IP Library Granted Patent US 11,332,691
Granted Patent B2
US 11,332,691 · App. 17/044,761 · Granted May 17, 2022

Process for producing oils and defatted meal by means of solid/liquid extraction

Inventors: Vincent Rapinel (Montfavet, FR); Norbert Patouillard (Charbonnieres les bains, FR); Farid Chemat (Avignon, FR); Anne-Sylvie Fabiano Tixier (Avignon, FR); Karine Ruiz (Avignon, FR); Laurence Jacques (Dunkirk, FR)
Assignee: PENNAKEM EUROPA
C11B1/10A23D9/007B01D11/0288B01D11/0292C11B3/14
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,332,691
App. No.
17/044,761
Granted
May 17, 2022
Kind
B2
Abstract

The present invention relates to a process for producing an oil and a defatted cake by solid/liquid extraction. The process comprises a step of solid/liquid extraction using a solvent comprising 2-methyloxolane and water.

Claims (26)

1. A process for producing a polyphenol-rich crude oil from a biological substrate comprising a step of:

a) solid/liquid extraction of the biological substrate with a solvent to obtain on the one hand a liquid fraction comprising the crude oil and the solvent and on the other hand a solid residue,

wherein,

the solvent is a mixture of 2-methyloxolane and water, the percentage of 2-methyloxolane by weight in the solvent in the extraction step a) is higher than 80%, and

the percentage of water by weight in the solvent in the extraction step a) is from 0.3% to 20%.

2. The process according to claim 1 , in which the biological substrate is selected from a plant, an alga, a microorganism and mixtures thereof.

3. The process according to claim 2 , in which the biological substrate is a plant selected from almond, amaranth, peanut, argan, sea buckthorn, cashew tree, avocado, oat, borage, safflower, camelina, carrot, cocoa, cashew, hemp, colza, copra, cucurbit, cotton, croton, rosehip, fig, prickly pear, pomegranate, hop, illipé, jojoba, karite, flax, lupine, maize, hazel, walnut, coconut palm, poppy, olive, evening primrose, cabbage palm, paprika, pistachio, pepper, castor-oil plant, rice, musk rose bush, sesame, soybean, marigold, sunflower, Calophyllum inophyllum , madhuca, Queensland walnut, raspberry, blackcurrant, melon, grape, tomato, baobab, babassu, cranberry, chia, pumpkin, mustard, neem, Nigella sativa , niger, poppy, pecan, Perilla, Plukenetia volubilis , pumpkin, annatto, Taramira, apricot, plum, peach, wheat.

4. The process according to claim 1 , in which the extraction step a) is carried out at a temperature of 20° C. to 100° C.

5. The process according to claim 1 , comprising, in addition to the extraction step a), the following steps:

b) recovering the liquid fraction comprising the crude oil and the solvent, and

c) separating the crude oil and the solvent from the liquid fraction to recover on the one hand the crude oil and on the other hand the solvent.

6. A process for producing a refined oil comprising a step of refining the crude oil recovered in step c) of the process for producing a crude oil as defined in claim 5 .

7. A process for producing a solid residue comprising a step e) of recovery of the solid residue obtained in step a) of solid/liquid extraction of the process as defined in claim 1 .

8. A process for producing a desolvated solid residue further comprising a step f) of desolvation of the solid residue recovered in step e) of the process as defined in claim 7 to recover on the one hand the solvent and on the other hand the desolvated solid residue.

9. A process for producing a byproduct comprising a step g) of transforming the desolvated solid residue recovered in step f) of the process as defined in claim 8 to obtain the byproduct.

10. The process according to claim 9 , in which the byproduct is selected from a flour, a protein concentrate, a protein isolate, a textured protein and mixtures thereof.

11. A crude oil derived from a biological substrate, said crude oil comprising a polyphenol and 2-methyloxolane, the concentration of polyphenol by weight being greater than or equal to 320 ppm.

12. The crude oil according to claim 11 , in which the concentration of 2-methyloxolane by weight is from 0.5 ppm to 500 ppm.

13. A refined oil derived from a biological substrate comprising a tocopherol, the concentration of tocopherol by weight being greater than or equal to 1500 ppm.

14. The refined oil according to claim 13 further comprising 2-methyloxolane.

15. A solid residue derived from a biological substrate and comprising a polyphenol and a residual oil, wherein the concentration of polyphenol by weight is less than or equal to 3000 ppm and the concentration of residual oil by weight is less than or equal to 5%.

16. The solid residue according to claim 15 further comprising 2-methyloxolane.

17. A desolvated solid residue derived from a biological substrate comprising 2-methyloxolane, wherein the concentration of 2-methyloxolane by weight is below 1000 ppm.

18. A byproduct derived from a biological substrate comprising 2-methyloxolane, wherein the concentration of 2-methyloxolane by weight is below 1000 ppm.

19. The byproduct according to claim 18 selected from a flour, a protein concentrate, protein isolate, a textured protein, and mixtures thereof.

20. The process according to claim 1 wherein the mixture is a binary mixture.

Assignments (2)
CHANGE OF NAME Recorded Nov 21, 2024
From: PENNAKEM EUROPA
To: ECOXTRACT
Reel/Frame 069429/0919 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2022
From: RAPINEL, VINCENT; PATOUILLARD, NORBERT; CHEMAT, FARID; FABIANO TIXIER, ANNE-SYLVIE; RUIZ, KARINE; JACQUES, LAURENCE
To: PENNAKEM EUROPA
Reel/Frame 059556/0845 →
Priority Claims (1)
FR 18 73103 · Dec 17, 2018 · national
Continuity (1)
Related Publication 20210108150A1 · Apr 15, 2021