Thermal analyzer
Provided is a thermal analyzer, with which a sample can be observed even under a state in which a heat sink is cooled to a room temperature or lower. The thermal analyzer includes: the heat sink, in which a measurement sample container and a reference sample container are placed; a heat sink cover configured to cover the heat sink; a heat sink window provided in the heat sink; a heat sink cover window provided in the heat sink cover; an imaging device configured to image the sample in the heat sink through the heat sink window and the heat sink cover window; a purge gas introduction portion, through which a purge gas is introduced into the heat sink; and a discharge port, through which the purge gas is allowed to flow from one of the heat sink window and the heat sink to a space inside the heat sink cover.
1. A thermal analyzer, comprising:
a heat sink, in which a measurement sample container and a reference sample container are to be placed, the measurement sample container being configured to contain a measurement sample, the reference sample container being configured to contain a reference sample;
a differential heat flow detector configured to detect, under a state in which the measurement sample and the reference sample are placed in the heat sink, a temperature difference between the measurement sample and the reference sample caused by heat absorbed or released by the measurement sample;
a measurement circuit configured to convert the temperature difference detected and input thereto by the differential heat flow detector into a DSC signal;
a heat sink cover configured to cover the heat sink;
a heat sink window provided in a part of the heat sink;
a heat sink cover window provided in a part of the heat sink cover;
an imaging device configured to image at least the measurement sample placed in the heat sink through the heat sink window and the heat sink cover window;
a purge gas introduction portion, through which a purge gas is introduced into an internal space of the heat sink; and
a discharge port, through which the purge gas is allowed to flow from the internal space of the heat sink through one of the heat sink window and the heat sink to a space inside the heat sink cover.
2. The thermal analyzer according to claim 1 , further comprising a heat sink cover heater configured to heat the heat sink cover window.
3. The thermal analyzer according to claim 1 , further comprising an outlet port configured to blow the purge gas inside the heat sink cover at an outdoor air side of the heat sink cover window.
4. The thermal analyzer according to any one of claims 1 to 3 , wherein the heat sink window is formed of a transparent material and a material having a high heat conductivity.
5. The thermal analyzer according to any one of claims 1 to 3 , wherein the heat sink cover window is formed of a transparent material and a material having a high heat conductivity.