IP Library Granted Patent US 11,708,319
Granted Patent B2
US 11,708,319 · App. 17/375,882 · Granted Jul 25, 2023

Biphenyl amides with modified ether groups as HSP90 inhibitors and HSP70 inducers

Inventors: Brian S. J. Blagg (Lawrence, KS); Rick T. Dobrowsky (Olathe, KS); Mercy Anyika (Lawrence, KS)
Assignee: UNIVERSITY OF KANSAS
C07C233/18C07D307/20C07D309/10C07D311/08C07D311/16C07H15/203C07C2601/08C07C2601/14C07C2601/16
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Quick Facts
Patent No.
US 11,708,319
App. No.
17/375,882
Granted
Jul 25, 2023
Kind
B2
Abstract

Provided herein are compounds of the formulas: wherein: n, X 2 , R 3 , R 3 ′, R 4 , R 4 ′, R 5 , R 5 ′, R 6 , and R 6 ′ are as defined herein. Pharmaceutical compositions of the compounds are also provided. In some aspects, these compounds may be used for the treatment of diseases, including diabetic peripheral neuropathy or cancer.

Claims (27)

1. A pharmaceutical composition comprising:

(A) a compound of the formula:

wherein:

R 7 is aryl (C≤12) , aralkyl (C≤12) , or a substituted version of either of these groups;

R 8 is hydrogen, alkyl (C≤12) , cycloalkyl (C≤12) , substituted alkyl (C≤12) , or substituted cycloalkyl (C≤12) ;

R 9 is alkyl (C≤12) , cycloalkyl (C≤12) , aryl (C≤12) , heteroaryl (C≤12) , or a substituted version of any of these groups; and

Y 1 and Y 2 are each independently hydrogen or hydroxy; and

(B) an excipient; wherein the pharmaceutical composition has been formulated as a unit dose.

2. The pharmaceutical composition of claim 1 , wherein the bond between atom 1 and atom 2 in formula II is a single bond.

3. The pharmaceutical composition of claim 1 , wherein the bond between atom 1 and atom 2 in formula II is a double bond.

4. The pharmaceutical composition of claim 1 , wherein Y 1 is hydrogen.

5. The pharmaceutical composition of claim 1 , wherein Y 1 is hydroxy.

6. The pharmaceutical composition of claim 1 , wherein Y 2 is hydrogen.

7. The pharmaceutical composition of claim 1 , wherein Y 2 is hydroxy.

8. The pharmaceutical composition of claim 1 , wherein R 8 is alkyl (C≤12) .

9. The pharmaceutical composition of claim 8 , wherein R 8 is methyl.

10. The pharmaceutical composition of claim 1 , wherein R 9 is alkyl (C≤12) .

11. The pharmaceutical composition of claim 10 , wherein R 9 is methyl.

12. The pharmaceutical composition of claim 1 , wherein R 7 is aralkyl (C≤12) or substituted aralkyl (C≤12) .

13. The pharmaceutical composition of claim 12 , wherein R 7 is aralkyl (C≤12) .

14. The pharmaceutical composition of claim 13 , wherein R 7 is benzyl.

15. The pharmaceutical composition of claim 12 , wherein R 7 is substituted aralkyl (C≤12) .

16. The pharmaceutical composition of claim 15 , wherein R 7 is 4-chlorophenylmethyl, 2-bromophenylmethyl, or 2-methoxyphenylmethyl.

17. The pharmaceutical composition of claim 1 , wherein the composition further comprises a compound of the formula:

or a pharmaceutically acceptable salt thereof.

18. A method of treating a neurodegenerative disease or disorder associated with Hsp70 or Hsp90 in a patient comprising administering to the patient in need thereof a therapeutically effective amount of the pharmaceutical composition of claim 1 .

19. A method of inducing expression of a Hsp70 protein comprising contacting the protein with an effective amount of the pharmaceutical composition of claim 1 sufficient to induce the expression of the Hsp70 protein.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Apr 9, 2025
From: BIOPHARMA CREDIT PLC
To: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
Reel/Frame 070793/0130 →
RELEASE OF SECURITY INTEREST Recorded Apr 9, 2025
From: BIOPHARMA CREDIT PLC
To: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
Reel/Frame 070793/0228 →
AMENDED AND RESTATED PATENT SECURITY AGREEMENT Recorded Jul 12, 2023
From: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 064264/0557 →
PATENT SECURITY AGREEMENT Recorded May 18, 2023
From: REATA PHARMACEUTICALS HOLDINGS, LLC; REATA PHARMACEUTICALS GLOBAL, INC.; REATA PHARMACEUTICALS, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 063697/0461 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2023
From: BLAGG, BRIAN S.J.; DOBROWSKY, RICK T.; ANYIKA, MERCY
To: UNIVERSITY OF KANSAS
Reel/Frame 063419/0359 →
Continuity (4)
Division 16776091 · Jan 29, 2020
Division 15321289
Provisional Application 62016473 · Jun 24, 2014
Related Publication 20220041543A1 · Feb 10, 2022
Cited By (2)
US 12,595,278 US 12,679,860