IP Library Granted Patent US 12,191,543
Granted Patent B2
US 12,191,543 · App. 17/191,992 · Granted Jan 7, 2025

Integrated production of hydrogen, electricity, and heat

Inventors: Kunho Lee (Dhahran, SA); Aadesh Harale (Dhahran, SA); Thang Pham (Dhahran, SA); Aqil Jamal (Dhahran, SA); Ahmad O. Khowaiter (Dhahran, SA)
Assignee: Saudi Arabian Oil Company
H01M8/0618B01D53/04B01D53/229B01D71/021B01D71/022B01D71/028B01J23/745B01J23/755C01B3/48C01B3/501C01B3/56H01M8/04014H01M8/0675H01M8/0687H01M8/1231B01D2256/16B01D2257/302C01B2203/0233C01B2203/0283C01B2203/066C01B2203/0894C01B2203/1058C01B2203/1241C01B2203/127C01B2203/84H01M2008/1293
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Quick Facts
Patent No.
US 12,191,543
App. No.
17/191,992
Granted
Jan 7, 2025
Kind
B2
Abstract

A method and a system for the coproduction of hydrogen, electrical power, and heat energy. An exemplary method includes desulfurizing a feed stream to form a desulfurized feed stream, reforming the desulfurized feed stream to form a methane rich gas, and providing the methane rich gas to a membrane separator. A hydrogen stream is produced in a permeate from the membrane separator. A retentate stream from the membrane separator is provided to a solid oxide fuel cell (SOFC). Electrical power is produced in the SOFC from the retentate stream.

Claims (32)

1. A trigeneration facility, comprising:

a desulfurization unit to remove sulfur from a hydrocarbon feed stream forming a desulfurized feed stream, the desulfurization unit comprising a desulfurization catalyst, the desulfurization catalyst comprising a gamma alumina based support, at least one catalytic metal from group VI, at least one catalytic metal from group VIII, and at least one dopant selected from a group consisting of boron, phosphorous, halogen, and silicon;

a pre-reformer to convert the desulfurized feed stream to a methane rich gas, the pre-reformer comprising a steam reformer comprising a nickel catalyst;

a membrane separator to remove at least a portion of hydrogen from the methane rich gas in a permeate, the membrane separator comprising a water-gas shift catalyst to increase an amount of hydrogen in the methane rich gas;

a pressure swing adsorption unit to purify hydrogen in the permeate, providing a purified stream;

a compressed hydrogen stream of about 400 bar to about 900 bar, wherein the compressed hydrogen stream is a fuel stream to a fuel cell vehicle from the purified stream; and

a solid oxide fuel cell (SOFC) to generate electrical power and heat from a retentate from the membrane separator, wherein the retentate comprises methane.

2. The trigeneration facility of claim 1 , comprising a heat exchanger to utilize the generated heat.

3. The trigeneration facility of claim 1 , comprising a heat exchanger to heat the retentate, using the generated heat, to an operating temperature of the SOFC.

4. The trigeneration facility of claim 1 , wherein the pre-reformer operates at a temperature between about 300° C. and about 550° C.

5. The trigeneration facility of claim 1 , wherein the steam reformer operates at a pressure of between about 2 bar and about 30 bar.

6. The trigeneration facility of claim 1 , wherein the water-gas shift catalyst comprises iron oxides or copper oxides.

7. The trigeneration facility of claim 1 , wherein the membrane separator is a high-temperature hydrogen selective membrane.

8. The trigeneration facility of claim 7 , wherein the membrane separator comprises palladium, or a palladium alloy, or both.

9. The trigeneration facility of claim 7 , wherein the membrane separator comprises a carbon-based membrane, or a zeolite based membrane, or both.

10. The trigeneration facility of claim 1 , wherein the membrane separator comprises an integrated water-gas shift catalyst.

11. The trigeneration facility of claim 1 , wherein the membrane separator comprises a proton conducting material, which is electrically driven to transport the hydrogen to the permeation side.

12. The trigeneration facility of claim 1 , wherein the feed stream comprises propane, or butane, or both.

13. The trigeneration facility of claim 1 , wherein the feed stream comprises liquefied natural gas.

14. The trigeneration facility of claim 1 , wherein the feed stream comprises a raw natural gas.

15. A trigeneration facility, comprising:

a desulfurization unit to remove sulfur from a hydrocarbon feed stream forming a desulfurized feed stream;

a pre-reformer to convert the desulfurized feed stream to a methane rich gas;

a membrane separator to remove at least a portion of hydrogen from the methane rich gas in a permeate, the membrane separator comprising a water-gas shift catalyst to increase an amount of hydrogen in the methane rich gas;

a compressed hydrogen stream of about 400 bar to about 900 bar, wherein the compressed hydrogen stream is a fuel stream to a fuel cell vehicle from the trigeneration facility; and

a solid oxide fuel cell (SOFC) to generate electrical power and heat from a retentate from the membrane separator, wherein the retentate comprises methane.

16. A trigeneration facility, comprising:

a desulfurization unit operating at a temperature between about 300° C. and about 550° C. to remove sulfur from a hydrocarbon feed stream forming a desulfurized feed stream;

a pre-reformer operating at a temperature between about 300° C. and about 550° C. to convert the desulfurized feed stream to a methane rich gas;

a membrane separator operating at a temperature between about 300° C. and about 550° C. to remove at least a portion of hydrogen from the methane rich gas in a permeate, the membrane separator comprising a water-gas shift catalyst to increase an amount of hydrogen in the methane rich gas;

a compressed hydrogen stream of about 400 bar to about 900 bar, wherein the compressed hydrogen stream is a fuel stream to a fuel cell vehicle from the trigeneration facility; and

a solid oxide fuel cell (SOFC) to generate electrical power and heat from a retentate from the membrane separator, wherein the retentate comprises methane.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2021
From: LEE, KUNHO; HARALE, AADESH; PHAM, THANG; JAMAL, AQIL; KHOWAITER, AHMAD O.
To: SAUDI ARABIAN OIL COMPANY
Reel/Frame 055520/0400 →
Continuity (1)
Related Publication 20220285712A1 · Sep 8, 2022
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