IP Library Granted Patent US 11,658,213
Granted Patent B2
US 11,658,213 · App. 17/254,499 · Granted May 23, 2023

Superlattice films for photonic and electronic devices

Inventors: Robert P. H. Chang (Glenview, IL); Woongkyu Lee (Evanston, IL)
Assignee: Northwestern University
H01L29/152H01L21/02175H01L21/02565H01L29/24
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Quick Facts
Patent No.
US 11,658,213
App. No.
17/254,499
Granted
May 23, 2023
Kind
B2
Abstract

Superlattices and methods of making them are disclosed herein. The superlattices are prepared by irradiating a sample to prepare an alternating superlattice of layers of a first material and a second material, wherein the ratio of the first deposition rate to the second deposition rate is between 1.0:2.0 and 2.0:1.0. The superlattice comprises a multiplicity of alternating layers, wherein the multiplicity of layers of the first material have a thickness between 0.1 nm and 50.0 nm or the multiplicity of layers of the second material have a thickness between 0.1 nm and 50.0.

Claims (18)

1. A method for preparing a superlattice, the method comprising:

(a) providing a chamber having a first material and a second material therein;

(b) positioning the first material in an irradiation zone within the chamber;

(c) irradiating the first material in the irradiation zone for an effective time to deposit a layer of the first material at a first deposition rate;

(d) positioning the second material in the irradiation zone;

(e) irradiating the second material in the irradiation zone for an effective time to deposit a layer of the second material at a second deposition rate; and

(f) repeating steps (b)-(e) a multiplicity of times, thereby forming an alternating superlattice of layers of the first material and the second material,

wherein the ratio of the first deposition rate to the second deposition rate is between 1.0:2.0 and 2.0:1.0 and

wherein the first material is selected from a crystalline semiconductive material and the second material is selected from an amorphous insulating material.

2. The method of claim 1 , wherein the effective time to deposit the layer of the first material results in a layer of the first material between 0.1 nm and 50.0 nm thick or the effective time to deposit the layer of the second material results in a layer of the second material between 0.1 nm and 50.0 nm thick.

3. The method of claim 2 , wherein the effective time to deposit the layer of the first material results in a layer of the first material between 0.1 nm and 10.0 nm thick and the effective time to deposit the layer of the second material results in a layer of the second material between 0.1 nm and 10.0 nm thick.

4. The method of claim 1 , wherein the first material and the second material are transparent materials.

5. The method of claim 1 , wherein the first material is a crystalline transparent semiconducting material and the second material is an amorphous transparent insulating material.

6. The method of claim 5 , wherein the crystalline transparent semiconducting material comprises a transparent conducting oxide, a transparent conducting nitride, a transparent conducting carbide, or a transparent conducting chalcogenite.

7. The method of claim 6 , wherein the crystalline transparent semiconducting material comprises In 2 O 3 .

8. The method of claim 5 , wherein the amorphous transparent insulating material comprises an insulating oxide.

9. The method of claim 8 , wherein the amorphous transparent insulating material comprises MoO 3 .

10. The method of claim 1 , wherein the first material is In 2 O 3 and the second material is MoO 3 .

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 3, 2025
From: NORTHWESTERN UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 070095/0923 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2020
From: CHANG, ROBERT P.H.; LEE, WOONGKYU
To: NORTHWESTERN UNIVERSITY
Reel/Frame 054712/0209 →
Continuity (2)
Provisional Application 62688812 · Jun 22, 2018
Related Publication 20210126091A1 · Apr 29, 2021