IP Library Granted Patent US 11,081,314
Granted Patent B2
US 11,081,314 · App. 17/035,267 · Granted Aug 3, 2021

Integrated transmission electron microscope

Inventors: Katherine L. Jungjohann (Sandia Park, NM); Khalid M. Hattar (Albuquerque, NM)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
H01J37/28H01J37/12H01J37/1477H01J2237/063H01J2237/2007H01J2237/2802
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Quick Facts
Patent No.
US 11,081,314
App. No.
17/035,267
Granted
Aug 3, 2021
Kind
B2
Abstract

An integrated transmission electron microscope comprising multiple electron sources for tuned beams of ultrafast, scanning probe, and parallel illumination in varied beam energies can be alternated within sub-microseconds onto a sample with dynamic ‘transient state’ processes to acquire atomic-scale structural/chemical data with site specificity. The various electron sources and condenser optics enable high-resolution imaging, high-temporal resolution imaging, and chemical imaging, using fast-switching magnets to direct the different electron beams onto a single maneuverable objective pole piece where the sample resides. Such multimodal in situ characterization tools housed in a single microscope have the potential to revolutionize materials science.

Claims (13)

1. An integrated transmission electron microscope, comprising:

an electron illumination system, comprising

at least two electron sources with associated condenser lenses, each providing a separate electron beam, and

an incident beam electrostatic deflector to direct one of the electron beams to illuminate an electron-transparent sample and deflect the remaining electron beams to one or more beam dumps;

a sample chamber, comprising

a sample holder to hold and manipulate the sample,

an upper objective lens to collimate the illuminating beam on the sample, and

a lower objective lens to image a transmitted beam; and

a detection chamber, comprising at least two detectors, and

a projection system comprising a projection lens and a transmitted beam electrostatic deflector to project and deflect the transmitted beam image onto one of the at least two detectors.

2. The integrated transmission electron microscope of claim 1 , wherein the at least two electron sources and associated condenser lenses comprises at least one of an aberration-corrected transmission electron microscope (TEM), an ultrafast pulsed TEM, and a scanning probe TEM.

3. The integrated transmission electron microscope of claim 1 , wherein the incident beam electrostatic deflector can redirect the at least two electron beams within a time frame of less than one microsecond.

4. The integrated transmission electron microscope of claim 1 , wherein a gap between pole pieces of the upper objective lens and the lower objective lens is adjustable.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2020
From: JUNGJOHANN, KATHERINE L.; HATTAR, KHALID M.
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 054505/0038 →
CONFIRMATORY LICENSE Recorded Nov 24, 2020
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 054452/0904 →
Continuity (2)
Provisional Application 62908730 · Oct 1, 2019
Related Publication 20210098227A1 · Apr 1, 2021