IP Library Granted Patent US 11,697,691
Granted Patent B2
US 11,697,691 · App. 17/153,479 · Granted Jul 11, 2023

Assessing and improving wheat gluten quality with rheometric analysis

Inventor: Scott R. Frazer (Maple Grove, MN)
Assignee: Ardent Mills, LLC
C08B30/046G01N33/10
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Quick Facts
Patent No.
US 11,697,691
App. No.
17/153,479
Granted
Jul 11, 2023
Kind
B2
Abstract

Disclosed herein is a method of assessing rheology characteristics of vital wheat gluten to determine how to improve the quality of VWG product and the choice of VWG for a particular product.

Claims (31)

1. A method of making vital wheat gluten (VWG), comprising:

determining a quality feature of VWG obtained from a sample VWG-starch mixture by:

determining, from a rheometric analysis of the VWG, a sample viscosity plateau, a sample starch gelatinization portion, and a sample glutenin viscosity peak that is between the sample viscosity plateau and the sample starch gelatinization portion; and

comparing a standard viscosity plateau to the sample viscosity plateau;

adjusting a drying temperature until a difference between the standard viscosity plateau and the sample viscosity plateau is less than or equal to 1.2 newton meters (Nm).

2. The method of claim 1 , further comprising subjecting a standard VWG-starch mixture containing a predetermined ratio of VWG:starch to rheometric analysis to determine the standard viscosity plateau and the standard glutenin viscosity peak.

3. The method of claim 2 , wherein the predetermined ratio is from about 10:90 to about 80:20 by weight.

4. The method of claim 2 , wherein the predetermined ratio is about 10:90 by weight.

5. The method of claim 2 , wherein the predetermined ratio is about 40:60 by weight.

6. The method of claim 1 , further comprising comparing a standard starch gelatinization portion to the sample starch gelatinization portion.

7. The method of claim 6 , wherein a difference between the standard starch gelatinization portion and the sample starch gelatinization portion indicates a different concentration of amylase.

8. The method of claim 6 , wherein a difference between the standard starch gelatinization portion and the sample starch gelatinization is a decrease in the starch gelatinization portion of the sample rheometric profile.

9. The method of claim 1 , further comprising contacting the sample VWG-starch mixture with an aqueous solution having a pH to separate starch of the sample VWG-starch mixture from the VWG of the sample VWG-starch mixture.

10. The method of claim 1 , further comprising extracting the sample VWG-starch mixture from a production supply of flour.

11. The method of claim 1 , further comprising drying the VWG at the drying temperature, wherein the VWG is obtained from a sample VWG-starch mixture.

12. The method of claim 1 , wherein adjusting the drying temperature until the difference between the standard viscosity plateau and the sample viscosity plateau is less than or equal to 1.2 newton meters (Nm) comprises both adjusting the drying temperature and adjusting a pH until the difference between the standard viscosity plateau and the sample viscosity plateau is less than or equal to 1.2 newton meters (Nm).

13. A method of making vital wheat gluten (VWG), comprising:

determining a quality feature of VWG obtained from a sample VWG-starch mixture by:

determining, from a rheometric analysis of the VWG, a sample viscosity plateau, a sample starch gelatinization portion, and a sample glutenin viscosity peak that is between the sample viscosity plateau and the sample starch gelatinization portion; and

comparing a standard viscosity plateau to the sample viscosity plateau;

adjusting a pH until a difference between the standard viscosity plateau and the sample viscosity plateau is less than or equal to 1.2 newton meters (Nm).

14. The method of claim 13 , further comprising subjecting a standard VWG-starch mixture containing a predetermined ratio of VWG:starch to rheometric analysis to determine the standard viscosity plateau and the standard glutenin viscosity peak.

15. The method of claim 13 , further comprising drying the VWG at a drying temperature, wherein the VWG is obtained from a sample VWG-starch mixture.

16. A method of making vital wheat gluten (VWG), comprising:

determining a quality feature of VWG obtained from a sample VWG-starch mixture by:

determining, from a rheometric analysis of the VWG, a sample viscosity plateau, a sample starch gelatinization portion, and a sample glutenin viscosity peak that is between the sample viscosity plateau and the sample starch gelatinization portion; and

comparing a standard glutenin viscosity peak to the sample glutenin viscosity peak;

adjusting a pH until a difference between the standard glutenin viscosity peak and the sample glutenin viscosity peak is less than or equal to 1.2 newton meters (Nm).

17. The method of claim 16 , further comprising contacting the sample VWG-starch mixture with an aqueous solution having a pH to separate starch of the sample VWG-starch mixture from the VWG of the sample VWG-starch mixture.

18. The method of claim 16 , further comprising drying the VWG at a drying temperature, wherein the VWG is obtained from a sample VWG-starch mixture.

19. The method of claim 16 , further comprising adjusting a drying temperature until a difference between the standard glutenin viscosity peak and the sample glutenin viscosity peak is less than or equal to 1.2 newton meters (Nm).

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2023
From: FRAZER, SCOTT R.
To: CARGILL, INCORPORATED
Reel/Frame 062603/0418 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2023
From: CARGILL, INCORPORATED
To: CARGILL A.M. HOLDCO LLC
Reel/Frame 062603/0685 →
MERGER Recorded Feb 6, 2023
From: CARGILL A.M. HOLDCO LLC
To: HORIZON MILLING, LLC
Reel/Frame 062603/0785 →
CHANGE OF NAME Recorded Feb 6, 2023
From: HORIZON MILLING, LLC
To: ARDENT MILLS, LLC
Reel/Frame 062603/0862 →
Continuity (4)
Continuation 16830822 · Mar 26, 2020
Division 12415277 · Mar 31, 2009
Provisional Application 61041571 · Apr 1, 2008
Related Publication 20210139614A1 · May 13, 2021