IP Library Granted Patent US 11,897,822
Granted Patent B2
US 11,897,822 · App. 17/093,123 · Granted Feb 13, 2024

Reciprocating freeze concentration for urine-based fertilizer production

Inventors: Abraham Noe-Hays (Putney, VT); Nancy G. Love (Ann Arbor, MI)
Assignee: The Regents of the University of Michigan
C05C3/00B01D9/0013C01C1/10
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Quick Facts
Patent No.
US 11,897,822
App. No.
17/093,123
Granted
Feb 13, 2024
Kind
B2
Abstract

A system for generating a concentrated product from a feedstock includes a reciprocating concentration system that includes first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed, and a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber. The system further includes a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system.

Claims (50)

1. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber; and

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system;

wherein the heat dump system comprises a thermoelectric heat pump and a heat sink in thermal communication with the thermoelectric heat pump.

2. The system of claim 1 , wherein the heat dump system is in thermal communication with one of the first and second chambers or in alternating thermal communication with both of the first and second chambers.

3. The system of claim 1 , wherein the heat dump system is in thermal communication with the heat transfer system.

4. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber; and

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system;

wherein the heat transfer system comprises a heat pump.

5. The system of claim 4 , wherein:

the heat pump is disposed between the first and second chambers; and

the heat transfer system further comprises cooling and warming shells adjacent the first and second chambers, each of the cooling and warming shells carrying a respective thermal transfer fluid.

6. The system of claim 5 , wherein:

the cooling shell is disposed along a respective upper portion of the first and second chambers such that the feedstock freezes from the upper portion downward; and

the warming shell is disposed along a respective lower portion of the first and second chambers such that the feedstock melts from the lower portion upward.

7. The system of claim 4 , wherein the heat transfer system further comprises first and second pairs of thermal transfer channels in thermal communication with the first and second chambers, respectively, each thermal transfer channel passing through the heat pump.

8. The system of claim 4 , wherein the heat pump comprises a thermoelectric heat pump.

9. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber;

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system; and

insulation disposed between a heat sink of the heat dump system and the reciprocating concentration system.

10. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber; and

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system;

wherein the heat transfer system comprises:

first and second thermally conductive blocks adjacent to the first and second chambers, respectively; and

a Peltier cell disposed between the first and second thermally conductive blocks.

11. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber; and

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system;

wherein the first and second chambers are disposed in an inclined orientation.

12. A system for generating a concentrated product from a feedstock, the system comprising:

a reciprocating concentration system comprising:

first and second chambers to which the feedstock is alternately provided and from which the concentrated product is alternately removed; and

a heat transfer system in thermal communication with the first and second chambers, the heat transfer system being configured to reversibly transfer heat between the first and second chambers such that the first chamber alternates between melting a frozen portion of the feedstock in the second chamber and having a frozen portion of the feedstock in the first chamber melted by the feedstock in the second chamber; and

a heat dump system in thermal communication with the reciprocating concentration system, the heat dump system being configured to remove heat from the reciprocating concentration system;

wherein:

the reciprocating concentration system further comprises a third chamber to which the feedstock is provided and from which the concentrated product is removed; and

the heat transfer system in thermal communication with the third chamber such that the feedstock in the third chamber melts and freezes out of phase relative to both the first and second chambers.

Assignments (2)
CONFIRMATORY LICENSE Recorded Apr 9, 2025
From: UNIVERSITY OF MICHIGAN
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 070792/0883 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 10, 2020
From: LOVE, NANCY G.
To: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
Reel/Frame 054678/0588 →
Continuity (2)
Provisional Application 62932104 · Nov 7, 2019
Related Publication 20210139385A1 · May 13, 2021