IP Library Granted Patent US 11,950,609
Granted Patent B2
US 11,950,609 · App. 17/062,872 · Granted Apr 9, 2024

Low moisture feed block with cold flow resistance

Inventors: Chunjiang Fu (North Mankato, MN); Dan Dhuyvetter (St. Peter, MN)
Assignee: RIDLEY USA INC.
A23K10/40A23K10/33A23K20/163A23K20/20A23K20/24A23K40/20A23K50/10Y02P60/87
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Quick Facts
Patent No.
US 11,950,609
App. No.
17/062,872
Granted
Apr 9, 2024
Kind
B2
Abstract

A method of forming a low moisture block with cold flow resistance proceeds by subjecting a feed mixture containing molasses-like liquids to mixing to form a homogenous mixture; dehydrating the molasses-like mixture to less than about 2.0% moisture using heating; adding to the dehydrated molasses-like liquid mixture one or more feed ingredients in dry ingredient form, comprising 10% to 50% by weight of the resulting mixture; and adding to the dehydrated molasses-like mixture a composition comprising CaO or reactive MgO or combinations thereof, with the composition comprising 0.1% to 10% by weight of the resulting mixture. The composition is mixed in to form a homogenous mixture.

Claims (29)

1. A method of forming a low moisture block with cold flow resistance comprising:

subjecting a feed composition containing liquids comprising one or more of cane molasses, beet molasses, condensed separator by-products (CSB), separator molasses solubles (SMS), soy molasses, molasses, lactose whey, liquid sources of mono-, di- or polysaccharides, and any combination thereof to mixing to form a first mixture;

dehydrating the first mixture to less than about 2.0% moisture to form a second mixture;

adding to the second mixture i) or more feed ingredients in dry ingredient form and ii) a composition comprising at least one of CaO, reactive MgO, ZnO, MnO, FeO, CuO, CuO 2 or combinations thereof to form a third mixture, wherein the third mixture comprises between 10% to 50% by weight of the one or more feed ingredients and between 0.1% to 10% by weight of the composition;

wherein the addition of the composition is performed before sugar crystallization occurs and forms the low moisture block with cold flow resistance.

2. The method of claim 1 , wherein the step of dehydrating comprises heating to between 250° F. and 300° F. and the application of a vacuum.

3. The method of claim 1 , wherein the liquids are condensed separator by-products (CSB), separator molasses solubles (SMS), soy molasses, lactose whey, or mixtures thereof.

4. The method of claim 1 further comprising adding hydrolyzed vegetable oils to the liquids in amount of 0% to 20% by weight of the first mixture.

5. The method of claim 1 , wherein the liquids are cane molasses beet molasses, or mixtures thereof.

6. The method of claim 1 wherein the composition comprises 0.5% to 8.0% by weight of the third mixture.

7. The method of claim 1 wherein the composition comprises 0.5% to 3.0% by weight of the third mixture.

8. The method of claim 1 wherein the composition comprises 1.5% to 3% by weight of the third mixture.

9. The method of claim 1 , wherein the composition comprises reactive MgO, and wherein the composition optionally comprises at least one of CaO, ZnO, MnO, FeO, CuO, CuO 2 or combinations thereof.

10. The method of claim 1 , wherein the composition is added to the second mixture when it is at a temperature in the range of 145° F. to 180° F.

11. A method of forming a low moisture block with cold flow resistance comprising:

preparing a feed composition containing liquids comprising one or more of cane molasses, beet molasses, condensed separator by-products (CSB), separator molasses solubles (SMS), soy molasses, molasses, lactose whey, liquid sources of mono-, di- or polysaccharides, and any combination thereof;

dehydrating the feed composition to less than about 2.0% moisture to form a dehydrated mixture;

adding to the dehydrated mixture i) or more feed ingredients in dry ingredient form and ii) a composition comprising CaO, reactive MgO or combinations thereof to form a resulting mixture, wherein addition of the composition is performed before sugar crystallization,

wherein the one or more feed ingredients in dry ingredient form comprises between 10% to 50% by weight of the resulting mixture; and

wherein the composition comprises between 0.1% to 10% by weight of the resulting mixture.

12. The method of claim 11 wherein the composition comprises an amount within the range 0.5% to 8.0% by weight of the resulting mixture.

13. The method of claim 11 wherein the composition comprises an amount within the range 0.5% to 3.0% by weight of the resulting mixture.

14. The method of claim 11 wherein the composition comprises an amount within the range 1.5% to 3.0% by weight of the resulting mixture.

15. The method of claim 1 , wherein the composition comprises reactive MgO, and wherein the composition optionally comprises at least one of CaO, ZnO, MnO, FeO, CuO, CuO 2 or combinations thereof.

16. The method of claim 1 , wherein the composition is reacted with the dehydrated mixture to form the low moisture block.

17. The method of claim 1 , wherein the feed ingredients in dry ingredient form are selected from the group consisting of protein meal, vitamin, phosphate, urea, limestone, medication, and any combination thereof.

18. The method of claim 15 wherein the composition comprises reactive MgO at 0.5% to 8.0% by weight of the resulting mixture.

19. The method of claim 15 wherein the composition comprises reactive MgO at 0.5% to 3.0% by weight of the resulting mixture.

20. The method of claim 15 wherein the composition comprises reactive MgO at 1.5% to 3% by weight of the resulting mixture.

Assignments (8)
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Nov 14, 2024
From: ALLTECH, INC.; RIDLEY USA INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 069357/0281 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 11, 2022
From: FU, CHUNJIANG; DHUYVETTER, DAN
To: RIDLEY BLOCK OPERATIONS, INC.
Reel/Frame 058617/0870 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 11, 2022
From: RIDLEY BLOCK OPERATIONS, INC.
To: RIDLEY USA INC.
Reel/Frame 058618/0275 →
PATENT SECURITY AGREEMENT Recorded Dec 1, 2021
From: RIDLEY USA INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 058292/0942 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS (8) Recorded Nov 30, 2021
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: RIDLEY USA INC.
Reel/Frame 058291/0987 →
RELEASE OF SECURITY INTEREST Recorded Oct 26, 2021
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: ALLTECH, INC.; RIDLEY USA INC.
Reel/Frame 057919/0761 →
PATENT SECURITY AGREEMENT Recorded Mar 23, 2021
From: RIDLEY USA INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 055693/0555 →
SECURITY INTEREST Recorded Mar 23, 2021
From: RIDLEY USA INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 055692/0607 →
Continuity (2)
Division 13838089 · Mar 15, 2013
Related Publication 20210084937A1 · Mar 25, 2021