Graphene preparation apparatus using Joule heating and preparation method therefor
Provided are a graphene preparation apparatus, including: a chamber having a space for preparation of graphene; a first electrode and a second electrode disposed in the chamber to be separated a predetermined distance from each other, the first electrode and the second electrode supporting a catalytic metal and receiving electric current for preparation of the graphene to heat the catalytic metal using Joule heating; additional heaters disposed at opposite sides of the catalytic metal, respectively, and heating the catalytic metal to compensate for a temperature difference between both end regions and a central region of the catalytic metal heated using Joule heating induced by the first electrode and the second electrode; and a current supply unit supplying electric current to the first electrode and the second electrode.
1. A graphene preparation apparatus using Joule heating, comprising:
a chamber having a space for preparation of graphene;
a first electrode and a second electrode disposed in the chamber to be separated a predetermined distance from each other, the first electrode and the second electrode supporting a catalytic metal and receiving electric current for preparation of the graphene to heat the catalytic metal using Joule heating;
additional heaters embedded in the first and the second electrodes, respectively, the additional heater heating the first and the second electrodes, respectively to heat the catalytic metal to compensate for a temperature difference between both end regions and a central region of the catalytic metal heated using Joule heating induced by the first electrode and the second electrode; and
a current supply unit supplying electric current to the first electrode and the second electrode.
2. The graphene preparation apparatus according to claim 1 , further comprising:
a first support member disposed to face the first electrode, wherein the catalyst metal is disposed between the first support member and the first electrode; and
a second support member disposed to face the second electrode, wherein the catalyst metal is disposed between the second support member and the second electrode,
wherein the additional heaters are disposed in the first support member and the second support member, respectively.
3. The graphene preparation apparatus according to claim 2 , further comprising:
a first connecting member connecting a side surface of the first electrode to a side surface of the first support member to selectively separate the first support member from the first electrode; and
a second connecting member connecting a side surface of the second electrode to a side surface of the second support member to selectively separate the second support member from the second electrode.
4. The graphene preparation apparatus according to claim 2 , wherein each of the first electrode, the second electrode, the first support member, and the second support member is provided in the form of a roller.
5. The graphene preparation apparatus according to claim 4 , further comprising:
a feed unit disposed in the chamber to supply the catalytic metal to a region for preparation of the graphene; and
a reception unit separated a predetermined distance from the feed unit to receive the catalytic metal having the graphene formed thereon.
6. The graphene preparation apparatus according to claim 1 , wherein each of the additional heaters has a built-in battery.
7. The graphene preparation apparatus according to claim 1 , further comprising:
a temperature sensor disposed adjacent to each of the additional heaters to detect the temperature of the additional heaters; and
an additional current supply unit connected to the additional heaters to supply electric current to the additional heaters.
8. The graphene preparation apparatus according to claim 1 , wherein the number of additional heaters disposed at the first electrode side is equal to the number of additional heaters disposed at the second electrode side.
9. A graphene preparation method using Joule heating, the graphene being prepared using the graphene preparation apparatus according to claim 1 , the graphene preparation method comprising:
heating the additional heaters;
maintaining the temperature of the additional heaters for a predetermined period of time; and
forming the graphene on the catalytic metal using both heat generated by the additional heaters and Joule heating induced by the first electrode and the second electrode.