IP Library Granted Patent US 11,752,484
Granted Patent B2
US 11,752,484 · App. 17/278,741 · Granted Sep 12, 2023

Apparatus and method for analyzing reactions

Inventor: Armin Lange de Oliveira (Heidelberg, DE)
Assignee: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION
B01J19/0046B01J2219/00286B01J2219/00306B01J2219/00389B01J2219/00477B01J2219/00587B01J2219/00594B01J2219/00702B01J2219/00747
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Quick Facts
Patent No.
US 11,752,484
App. No.
17/278,741
Granted
Sep 12, 2023
Kind
B2
Abstract

The invention proceeds from an apparatus for analyzing reactions, comprising a starting material distributor and at least two reactors which are connected in parallel and are each connected via a connecting conduit to an outlet of the starting material distributor. To set the inflow, a pressure regulator and a restrictor are installed in each connecting conduit between the starting material distributor and the reactors or an outlet conduit in which a restrictor and a pressure regulator are installed branches off from each connecting conduit. The invention further relates to a method for analyzing reactions in such an apparatus.

Claims (16)

1. An apparatus for analyzing reactions, comprising a starting material distributor and at least two reactors which are connected in parallel and are each connected via a connecting conduit to an outlet of the starting material distributor, wherein a pressure regulator and a restrictor are installed in each connecting conduit between the starting material distributor and the reactors in order to set the inflow or wherein a restrictor and a pressure regulator are installed in an outlet conduit which branches off from each connecting conduit.

2. The apparatus according to claim 1 , wherein the pressure regulator is an exit pressure regulator and is installed between the starting material distributor and the restrictor.

3. The apparatus according to claim 1 , wherein the pressure regulator is an admission pressure regulator and is installed between the restrictor and the reactor.

4. The apparatus according to claim 1 , wherein the restrictor is a capillary, a microstructured component, an orifice plate or a nozzle.

5. The apparatus according to claim 1 , wherein the reactors are connected to a further distributor.

6. The apparatus according to claim 5 , wherein a restrictor is positioned between the further distributor and each reactor.

7. The apparatus according to claim 5 , wherein a pressure regulator is installed between the further distributor and each restrictor or between each restrictor located downstream of the further distributor and the reactor.

8. The apparatus according to claim 5 , wherein the starting material distributor and the further distributor are each connected by means of a connecting conduit to the reactor, where the connecting conduits are brought together as a connecting point and a joint feed conduit which opens into the reactor branches off from the connecting point and the pressure regulator is installed in the joint feed conduit.

9. The apparatus according to claim 8 , wherein a restrictor is installed in the connecting conduit.

10. A method for analyzing reactions in an apparatus according to claim 1 , in which starting materials are fed into each reactor via the starting material distributor, wherein the flow of the starting materials is regulated by means of the pressure regulators and evaluation of the reaction product from each reactor is carried out in an analysis unit.

11. The method according to claim 10 , wherein at least one starting material is fed in via the starting material distributor and at least one further starting material is fed in via the further distributor.

12. The method according to claim 10 , wherein starting materials are fed in via the starting material distributor and diluent gases or gases comprising moderators are fed in via the further distributor.

13. The method according to claim 10 , wherein each reactor is charged with a catalyst to be examined.

14. The method according to claim 10 , wherein the reactors are supplied with different volume flows of starting material and/or different partial pressures and/or different compositions and/or different pressures.

15. The method according claim 10 , wherein the reactors are all supplied with the same volume flow and subjected to the same pressure.

16. An apparatus for analyzing reactions, comprising a starting material distributor and at least two reactors which are connected in parallel and are each connected via a connecting conduit to an outlet of the starting material distributor, wherein a pressure regulator and a restrictor are installed in each connecting conduit between the starting material distributor and the reactors in order to set the inflow.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 21, 2021
From: LANGE DE OLIVEIRA, ARMIN
To: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION COMPANY
Reel/Frame 056313/0545 →
Priority Claims (1)
EP 18196194 · Sep 24, 2018 · regional
Continuity (1)
Related Publication 20220040661A1 · Feb 10, 2022