PVDF) membrane with polydopamine (PDA); and

fluorinating the PDA-coated PVDF membrane by coating the PDA-coated PVDF membrane with tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS).

6. The process of claim 5 , wherein the coating is achieved via in situ oxidative polymerization of dopamine or adsorption of pre-synthesized PDA.

7. The process of claim 5 , wherein the fluorination of the PDA-coated PVDF membrane is achieved via fluoro-silanization with tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS).

8. A photothermal aerogel membrane comprising a fluorine-containing organic molecule and polydopamine (PDA)-containing bacterial nanocellulose (BNC), wherein the photothermal aerogel membrane is hydrophobic.

9. The photothermal aerogel membrane of claim 8 , wherein the photothermal aerogel membrane is a bilayer membrane.

10. The photothermal aerogel membrane of claim 9 , wherein the bilayer membrane comprises a photothermal layer and a heat insulating layer.

11. The photothermal aerogel membrane of claim 10 , wherein the photothermal layer is a PDA-loaded BNC layer and wherein the heat insulating layer is a pristine BNC layer.

12. The photothermal aerogel membrane of claim 8 , wherein the photothermal aerogel membrane is self-disinfecting.

13. The photothermal aerogel membrane of claim 8 , wherein the photothermal aerogel membrane has a solar efficiency of at least about 10%.

14. The photothermal aerogel membrane of claim 8 , wherein the photothermal aerogel membrane has a permeate flux of at least about 1.0 kg m −2 h −1 .

15. A process for synthesizing a photothermal aerogel membrane according to claim 8 , the process comprising:

incorporating polydopamine (PDA) particles into a bacterial nanocellulose (BNC) hydrogel; and

fluorinating the PDA-containing BNC hydrogel by coating the PDA-containing BNC hydrogel with a fluorine-containing organic molecule.

16. The process of claim 15 , wherein the BNC hydrogel is synthesized from a Gluconacetobacter hansenii culture.

17. The process of claim 15 , wherein the PDA particles are spherical.

18. The process of claim 15 , further comprising freeze-drying the PDA-containing BNC hydrogel prior to the fluorination.

19. The process of claim 15 , wherein the fluorination is achieved via a fluoro-silanization with tridecafluoro-1,1,2,2-tetrahydrooctyl-trichlorosilane (FTCS).

Assignments (3)
CONFIRMATORY LICENSE Recorded May 23, 2023
From: WASHINGTON UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 064105/0390 →
CONFIRMATORY LICENSE Recorded Jan 8, 2021
From: WASHINGTON UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 054942/0765 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 3, 2020
From: JUN, YOUNG-SHIN; SINGAMANENI, SRIKANTH; WU, XUANHAO; JIANG, QISHENG
To: WASHINGTON UNIVERSITY
Reel/Frame 053382/0866 →
Continuity (2)
Provisional Application 62878907 · Jul 26, 2019
Related Publication 20210023505A1 · Jan 28, 2021