IP Library Granted Patent US 11,519,507
Granted Patent B2
US 11,519,507 · App. 17/036,984 · Granted Dec 6, 2022

Graphene embedded seal

Inventors: Ali Erdemir (Naperville, IL); Vanessa DaSilva (Countryside, IL); Osman Levent Eryilmaz (Plainfield, IL)
Assignee: UChicago Argonne, LLC
F16J15/162B29B7/945F16J15/328F16J15/3284
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Quick Facts
Patent No.
US 11,519,507
App. No.
17/036,984
Granted
Dec 6, 2022
Kind
B2
Abstract

Systems and processes for forming seals. The seals have graphene embedded in the seal. The graphene-embedded seals exhibit improved wear resistance over seals without graphene.

Claims (29)

1. A method of forming a graphene-embedded seal comprising:

mixing graphene and alcohol forming a graphene alcohol solution; and

cold pressing polymer powder to form a pressed seal powder;

exposing the pressed seal powder to the graphene alcohol solution wherein a portion of the graphene alcohol solution infiltrates the pressed seal powder forming an infiltrated pressed seal powder; and

sintering the infiltrated pressed seal powder forming a polymer seal having graphene embedded within the polymer seal.

2. The method of claim 1 , wherein the graphene and alcohol solution comprises 0.1-10 mg/L of graphene.

3. The method of claim 2 , wherein the graphene has an average lateral size of 150-3000 nm.

4. The method of claim 1 , wherein the alcohol is ethanol.

5. The method of claim 1 , wherein the polymer powder is polytetrafluoroethylene.

6. The method of claim 1 , wherein exposing the pressed seal powder comprises soaking the pressed seal powder with the graphene alcohol solution.

7. The method of claim 1 , wherein exposing the pressed seal powder is for 3-5 seconds.

8. The method of claim 1 , wherein, prior to sintering, the alcohol is evaporated.

9. A method of forming a graphene-embedded seal comprising:

mixing graphene and alcohol forming a graphene alcohol solution;

exposing a polymer seal to the graphene alcohol solution wherein a portion of the graphene alcohol solution infiltrates pores of the polymer seal; and

evaporating alcohol from the graphene alcohol solution.

10. The method of claim 9 , wherein the graphene and alcohol solution comprises 0.1-10 mg/L of graphene.

11. The method of claim 10 , wherein the graphene has an average lateral size of 150-3000 nm.

12. The method of claim 9 , wherein the alcohol is ethanol.

13. The method of claim 9 , wherein the polymer seal comprises polytetrafluoroethylene.

14. The method of claim 9 , wherein exposing the polymer seal comprises submerging the polymer seal in the graphene alcohol solution for 5-10 seconds.

15. The method of claim 9 , wherein exposing the polymer seal further comprises applying a vacuum to the polymer seal.

16. The method of claim 9 , wherein exposing the polymer seal further comprises applying a pressure greater than atmospheric to the polymer seal.

17. A method of forming a graphene-embedded seal comprising:

mixing graphene and alcohol forming a graphene alcohol solution;

exposing a polymeric material to the graphene alcohol solution; and

evaporating alcohol from the graphene alcohol solution, depositing graphene within the polymeric material.

18. The method of claim 17 , wherein the polymeric material is a polymer powder.

19. The method of claim 17 , wherein the polymeric material is a polymer seal.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 24, 2021
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 055696/0270 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2020
From: ERYILMAZ, OSMAN LEVENT; ERDIMER, ALI; DASILVA, VANESSA
To: UCHICAGO ARGONNE, LLC
Reel/Frame 054362/0004 →
Continuity (1)
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