IP Library Granted Patent US 11,557,499
Granted Patent B2
US 11,557,499 · App. 17/072,082 · Granted Jan 17, 2023

Methods and apparatus for prevention of component cracking using stress relief layer

Inventors: Yuichi Wada (Chiba, JP); Kok Wei Tan (Singapore, SG); Chul Nyoung Lee (Singapore, SG); Siew Kit Hoi (Singapore, SG); Xinxin Wang (Singapore, SG); Zheng Min Clarence Chong (Singapore, SG); Yaoying Zhong (Singapore, SG); Kok Seong Teo (Singapore, SG)
Assignee: APPLIED MATERIALS, INC.
H01L21/6833C23C4/134C23C14/34H01J37/32477
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Quick Facts
Patent No.
US 11,557,499
App. No.
17/072,082
Granted
Jan 17, 2023
Kind
B2
Abstract

Methods and apparatus for protecting parts of a process chamber from thermal cycling effects of deposited materials. In some embodiments, a method of protecting the part of the process chamber includes wet etching the part with a weak alkali or acid, cleaning the part by bead blasting, coating at least a portion of a surface of the part with a stress relief layer. The stress relief layer forms a continuous layer that is approximately 50 microns to approximately 250 microns thick and is configured to preserve a structural integrity of the part from the thermal cycling of aluminum deposited on the part. The method may also include wet cleaning of the part with a heated deionized water rinse after formation of the stress relief layer.

Claims (28)

1. A method of protecting a part of a process chamber, comprising:

wet etching a deposition ring of an electrostatic chuck with a weak alkali or acid;

bead blasting a first uppermost surface of the deposition ring to increase adhesion of the first uppermost surface to a subsequently applied stress relief layer, wherein the deposition ring is a ceramic material;

coating at least a portion of the first uppermost surface of the deposition ring with the stress relief layer, wherein the stress relief layer forms a continuous layer, wherein the stress relief layer has a first adhesion threshold with the ceramic material of the deposition ring, wherein the stress relief layer has a second adhesion threshold with aluminum on a second uppermost surface of the stress relief layer, and wherein a ratio of the second adhesion threshold to the first adhesion threshold is at least 5 to 1 to preserve a structural integrity of the deposition ring from a thermal cycling of aluminum deposited on the deposition ring; and

wet cleaning the part with a heated deionized water rinse.

2. The method of claim 1 , wherein the first adhesion threshold is approximately 6 MPa and the second adhesion threshold is approximately 30 MPa.

3. The method of claim 1 , wherein a plasma spray process is used to coat the at least a portion of the surface of the part.

4. The method of claim 1 , wherein a per-hydro-poly-silazane (PHPS) process is used to coat the at least a portion of the surface of the part.

5. The method of claim 1 , wherein the deposition ring is configured to surround the electrostatic chuck in a plasma vapor deposition chamber.

6. The method of claim 1 , wherein the stress relief layer forms a continuous layer that is approximately 100 microns to approximately 150 microns thick.

7. The method of claim 1 , wherein the deposition ring has a kit life of approximately 2500 kWh or more.

8. The method of claim 1 , wherein the thermal cycling is between approximately 200 degrees Celsius and approximately 400 degrees Celsius.

9. The method of claim 1 , wherein the second adhesion threshold is an adhesion threshold of aluminum deposited in a vacuum.

10. The method of claim 1 , wherein the stress relief layer maintains structural integrity of the deposition ring for an aluminum deposition thickness having a ratio of greater than 0.8 compared to a deposition ring thickness.

11. A method of protecting a part of a process chamber, comprising:

coating at least a portion of a first uppermost surface of a deposition ring of a ceramic material with a stress relief layer, wherein the stress relief layer forms a continuous layer, wherein the stress relief layer has a first adhesion threshold with the ceramic material of the deposition ring, wherein the stress relief layer has a second adhesion threshold with aluminum on a second uppermost surface of the stress relief layer, and wherein a ratio of the second adhesion threshold to the first adhesion threshold is at least approximately 5 to 1 to preserve a structural integrity of the deposition ring from a thermal cycling below a plastic deformation temperature of aluminum deposited on the part deposition ring in a vacuum.

12. The method of claim 11 , further comprising:

wet etching the part with a weak alkali or acid prior to coating the part; and

bead blasting the first uppermost surface of the deposition ring to increase adhesion of the first uppermost surface to a subsequently applied stress relief layer, wherein the deposition ring.

13. The method of claim 11 , wherein the first adhesion threshold is approximately 6 MPa and the second adhesion threshold is approximately 30 MPa.

14. The method of claim 11 , wherein a plasma spray process using powdered aluminum oxide is used to coat the at least a portion of the surface of the part.

15. The method of claim 11 , wherein the deposition ring is configured to surround the electrostatic chuck in a plasma vapor deposition chamber.

16. The method of claim 11 , wherein the stress relief layer forms a continuous layer that is approximately 100 microns to approximately 150 microns thick.

17. The method of claim 11 , wherein the deposition ring is configured to surround an electrostatic chuck.

18. The method of claim 11 , wherein the stress relief layer maintains structural integrity of the deposition ring for an aluminum deposition thickness having a ratio of greater than 0.8 compared to a deposition ring thickness.

19. An apparatus for installation into a process chamber, comprising:

a deposition ring of a ceramic material with at least a portion of a first uppermost surface having a stress relief layer, wherein the stress relief layer forms a continuous layer, wherein the stress relief layer has a first adhesion threshold with the ceramic material of the deposition ring, wherein the stress relief layer has a second adhesion threshold with aluminum deposited in a vacuum on a second uppermost surface of the stress relief layer, and wherein a ratio of the second adhesion threshold to the first adhesion threshold is at least 5 to 1 to preserve a structural integrity of the deposition ring from a thermal cycling of aluminum deposited on the deposition ring at temperatures of less than a plastic deformation temperature of aluminum.

20. The apparatus of claim 19 , wherein the first adhesion threshold is approximately 6 MPa and the second adhesion threshold is approximately 30 MPa.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2021
From: APPLIED MATERIALS SINGAPORE TECHNOLOGY PTE. LTD.
To: APPLIED MATERIALS, INC.
Reel/Frame 055145/0094 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2020
From: WADA, YUICHI
To: APPLIED MATERIALS, INC.
Reel/Frame 054177/0186 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2020
From: TAN, KOK WEI; LEE, CHUL NYOUNG; HOI, SIEW KIT; WANG, XINXIN; CHONG, ZHENG MIN CLARENCE; ZHONG, YAOYING; TEO, KOK SEONG
To: APPLIED MATERIALS SINGAPORE TECHNOLOGY PTE. LTD.
Reel/Frame 054178/0470 →
Continuity (1)
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