IP Library › Granted Patent US 11,421,075
Granted Patent B2
US 11,421,075 · App. 17/129,239 · Granted Aug 23, 2022

Curative

Inventors: Aaron Kenneth Amstutz (Peoria, IL); Luke Michael Haverhals (Peoria, IL); Albert C Pierz (Peoria, IL); Ian T Pierz (Peoria, IL)
Assignee: Natural Fiber Welding, Inc.
C08G63/42B32B5/022B32B5/024B32B9/06B32B25/10B32B25/12C08C19/06C08G63/81C08J3/24B32B2305/72B32B2307/50B32B2319/00C08J2315/00
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Quick Facts
Patent No.
US 11,421,075
App. No.
17/129,239
Granted
Aug 23, 2022
Kind
B2
Abstract

A curative for epoxidized plant-based oils and epoxidized natural rubber is created from the reaction between a naturally occurring polyfunctional acid and an epoxidized plant-based oil is disclosed. The curative may be used to produce porosity-free castable resins and vulcanize rubber formulations based on epoxidized natural rubber. Materials made from disclosed materials may be advantageously used as leather substitutes.

Claims (28)

1. An article configured as a sheet, said article comprising:

a. a first layer of an epoxidized natural rubber-based material comprising a mixture of a curative and an epoxidized natural rubber, wherein said curative includes a formed ester linkage between a hydroxyl-containing solvent and a naturally occurring polyfunctional carboxylic acid; and,

b. a backing material positioned adjacent said first layer.

2. The article according to claim 1 wherein an area of said first layer is further defined as being formed with a surface feature thereon.

3. The article according to claim 1 further comprising a second layer of an epoxidized natural rubber-based material comprising a mixture of a curative and an epoxidized natural rubber, wherein said curative includes a formed ester linkage between a hydroxyl-containing solvent and a naturally occurring polyfunctional carboxylic acid, and wherein said second layer is positioned adjacent said backing material.

4. The article according to claim 1 wherein said curative is further defined as comprising a reaction product among said naturally occurring polyfunctional carboxylic acid, said hydroxyl-containing solvent, and an epoxidized triglyceride.

5. An article comprising:

a. a resin comprising a mixture of a pre-polymer and an epoxidized triglyceride, wherein said prepolymer includes a formed ester linkage between a hydroxyl-containing solvent and a naturally occurring polyfunctional carboxylic acid; and,

b. a backing layer, wherein said resin impregnates a portion of said backing layer.

6. The article according to claim 5 wherein said backing layer is further defined as a textile.

7. The article according to claim 6 wherein said textile backing layer is further defined as a non-woven mat comprised of a fibrous content that is substantially all non-petrochemical.

8. The article according to claim 7 wherein said fibrous content is substantially all cellulosic.

9. The article according to claim 7 wherein said textile backing layer is further defined as fibrous recycled cotton fiber.

10. The article according to claim 5 wherein the resin is selected and said backing layer is configured such that said backing layer is visible through said resin.

11. The article according to claim 5 wherein said article further comprises an embossed portion formed in said resin.

12. The article according to claim 6 wherein said textile backing layer is further defined as being comprised of a protein-based fiber.

13. The article according to claim 6 wherein said textile backing layer is further defined as being selected from a group consisting of wool, silk, alpaca fiber, qiviut, vicuna fiber, llama wool, cashmere, and angora.

14. The article according to claim 5 wherein said pre-polymer is further defined as comprising a reaction product among said naturally occurring polyfunctional carboxylic acid, said hydroxyl-containing solvent, and an epoxidized triglyceride.

15. A method of making an article, said method comprising the steps of:

a. selecting a backing material;

b. applying a resin to said backing material to create a first layer, wherein said resin comprises a mixture of a pre-polymer and an epoxidized triglyceride, wherein said prepolymer includes a formed ester linkage between a hydroxyl-containing solvent and a naturally occurring polyfunctional carboxylic acid; and,

c. controlling a temperature of said article; and,

d. allowing said resin to cure.

16. The method according to claim 15 further comprising the step of embossing a portion of said resin during said step of controlling said temperature of said article.

17. The method according to claim 15 wherein said backing material is further defined as a woven fabric.

18. The method according to claim 16 wherein said backing material is further defined as a nonwoven fabric.

19. The method according to claim 15 further comprising the step of positioning a texture paper adjacent said first layer prior to said step of allowing said resin to cure.

20. The method according to claim 19 further comprising the step of positioning a silicone release sheet adjacent said texture paper.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2021
From: AMSTUTZ, AARON KENNETH; HAVERHALS, LUKE; PIERZ, ALBERT C; PIERZ, IAN T
To: NATURAL FIBER WELDING, INC.
Reel/Frame 056333/0524 →
Continuity (10)
Continuation 16457352 · Jun 28, 2019
Continuation 16388693 · Apr 18, 2019
Provisional Application 62806480 · Feb 15, 2019
Provisional Application 62772715 · Nov 29, 2018
Provisional Application 62772744 · Nov 29, 2018
Provisional Application 62756062 · Nov 5, 2018
Provisional Application 62669483 · May 10, 2018
Provisional Application 62669502 · May 10, 2018
Provisional Application 62660943 · Apr 21, 2018
Related Publication 20210108030A1 · Apr 15, 2021
Cited By (1)
US 12,344,706