IP Library Granted Patent US 11,923,527
Granted Patent B2
US 11,923,527 · App. 17/017,081 · Granted Mar 5, 2024

Phosphorus-carbon composites as battery anode materials

Inventors: Guiliang Xu (Downers Grove, IL); Zonghai Chen (Bolingbrook, IL); Khalil Amine (Oak Brook, IL)
Assignee: UCHICAGO ARGONNE, LLC
H01M4/13H01M4/043H01M4/131H01M4/134H01M4/139H01M4/38H01M4/382H01M4/525H01M4/621H01M4/625H01M10/0525H01M10/054H01M10/0568H01M10/0569
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Quick Facts
Patent No.
US 11,923,527
App. No.
17/017,081
Granted
Mar 5, 2024
Kind
B2
Abstract

An electrochemical device includes an anode containing a phosphorus-carbon composite including a conductive carbon matrix and nano-sized phosphorus particles, wherein the nano-sized phosphorus particles are uniformly dispersed on the surface and/or pores of the carbon matrix.

Claims (19)

1. A sodium-ion battery comprising:

a cathode;

a non-aqueous electrolyte;

an anode; and

a separator between the cathode and the anode;

wherein:

the anode comprises a phosphorus-carbon composite comprising:

nano-sized phosphorus particles uniformly dispersed on a surface of a dual-component carbon matrix and/or pores of a dual-component carbon matrix;

the nano-sized phosphorus particles comprising black phosphorus; and

a dual-component conductive carbon matrix comprising:

a first component selected from the group consisting of graphene, reduced graphene oxide, acetylene black, carbon black, a metal-organic framework, porous carbon, carbon spheres, and carbon aerogel; and

a second component selected from the group consisting of single-walled carbon nanotubes, multi-walled carbon nanotubes, carbon nanofibers, carbon nanotube arrays, polypyrrole, and polyaniline;

the first component is present in an amount of about 1% to about 60% by weight of the phosphorus-carbon composite, and the second component is present in an amount of about 0.5% to about 30% by weight of the phosphorus-carbon composite; and

the phosphorus-carbon composite comprises the nano-sized phosphorus particles, the carbon black, and the multi-walled carbon nanotubes, and they are present in the phosphorus-carbon composite at a ratio of 7:2.5:0.5, respectively.

2. The sodium-ion battery of claim 1 , wherein the cathode comprises one or more selected from the group consisting of a cathode active material, a current collector, a conductive carbon material, and a binder.

3. The sodium-ion battery of claim 1 , wherein the nano-sized phosphorus particles further comprise red phosphorus.

4. The sodium-ion battery of claim 1 , wherein the nano-sized phosphorus particles have a particle size of about 1 nm to about 200 nm.

5. The sodium-ion battery of claim 1 , wherein the phosphorus-carbon composite has a dual-component conductive carbon matrix content of about 1% to about 70% by weight of the composite.

6. The sodium-ion battery of claim 1 , wherein the phosphorus-carbon composite comprises the nano-sized phosphorus particles at about 0.1% to about 99.9% by weight.

Assignments (2)
CONFIRMATORY LICENSE Recorded Sep 12, 2024
From: UCHICAGO ARGONNE LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 068949/0421 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 8, 2021
From: AMINE, KHALIL; CHEN, ZONGHAI; XU, GUILIANG
To: UCHICAGO ARGONNE, LLC
Reel/Frame 056797/0353 →
Continuity (2)
Continuation 15006456 · Jan 26, 2016
Related Publication 20210013485A1 · Jan 14, 2021
Cited By (1)
US 12,469,850