IP Library › Granted Patent US 11,718,698
Granted Patent B2
US 11,718,698 · App. 17/138,015 · Granted Aug 8, 2023

Polyolefin grafted polydiene polymers, and methods of making and using same

Inventors: Terrence E. Hogan (Uniontown, OH); Arif O. Gozen (Dundee, MI); James D. Ulmer (Akron, OH)
Assignee: Bridgestone Corporation
C08F279/02B60C1/00B60C1/0025C08F8/32C08F8/34C08F8/46C08F22/06C08F136/06C08F299/00C08G81/00C08K5/3725C08L7/00C08L9/00C08L21/00C08L23/02C08L23/0815C08L23/14C08L23/32C08L51/04C08K3/013
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Quick Facts
Patent No.
US 11,718,698
App. No.
17/138,015
Granted
Aug 8, 2023
Kind
B2
Abstract

Embodiments of the present disclosure are directed to polyolefin grafted polydiene polymers, wherein the polyolefin grafted polydiene polymers comprises a polydiene having a polydiene polymer backbone, a polyolefin, and at least one sulfur containing functionalizing agent which grafts the polyolefin onto at least one non-terminal position on the polydiene polymer backbone.

Claims (21)

1. A polyolefin grafted polydiene polymer comprising:

a polydiene having a polydiene polymer backbone;

a polyolefin having an anhydride polymeric modifier; and

at least one sulfur containing functionalizing agent which grafts the polyolefin onto at least one non-terminal position on the polydiene polymer backbone.

2. The polyolefin grafted polydiene polymer of claim 1 , wherein the anhydride polymeric modifier comprises maleic anhydride.

3. The polyolefin grafted polydiene polymer of claim 1 , wherein the sulfur containing functionalizing agent comprises an aminothiol, the aminothiol having an amine moiety which reacts with the anhydride polymeric modifier.

4. The polyolefin grafted polydiene polymer of claim 1 , wherein the polyolefin comprises one or more C 2 -C 12 olefins.

5. The polyolefin grafted polydiene polymer of claim 1 , wherein the polydiene comprises 1,4-polybutadiene having a cis % of at least 85%.

6. A rubber composition comprising:

one or more rubbers selected from natural rubber and polydiene rubber;

reinforcing filler; and

the polyolefin grafted polydiene polymer of claim 1 .

7. The rubber composition of claim 6 , wherein a volume fraction of reinforcing filler plus polyolefin in the rubber composition is about 0.200 to about 0.350.

8. A method of producing a polyolefin grafted polydiene polymer comprising:

reacting a polyolefin having an anhydride polymeric modifier with at least one sulfur containing functionalizing agent to produce a functionalized polyolefin; and

producing the polyolefin grafted polydiene polymer by reacting the functionalized polyolefin with an unsaturated polydiene polymer.

9. The method of claim 8 , wherein the unsaturated polydiene polymer comprises 1,4-polybutadiene having a cis % of at least 85%.

10. The method of claim 8 , wherein the polymeric modifier reacts with the sulfur containing functionalizing agent.

11. The method of claim 8 , wherein the polymeric modifier is maleic anhydride, and the sulfur containing functionalizing agent includes thiols, polysulfides, or combinations thereof.

12. The method of claim 8 , wherein the functionalized polyolefin is grafted onto at least one non-terminal position on the unsaturated polydiene polymer.

13. The method of claim 8 , wherein the polyolefin is a copolymer, wherein the copolymer includes an ethylene monomer and at least one C 3 -C 12 olefin comonomer.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 4, 2021
From: HOGAN, TERRENCE E.; GOZEN, ARIF O.; ULMER, JAMES D.
To: BRIDGESTONE CORPORATION
Reel/Frame 054802/0053 →
Continuity (3)
Continuation 16066945
Provisional Application 62272121 · Dec 29, 2015
Related Publication 20210230420A1 · Jul 29, 2021