IP Library Granted Patent US 11,804,620
Granted Patent B2
US 11,804,620 · App. 16/967,851 · Granted Oct 31, 2023

Rational design of redox mediator for fast and energy-efficient charging of sulfur cathodes

Inventors: Zhenan Bao (Stanford, CA); Yi Cui (Stanford, CA); Yuchi Tsao (Palo Alto, CA); Min Ah Lee (Seoul, KR)
Assignee: The Board of Trustees of the Leland Stanford Junior University
H01M10/0567H01M4/5815H01M10/052H01M10/0568H01M2004/028H01M2300/0025
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Quick Facts
Patent No.
US 11,804,620
App. No.
16/967,851
Granted
Oct 31, 2023
Kind
B2
Abstract

A battery electrolyte solution is that includes an organic electrolyte solution, a lithium-sulfur (Li 2 S) compound, soluble lithium polysulfide (Li 2 S x ) microparticles, and a redox mediator comprising a soluble quinone derivative.

Claims (31)

1. A battery electrolyte solution comprising:

a) an organic electrolyte solution;

b) a lithium-sulfur (Li 2 S) compound;

c) soluble lithium polysulfide (Li 2 S x ) microparticles; and

d) a redox mediator comprising a soluble quinone derivative.

2. The battery electrolyte solution of claim 1 , wherein said quinone derivative comprises 1,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)anthra-9,10-quinon (AQT).

3. The battery electrolyte solution of claim 1 , wherein said soluble polysulfide Li 2 S x comprises a compound selected from the group is consisting of Li 2 S 2 , Li 2 S 4 , Li 2 S 6 , Li 2 S 8 , and Li 2 S x —S, wherein x={2, 4, 6, 8}.

4. The battery electrolyte solution of claim 1 , wherein a reduction energy level of said redox mediator is higher than an oxidation energy level of said battery electrode active material.

5. The battery electrolyte solution of claim 1 , wherein a reduction potential of said redox mediator is higher than an oxidation potential of said battery electrode active material.

6. The battery electrolyte solution of claim 1 , wherein a reduction energy level of said redox mediator is higher than an oxidation energy level of said redox mediator.

7. The battery electrolyte solution of claim 6 , wherein a reduction energy level of said redox mediator is higher than an oxidation energy level of said Li 2 S compound.

8. The battery electrolyte solution of claim 6 , wherein said is reduction energy level is in a range of 2.15 V to 2.3 V.

9. The battery electrolyte solution of claim 6 , wherein an oxidation energy level of said redox mediator is higher than and proximal to an oxidation energy level of said Li 2 S compound.

10. The battery electrolyte solution of claim 9 , wherein said reduction energy level is in a range of 2.15 V to 2.3 V.

11. The battery electrolyte solution of claim 1 , wherein a redox potential of said quinone derivative ranges from 1.7 V to 3.2 V.

12. A Li—S battery comprising:

a) an anode;

b) a cathode;

c) an organic electrolyte solution;

d) a current collector;

e) a lithium-sulfur (Li 2 S) compound;

f) soluble lithium polysulfide (Li 2 S x ) microparticles; and

g) a redox mediator comprising a soluble quinone derivative.

13. The Li—S battery of claim 12 , wherein said quinone derivative comprises 1,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)anthra-9,10-quinon (AQT).

14. The Li—S battery of claim 12 , wherein said soluble polysulfide Li 2 S x comprises a compound selected from the group consisting of Li 2 S 2 , Li 2 S 4 , Li 2 S 6 , Li 2 S 8 , and Li 2 S x —S, wherein x={2, 4, 6, 8}.

15. The Li—S battery of claim 12 , wherein a reduction energy level of said redox mediator is higher than an oxidation energy level of said redox mediator.

16. The Li—S battery of claim 12 , wherein a reduction energy level of said redox mediator is higher than an oxidation energy level of said Li 2 S compound.

17. The Li—S battery of claim 16 , wherein said reduction energy level is in a range of 2.15 V to 2.3 V.

18. The Li—S battery of claim 16 , wherein an oxidation energy level of said redox mediator is higher than and proximal to an oxidation energy level of said Li 2 S compound.

19. The Li—S battery of claim 18 , wherein said reduction energy level is in a range of 2.15 V to 2.3 V.

20. The Li—S battery of claim 12 , wherein a redox potential of said quinone derivative ranges from 1.7 V to 3.2 V.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 24, 2023
From: STANFORD UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 062478/0945 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 1, 2020
From: BAO, ZHENAN; CUI, YI; TSAO, YUCHI; LEE, MIN AH
To: THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY
Reel/Frame 053657/0850 →
Continuity (3)
Provisional Application 62627458 · Feb 7, 2018
Provisional Application 62626936 · Feb 6, 2018
Related Publication 20210050624A1 · Feb 18, 2021