IP Library Granted Patent US 11,939,481
Granted Patent B2
US 11,939,481 · App. 17/357,805 · Granted Mar 26, 2024

Nanosurfactant formulations and use therefor

Inventors: Yanliang Zhang (South Bend, IN); Minxiang Zeng (South Bend, IN)
Assignee: University of Notre Dame du Lac
C09D11/38C09D11/033C09D11/037C09D11/322C09D11/52G01J1/42B82Y15/00B82Y40/00
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Quick Facts
Patent No.
US 11,939,481
App. No.
17/357,805
Granted
Mar 26, 2024
Kind
B2
Abstract

Provided are an ink composition, comprising greater than 0.2% by weight a graphene quantum dot nanosurfactant, a printable material, and a solvent, wherein the printable material is dispersed in the solvent by the graphene quantum dot nanosurfactant, and a method of preparing an ink composition. Advantageously, the present ink composition may be printed onto 2D and 3D substrates to form printed films with improved mechanical stability and photoconductance.

Claims (21)

1. An ink composition, comprising:

about 0.5% to about 2.0% by weight of a graphene quantum dot nanosurfactant;

a printable material; and

a solvent,

wherein the printable material is dispersed in the solvent by the graphene quantum dot nanosurfactant, and

wherein a weight ratio of the printable material to the graphene quantum dot nanosurfactant is about 0.1:1 to about 2:1.

2. The ink composition of claim 1 , wherein the graphene quantum dot nanosurfactant is produced by reacting citric acid and 4-styrenesulfonic acid sodium salt.

3. The ink composition of claim 1 , wherein the printable material comprises graphene, transition metal dichalcogenide (TMD), hexagonal boron nitride (h-BN), carbon nanotubes (CNT), or a combination thereof.

4. The ink composition of claim 1 , comprising about 0.1% to about 2.0% by weight the printable material.

5. The ink composition of claim 1 , comprising about 0.5% to about 2.0% by weight the printable material.

6. The ink composition of claim 1 , wherein the solvent comprises water, ethanol, isopropanol, cyclohexanone, terpineol, ethylene glycol, or a combination thereof.

7. The ink composition of claim 1 , having a Zeta potential of about −50 mV to about −65 mV.

8. An ink composition, comprising:

greater than 0.2% by weight of a graphene quantum dot nanosurfactant;

about 0.5% to about 2.0% by weight of a printable material; and

a solvent,

wherein the printable material is dispersed in the solvent by the graphene quantum dot nanosurfactant, and

wherein a weight ratio of the printable material to the graphene quantum dot nanosurfactant is about 0.1:1 to about 2:1.

9. The ink composition of claim 8 , wherein the graphene quantum dot nanosurfactant is produced by reacting citric acid and 4-styrenesulfonic acid sodium salt.

10. The ink composition of claim 8 , wherein the printable material comprises graphene, transition metal dichalcogenide (TMD), hexagonal boron nitride (h-BN), carbon nanotubes (CNT), or a combination thereof.

11. The ink composition of claim 8 , wherein the solvent comprises water, ethanol, isopropanol, cyclohexanone, terpineol, ethylene glycol, or a combination thereof.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 21, 2025
From: UNIVERSITY OF NOTRE DAME
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 071337/0220 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 24, 2021
From: ZHANG, YANLIANG; ZENG, MINXIANG
To: UNIVERSITY OF NOTRE DAME DU LAC
Reel/Frame 056662/0432 →
Continuity (2)
Provisional Application 63043963 · Jun 25, 2020
Related Publication 20210403739A1 · Dec 30, 2021