IP Library Granted Patent US 11,499,110
Granted Patent B2
US 11,499,110 · App. 17/018,702 · Granted Nov 15, 2022

Catalytic upcycling of polyolefins into lubricants

Inventors: Gokhan Celik (Clarendon Hills, IL); Kimaya Prakash Vyavhare (Woodridge, IL); Robert M. Kennedy (Evanston, IL); Ryan Hackler (Chicago, IL); Ali Erdemir (Naperville, IL); Massimiliano Delferro (Chicago, IL)
Assignee: UChicago Argonne, LLC
C10M111/04B01J21/04B01J23/002B01J23/02B01J23/42B01J23/755B01J35/0013C10M105/04C10M107/02C10M177/00C10M2203/022C10M2205/0206
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Quick Facts
Patent No.
US 11,499,110
App. No.
17/018,702
Granted
Nov 15, 2022
Kind
B2
Abstract

A method of upcycling polymers to useful hydrocarbon materials. A catalyst with nanoparticles on a substrate selectively docks and cleaves longer hydrocarbon chains over shorter hydrocarbon chains. The nanoparticles exhibit an edge to facet ratio to provide for more interactions with the facets.

Claims (21)

1. A method of producing a lubricant comprising:

exposing, at a temperature of 150-350° C. and a pressure of 100-200 psi for 12— 72 hours, a plurality of polymer molecules to a catalyst comprising a substrate having a plurality of catalytic nanoparticles deposited thereon;

docking a first polymer molecule of the plurality of polymer molecules to the catalyst;

cleaving at least one carbon-carbon bond of the first polymer molecule;

forming a plurality of hydrocarbon fragments from the cleaving;

selectively docking to the catalyst a second polymer molecule of the plurality of polymer molecules, preferentially over the plurality of hydrocarbon fragments;

cleaving at least one carbon-carbon bond of the second polymer molecule; and

forming a second plurality of hydrocarbon fragments.

2. The method of claim 1 , wherein exposing the plurality of polymer molecules is for at least 24 hours.

3. The method of claim 1 , wherein the plurality of catalytic nanoparticles comprise Pt or Ni.

4. The method of claim 1 , wherein the substrate comprises a perovskite.

5. The method of claim 4 , wherein the substrate comprises strontium titanate.

6. The method of claim 3 , wherein the substrate comprises alumina.

7. The method of claim 1 , wherein the plurality of polymer molecules are solvent-free.

8. The method of claim 1 , wherein the plurality of polymer molecules have a molecular weight ranging from 400-1000 Da (number average molecular weight).

9. The method of claim 8 , wherein the plurality of hydrocarbon fragments are C 30 to C 76 alkanes.

10. The method of claim 9 , wherein the plurality of hydrocarbon fragments have 10 branches per 1000 carbon to 400 branches per 1000 carbon.

11. The method of claim 10 , wherein the plurality of hydrocarbon fragments are saturated hydrocarbons.

12. The method of claim 1 , wherein the first polymer molecule is polyethylene.

13. The method of claim 11 , wherein the first polymer is linear low-density polyethylene.

14. The method of claim 11 , wherein the first polymer is linear high-density polyethylene.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 24, 2022
From: VYAVHARE, KIMAYA PRAKASH
To: UCHICAGO ARGONNE, LLC
Reel/Frame 060891/0172 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2022
From: CELIK, GOKHAN; VYAVHARE, KIMAYA; DELFERRO, MASSIMILIANO; ERDEMIR, ALI; HACKLER, RYAN; KENNEDY, ROBERT M.
To: UCHICAGO ARGONNE, LLC
Reel/Frame 060804/0309 →
CONFIRMATORY LICENSE Recorded May 7, 2021
From: UCHICAGO ARGONNE LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 056168/0241 →
Continuity (1)
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