IP Library Granted Patent US 11,567,003
Granted Patent B2
US 11,567,003 · App. 17/017,671 · Granted Jan 31, 2023

Measuring dynamic light scattering of a sample

Inventor: Steven P. Trainoff (Santa Barbara, CA)
Assignee: WYATT TECHNOLOGY CORPORATION
G01N21/49G01N21/0332G01N21/39G01N2021/1744G01N2021/396
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,567,003
App. No.
17/017,671
Granted
Jan 31, 2023
Kind
B2
Abstract

The present disclosure describes a method and apparatus of measuring dynamic light scattering of a sample. In an embodiment, the apparatus includes a platen, a light source underneath the platen and configured to emit emitted light through the platen and into the sample, collector optics underneath the platen and configured to capture scattered light, and an optical absorber configured to be in contact with the sample, configured to absorb transmitted light, and configured to redirect reflected light away from the collector optics. In an embodiment, the method includes depositing a sample on a platen, emitting emitted light from a light source underneath the platen through the platen and into the sample, capturing via collector optics underneath the platen scattered light, contacting the sample with an optical absorber, absorbing via the absorber transmitted light, and redirecting via the absorber reflected light away from the collector optics.

Claims (43)

1. An apparatus comprising:

a platen comprising a top surface and a bottom surface,

wherein the top surface of the platen is configured to hold a sample;

a light source underneath the platen and configured to emit emitted light through the platen and into the sample;

collector optics underneath the platen and configured to capture scattered light scattered by the sample; and

an optical absorber above the platen, configured to be in contact with the sample, configured to absorb transmitted light transmitted through the sample, and configured to redirect reflected light reflected from an interface between the sample and a bottom surface of the absorber away from the collector optics.

2. The apparatus of claim 1 wherein the platen comprises a window.

3. The apparatus of claim 1 wherein the top surface of the platen and the bottom surface of the platen comprise polished optical surfaces.

4. The apparatus of claim 3 wherein the top surface of the platen and the bottom surface of the platen comprise flat surfaces.

5. The apparatus of claim 1 wherein the light source is configured to focus the emitted light into the sample.

6. The apparatus of claim 5 wherein the light source comprises a laser.

7. The apparatus of claim 6 wherein the laser is coupled to a single mode, polarization preserving optical fiber.

8. The apparatus of claim 5 wherein the light source is configured to focus the emitted light to have a beam waist of less than 0 . 5 mm within the sample.

9. The apparatus of claim 1 wherein the collector optics comprises:

an optical fiber; and

at least one lens coupled to the fiber,

wherein one of the fiber and the at least one lens is aligned to a focus of the light source within the sample.

10. The apparatus of claim 9 wherein the fiber comprises one of a single mode optical fiber and a multi-mode optical fiber.

11. The apparatus of claim 1

wherein the optical absorber is to absorb energy of the transmitted light within the optical absorber, and

wherein the optical absorber is chosen to be able to conduct the energy away from the sample.

12. The apparatus of claim 11 wherein the optical absorber is to absorb the energy within the optical absorber to an optical depth of less than or equal to 5 mm.

13. The apparatus of claim 11 wherein the optical absorber comprises neutral density glass.

14. The apparatus of claim 1 further comprising an optical absorber carrier,

wherein the carrier contains the optical absorber.

15. The apparatus of claim 14 where in the carrier comprises one of at least one swing arm, a vertical sliding block, and a horizontal sliding block.

16. The apparatus of claim 1 further comprising

a wiper configured to wipe the top surface of the platen.

17. The apparatus of claim 16 further comprising

a cleaning fluid injector configured to release cleaning fluid onto the top surface of the platen.

18. The apparatus of claim 1 further comprising

at least one temperature regulator configured to control a temperature of at least one of the absorber and the platen, thereby regulating a sample temperature of the sample.

19. A method comprising:

depositing a sample on a platen comprising a top surface and a bottom surface,

wherein the top surface of the platen is configured to hold the sample;

emitting emitted light from a light source underneath the platen through the platen and into the sample;

capturing via collector optics underneath the platen scattered light scattered by the sample;

contacting the sample with an optical absorber above the platen;

absorbing via the absorber transmitted light transmitted through the sample; and

redirecting via the absorber reflected light reflected from an interface between the sample and a bottom surface of the absorber away from the collector optics.

20. The method of claim 19 further comprising

controlling a temperature of at least one of the absorber and the platen to a temperature value via a temperature regulator, thereby regulating a sample temperature of the sample,

wherein the temperature value is one of a set value and a varying value that varies over time.

Assignments (2)
ENTITY CONVERSION Recorded Dec 11, 2023
From: WYATT TECHNOLOGY CORPORATION
To: WYATT TECHNOLOGY, LLC
Reel/Frame 066205/0082 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 20, 2023
From: TRAINOFF, STEVEN P.
To: WYATT TECHNOLOGY CORPORATION
Reel/Frame 062444/0167 →
Continuity (2)
Provisional Application 62898532 · Sep 10, 2019
Related Publication 20210072152A1 · Mar 11, 2021