IP Library Granted Patent US 11,492,725
Granted Patent B2
US 11,492,725 · App. 17/058,246 · Granted Nov 8, 2022

High-strength single-crystal like nanotwinned nickel coatings and methods of making the same

Inventors: Qiang Li (Ames, IA); Xinghang Zhang (West Lafayette, IN); Haiyan Wang (West Lafayette, IN); Jie Ding (West Lafayette, IN)
Assignee: Purdue Research Foundation
C30B23/02B32B15/01B32B15/20C23C14/165C23C28/023C25D3/18C25D5/18C25D5/605C25D5/617C25D7/00C30B7/12C30B29/02B82Y30/00B82Y40/00Y10T428/12944
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Quick Facts
Patent No.
US 11,492,725
App. No.
17/058,246
Granted
Nov 8, 2022
Kind
B2
Abstract

A high-strength coatings and methods of fabrication to yield single-crystal-like nickel containing nanotwins and stacking faults.

Claims (11)

1. A nickel coating on a substrate, the coating comprising single-crystal nickel containing nanotwins and stacking faults, the single-crystal nickel being grain boundary-free and having stepped twin boundaries.

2. The nickel coating of claim 1 , wherein the spacing of the nanotwins is in the range of about 5 to about 40 nm.

3. The nickel coating of claim 1 , wherein the boundaries between the nanotwins are substantially parallel to the substrate-coating interface.

4. The nickel coating of claim 1 , wherein the boundaries between the nanotwins are at an inclination to the substrate-coating interface.

5. The nickel coating of claim 1 , wherein the substrate is a metallic material.

6. The nickel coating of claim 5 , wherein the metallic material is single-crystal copper.

7. The nickel coating of claim 6 , wherein the single-crystal copper has a (111) orientation.

8. The nickel coating of claim 1 , wherein the yield stress of the coating is in the range of about 1.0 to about 2.0 GPa.

9. The nickel coating of claim 1 , wherein the flow stress of the coating is in the range of about 1.5 to about 2.5 GPa.

10. The nickel coating of claim 1 , wherein the thickness of the coating is in the range of about 100 nm to about 50 micrometers.

11. The nickel coating of claim 1 , wherein the coating is a component of an integrated circuit, a semi-conductive integrated circuit, or a micro/nanoelectromechanical system.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 11, 2022
From: LI, QIANG; ZHANG, XINGHANG; WANG, HAIYAN; DING, JIE
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 058989/0333 →
CONFIRMATORY LICENSE Recorded Apr 26, 2021
From: PURDUE UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 056046/0534 →
Continuity (2)
Provisional Application 62690181 · Jun 26, 2018
Related Publication 20210189581A1 · Jun 24, 2021