IP Library Granted Patent US 11,592,338
Granted Patent B2
US 11,592,338 · App. 17/183,122 · Granted Feb 28, 2023

Non-destructive, in-situ evaluation of water presence using thermal contrast and cooled detector

Inventor: Mihail Bora (Livermore, CA)
Assignee: Lawrence Livermore National Security, LLC
G01J5/0896G01J5/0037G01J5/0806
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,592,338
App. No.
17/183,122
Granted
Feb 28, 2023
Kind
B2
Abstract

Exemplary methods for detecting presence of water in a sample include: heating a light source to a predetermined temperature at which the light source emits thermal radiation; placing a sample between the light source and a detector; transmitting the thermal radiation from the light source through the sample and onto the detector; and determining a presence or an absence of water within the sample based on the thermal radiation transmitted onto the detector. Exemplary systems for detecting presence of water in a sample are also disclosed.

Claims (21)

1. A method, comprising:

heating a light source to a predetermined temperature at which the light source emits thermal radiation;

placing a sample between the light source and a detector;

transmitting the thermal radiation from the light source through the sample and onto the detector; and

determining a presence or an absence of water within the sample based on the thermal radiation transmitted onto the detector.

2. The method as recited in claim 1 , wherein the thermal radiation is substantially uniform thermal radiation.

3. The method as recited in claim 1 , further comprising cooling the detector and a filter optically coupled to the detector and the sample, wherein the cooling comprises reducing a temperature of each of the detector and the filter to a temperature less than a temperature of the sample.

4. The method as recited in claim 3 , wherein the cooling uses liquid nitrogen.

5. The method as recited in claim 1 , further comprising filtering the thermal radiation transmitted through the sample prior to arrival of the thermal radiation at the detector.

6. The method as recited in claim 5 , wherein the filtering:

selectively transmits, to the detector, first portions of the thermal radiation, the first portions being characterized by a wavelength at least partially overlapping a predefined water absorption band and/or a predefined water absorption line; and

selectively blocks second portions of the thermal radiation, the second portions being characterized by a wavelength outside the predefined water absorption band and/or the predefined water absorption line.

7. The method as recited in claim 6 , wherein each of the predefined water absorption band and the predefined water absorption line include wavelengths ranging from about 2.5 μm to about 3.3 μm.

8. The method as recited in claim 1 , further comprising calibrating the detector to exhibit a flat response to thermal radiation having a temperature between a first calibration temperature and a second calibration temperature.

9. The method as recited in claim 8 , wherein the calibrating comprises:

heating the light source to the first calibration temperature;

acquiring a first image of the light source using the detector, wherein the detector comprises an infrared camera having a focal plane array;

heating the light source to the second calibration temperature;

acquiring a second image of the light source using the detector; and

adjusting, based on the first and second images, at least a gain and an offset of pixels in the focal plane array such that any sample exhibiting a temperature in a range from the first calibration temperature to the second calibration temperature yields the flat response by the detector.

10. The method as recited in claim 9 , wherein the first calibration temperature is about 25° C. and the second calibration temperature is about 35 C.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 10, 2021
From: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC.
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 056193/0512 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2021
From: BORA, MIHAIL
To: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
Reel/Frame 055593/0880 →
Continuity (2)
Division 16004196 · Jun 8, 2018
Related Publication 20210181027A1 · Jun 17, 2021