IP Library › Granted Patent US 11,945,723
Granted Patent B2
US 11,945,723 · App. 17/049,863 · Granted Apr 2, 2024

Method for producing carbon material complex

Inventors: Syun Gohda (Osaka, JP); Tatsuya Yamaguchi (Hyogo, JP); Hironobu Ono (Osaka, JP); Osamu Konosu (Osaka, JP)
Assignee: Nippon Shokubai Co., Ltd.
C01B32/198C01B32/23C08K3/042C08L33/10C08L63/00
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Quick Facts
Patent No.
US 11,945,723
App. No.
17/049,863
Granted
Apr 2, 2024
Kind
B2
Abstract

Provided is a method of simply producing high-quality graphite oxide. The present invention relates to a method of producing a carbon material composite containing graphite oxide and at least one surfactant selected from the group consisting of a nonionic surfactant, a cationic surfactant, and an amphoteric surfactant, the method including: oxidizing graphite; mixing an aqueous dispersion obtained through the oxidizing, the aqueous dispersion containing graphite oxide dispersed therein, and the at least one surfactant selected from the group consisting of a nonionic surfactant, a cationic surfactant, and an amphoteric surfactant; and purifying the carbon material composite.

Claims (11)

1. A method of producing a carbon material composite containing graphite oxide and at least one surfactant selected from the group consisting of a nonionic surfactant, a cationic surfactant, and an amphoteric surfactant, the method comprising:

oxidizing graphite using sulfuric acid;

mixing an aqueous dispersion obtained through the oxidizing, the aqueous dispersion containing graphite oxide dispersed therein, and the at least one surfactant selected from the group consisting of a nonionic surfactant, a cationic surfactant, and an amphoteric surfactant; and

purifying the carbon material composite.

2. The method of producing a carbon material composite according to claim 1 ,

wherein the purifying includes purifying the carbon material composite by at least one technique selected from the group consisting of filtration, decantation, centrifugation, and solvent extraction.

3. The method of producing a carbon material composite according to claim 1 ,

wherein the mixing includes mixing the aqueous dispersion, the cationic surfactant, and the nonionic surfactant, or mixing the aqueous dispersion, the amphoteric surfactant, and the nonionic surfactant and/or the cationic surfactant.

4. The method of producing a carbon material composite according to claim 1 , further comprising exfoliating into layers the graphite oxide in the carbon material composite purified in the purifying.

5. The method of producing a carbon material composite according to claim 1 ,

wherein the aqueous dispersion contains sulfate ions in an amount of 1% by mass or more relative to 100% by mass of the aqueous dispersion.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 23, 2020
From: GOHDA, SYUN; YAMAGUCHI, TATSUYA; ONO, HIRONOBU; KONOSU, OSAMU
To: NIPPON SHOKUBAI CO., LTD.
Reel/Frame 054147/0013 →
Priority Claims (4)
JP 2018-086822 · Apr 27, 2018 · national
JP 2018-086823 · Apr 27, 2018 · national
JP 2018-123224 · Jun 28, 2018 · national
JP 2018-197835 · Oct 19, 2018 · national
Continuity (1)
Related Publication 20210238041A1 · Aug 5, 2021