IP Library Granted Patent US 11,715,616
Granted Patent B2
US 11,715,616 · App. 17/082,292 · Granted Aug 1, 2023

Dual low vacuum-ultrahigh vacuum system for large-scale production of micro-channel plate photomultipliers

Inventors: Henry J. Frisch (Chicago, IL); Evan Angelico (San Marcos, CA); Andrey Elagin (Bolingbrook, IL); Eric Spieglan (Lisle, IL); Bernhard W. Adams (Naperville, IL)
Assignee: THE UNIVERSITY OF CHICAGO
H01J9/12B23K1/0008G01T1/202H01J37/244
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Quick Facts
Patent No.
US 11,715,616
App. No.
17/082,292
Granted
Aug 1, 2023
Kind
B2
Abstract

Systems and methods for the batch production of large numbers of highly uniform multichannel-plate photomultiplier tubes (MCP-PMTs) for large-scale applications are provided. The systems and methods employ dual, nested low-vacuum (LV) and UHV processing in a rapid-cycling, small-footprint, scalable, batch-production facility that is capable of fabricating many MCP-PMTs simultaneously.

Claims (39)

1. A system for fabricating a plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors, the system comprising:

a low-vacuum vessel comprising a housing and a seal, wherein the housing and the seal define an interior volume;

a low-vacuum pumping system comprising at least one pump connected to the low-vacuum vessel, the low-vacuum pumping system configured to evacuate the interior volume of the low-vacuum vessel to a pressure in the range from 10 −5 to 10 −8 Torr;

a plurality of detector modules contained within the low-vacuum vessel, each detector module comprising:

a window;

a base, wherein the window and the base define an internal volume of the detector module; and

a microchannel-plate photomultiplier tube detector disposed within the internal volume of the detector module;

one or more heaters in thermal communication with the detector modules;

an ultrahigh-vacuum manifold connected to the internal volumes of the detector modules; and

an ultrahigh-vacuum system comprising at least one pump connected to the ultrahigh-vacuum manifold, the ultrahigh-vacuum system configured to evacuate the ultrahigh-vacuum manifold to a pressure of 10 −9 Torr or lower.

2. The system of claim 1 , wherein the seal is an elastomeric O-ring or an elastomeric gasket.

3. The system of claim 1 , further comprising an alkali metal vapor source connected to the ultrahigh-vacuum manifold and configured to introduce an alkali metal vapor into the internal volumes of the detector modules.

4. The system of claim 1 , further comprising:

an inert gas source connected to the ultrahigh-vacuum manifold and configured to introduce an inert gas into the internal volumes of the detector modules; and

a residual gas analyzer connected to the ultrahigh-vacuum manifold and configured to sample gases present in the internal volumes of the detector modules.

5. The system of claim 1 , wherein the plurality of detector modules comprises at least 100 detector modules.

6. The system of claim 1 , wherein the plurality of detector modules comprises at least 500 detector modules.

7. A method for fabricating a plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors using a system comprising:

a low-vacuum vessel comprising a housing and a seal, wherein the housing and the seal define an interior volume;

a low-vacuum pumping system comprising at least one pump connected to the low-vacuum vessel;

a plurality of detector modules contained within the low-vacuum vessel, each detector module comprising:

a window;

a base, wherein the window and the base define an internal volume of the detector module; and

a microchannel-plate photomultiplier tube detector disposed within the internal volume of the detector module;

one or more heaters in thermal communication with the detector modules;

an ultrahigh-vacuum manifold connected to the internal volumes of the detector modules; and

an ultrahigh-vacuum system comprising at least one pump connected to the ultrahigh-vacuum manifold,

the method comprising:

placing solder into a gap between the window and the base of the detector modules or adjacent to a gap between the window and the base of the detector modules;

evacuating the internal volume of the low-vacuum vessel to a low vacuum pressure in the range from 10 −5 to 10 −8 Torr;

evacuating the ultrahigh-vacuum manifold and the internal volumes of the detector modules to an ultrahigh vacuum pressure of 10 −9 Torr or lower;

heating the detector modules to a temperature at which the solder melts to fill the gaps between the windows and the bases, while the low vacuum pressure is maintained in the internal volume of the low-vacuum vessel and the ultrahigh vacuum pressure is maintained in the internal volumes of the detector modules;

cooling the detector modules to a temperature at which the solder solidifies to form a solder seal between the windows and the bases, while the low vacuum pressure is maintained in the internal volume of the low-vacuum vessel and the ultrahigh vacuum pressure is maintained in the internal volumes of the detector modules; and

releasing the vacuum in the internal volume of the low-vacuum vessel.

8. The method of claim 7 , wherein the low vacuum pressure is in the range from 1×10 −5 to 1×10 −7 Torr.

9. The method of claim 7 , further comprising leak testing all or selected detector modules by introducing a tracer gas into the low-vacuum vessel while maintaining the ultrahigh-vacuum pressure in the ultrahigh vacuum manifold and the internal volumes of the detector modules.

10. The method of claim 7 , further comprising forming a photocathode material on cathode surfaces of the microchannel plate detectors while maintaining the ultrahigh-vacuum pressure in the ultrahigh vacuum manifold and the internal volumes of the detector modules.

11. The method of claim 7 , further comprising testing a performance parameter of one or more of the microchannel plate detectors.

12. The method of claim 7 , wherein fabricating the plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors is conducted without heating the low vacuum vessel.

Assignments (2)
CONFIRMATORY LICENSE Recorded Sep 27, 2024
From: UNIVERSITY OF CHICAGO
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 069087/0057 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 12, 2023
From: FRISCH, HENRY J.; ANGELICO, EVAN; ELAGIN, ANDREY; SPIEGLAN, ERIC; ADAMS, BERNHARD W.
To: THE UNIVERSITY OF CHICAGO
Reel/Frame 063922/0950 →
Continuity (2)
Provisional Application 62928598 · Oct 31, 2019
Related Publication 20210134552A1 · May 6, 2021