Furnace system and method of use
A sintering furnace can include an outer shell defining an internal volume a reactive agent inlet configured to introduce a reactive agent into the internal volume; an insulation chamber within the outer shell; and a retort configured to retain an object. A method of operating a sintering furnace can include sintering a part precursor within a retort arranged within a chamber, wherein the chamber defines an intermediate volume between the retort and the chamber, wherein a sintering byproduct is oxidized within the intermediate volume.
1. A sintering furnace comprising: an outer shell defining an internal volume, the outer shell comprising: an oxidizing agent inlet configured to introduce an oxidizing agent into the internal volume; andan exhaust mechanism configured to release a reaction byproduct from within the internal volume into an external environment; an insulation chamber arranged within the outer shell, wherein the insulation chamber comprises a heating element configured to raise a temperature inside the insulation chamber to at least a sintering temperature; and a retort, arranged within the insulation chamber, defining a retort volume, the retort comprising: an interfacing wall that separates the retort volume into a working volume and a gas introduction volume, wherein the working volume is configured to receive a material for sintering, wherein the interfacing wall defines a hole configured to allow fluid communication between the working volume and the gas introduction volume; and a gas inlet configured to provide a flow of inert gas into the gas introduction volume, wherein the gas introduction volume defines a tortuous path comprising a boustrophedonic cross-section, wherein the tortuous path is configured to increase a temperature of the inert gas prior to the inert gas entering the working volume wherein the oxidizing agent is introduced into the internal volume when a temperature of the insulation chamber is between 9000 C and 14000 C, wherein the inert gas is introduced in the retort volume contemporaneously with the introduction of the oxidizing agent into the internal volume.
2. The sintering furnace of claim 1 , wherein the exhaust mechanism does not include a catalytic converter, wherein the reaction byproduct comprises at most 10% undegraded sintering byproducts.
3. The sintering furnace of claim 1 , wherein the insulation chamber comprises a ceramic material comprising at least one of fibrous alumina, firebrick, alumina, alumina cement, or bubble alumina.
4. The sintering furnace of claim 3 , wherein the ceramic material releases a low dose of a second oxidizing agent during furnace operation.
5. The sintering furnace of claim 1 , further comprising a sensor configured to detect a quantity of carbon dioxide within or released from the internal volume.
6. The sintering furnace of claim 5 , wherein the oxidizing agent is introduced in response to detection of a threshold quantity of at least one of: carbon dioxide, carbon monoxide, oxygen, or water by the sensor.
7. The sintering furnace of claim 1 , wherein a gas pressure within the retort is greater than a gas pressure within the internal volume.
8. The sintering furnace of claim 1 , wherein a concentration of oxidizing agent in the internal volume does not exceed about 1000 ppm.
9. The sintering furnace of claim 1 , wherein the retort comprises at least one of graphite, silicon carbide, or carbon fiber composite.
10. The sintering furnace of claim 1 , wherein a sintering byproduct produced during object sintering is oxidized by the oxidizing agent in the internal volume.