IP Library › Granted Patent US 11,813,377
Granted Patent B2
US 11,813,377 · App. 17/317,234 · Granted Nov 14, 2023

Microfiber structures and methods of synthesis and use thereof

Inventors: Jingwei Xie (Omaha, NE); Jiang Jiang (Omaha, NE)
Assignee: BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA
A61L27/56A61K9/0092A61K9/70A61L27/18A61L27/38D01D5/003D01D10/00A61L2400/12D10B2331/041D10B2401/10
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Quick Facts
Patent No.
US 11,813,377
App. No.
17/317,234
Granted
Nov 14, 2023
Kind
B2
Abstract

Three dimensional nanofiber structures are provided and methods of production thereof.

Claims (16)

1. A method for producing a microfibrous structure with increased porosity and thickness, the method comprising exposing a microfiber structure to gas bubbles, thereby increasing the porosity and thickness of the microfiber structure,

wherein said microfiber structure comprises a plurality of microfibers, and

wherein said microfiber structure comprises electrospun microfibers.

2. The method of claim 1 , wherein said gas bubbles are generated as a product of a chemical reaction.

3. The method of claim 2 , wherein said chemical reaction is the hydrolysis of sodium borohydride.

4. The method of claim 2 , wherein said exposure comprises immersing said microfiber structure in a liquid comprising the reagents for said chemical reaction.

5. The method of claim 1 , wherein said microfiber structure comprises a plurality of uniaxially-aligned microfibers, random microfibers, and/or entangled microfibers.

6. The method of claim 1 , further comprising preparing said microfiber structure comprising a plurality of microfibers prior to said exposure to bubbles.

7. The method of claim 1 , wherein said microfibers comprise hydrophobic polymers.

8. The method of claim 7 , wherein said hydrophobic polymer is poly(caprolactone).

9. The method of claim 1 , wherein said method further comprises washing the produced microfibrous structure and removing gas bubbles trapped within said microfibrous structure.

10. The method of claim 1 , wherein said method further comprises lyophilizing the produced microfibrous structure.

11. The method of claim 1 , wherein said microfiber structure comprises biodegradable fibers.

12. The method of claim 1 , wherein said microfiber structure consists of a plurality of microfibers, and wherein said microfibers consist of a polymer.

13. The method of claim 12 , wherein said polymer is a hydrophobic polymer.

14. The method of claim 1 , wherein said microfiber structure is a microfiber mat prior to said exposure to gas bubbles.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2021
From: XIE, JINGWEI; JIANG, JIANG
To: BOARD OF REGENTS OF THE UNIVERSITY OF NEBRASKA
Reel/Frame 056395/0621 →
Continuity (3)
Continuation 15510338
Provisional Application 62056899 · Sep 29, 2014
Related Publication 20210268154A1 · Sep 2, 2021