Method to fabricate a machinable ceramic matrix composite
A method to form a machinable ceramic matrix composite comprises forming a porous ceramic multilayer on a surface of a fiber preform. In one example, the porous ceramic multilayer comprises a gradient in porosity in a direction normal to the surface. In another example, the porous ceramic multilayer includes low-wettability particles having a high contact angle with molten silicon, where an amount of the low-wettability particles in the porous ceramic multilayer varies in a direction normal to the surface. After forming the porous ceramic multilayer, the fiber preform is infiltrated with a melt, and the melt is cooled to form a ceramic matrix composite with a surface coating thereon. An outer portion of the surface coating is more readily machinable than an inner portion of the surface coating. The outer portion of the surface coating is machined to form a ceramic matrix composite having a machined surface with a predetermined surface finish and/or dimensional tolerance.
1. A method to form a ceramic matrix composite having a predetermined surface finish and/or dimensional tolerance, the method comprising:
forming a porous ceramic multilayer on a surface of a fiber preform, the porous ceramic multilayer comprising a gradient in porosity in a direction normal to the surfacer, wherein forming the porous ceramic multilayer comprises:
applying an inner slurry layer to the surface and applying an outer slurry layer to the inner slurry layer, each of the inner and outer slurry layers comprising ceramic particles in a carrier liquid, wherein a carrier liquid volatility, a particle volume fraction, and/or a polymer content of the inner and outer slurry layers are different; and
removing the carrier liquid from the inner and outer slurry layers by passive and/or active drying, thereby forming the porous ceramic multilayer comprising the gradient in porosity;
after forming the porous ceramic multilayer, infiltrating the fiber preform with a melt;
cooling the melt to form a ceramic matrix composite with a surface coating thereon, an outer portion of the surface coating being more readily machinable than an inner portion of the surface coating; and
machining the outer portion to form a ceramic matrix composite having a machined surface with a predetermined surface finish and/or dimensional tolerance.
2. The method of claim 1 , wherein the porosity of the porous ceramic multilayer increases in a direction away from the surface.
3. The method of claim 1 , wherein the ceramic matrix composite comprises silicon carbide fibers in a matrix comprising silicon carbide, and wherein the surface coating comprises silicon carbide.
4. The method of claim 1 , wherein the carrier liquid of the inner slurry layer comprises an aqueous liquid, and wherein the carrier liquid of the outer slurry layer comprises a high-volatility liquid having a vapor pressure at of at least about 4 kPa at 20-25° C.
5. The method of claim 1 , wherein the outer slurry layer contains the ceramic particles at a volume fraction lower than that of the inner slurry layer.
6. The method of claim 1 , wherein the outer slurry layer has a polymer content higher than that of the inner slurry layer.
7. The method of claim 1 , wherein a plurality of the outer slurry layers are applied to the inner slurry layer, each successive outer slurry layer comprising a reduced volume fraction of ceramic particles and/or an increased polymer content compared to an underlying slurry layer.
8. The method of claim 1 , wherein application of the inner and outer slurry layers comprises spray coating, dip coating or spin coating.
9. A method to form a ceramic matrix composite having a predetermined surface finish and/or dimensional tolerance, the method comprising:
forming a porous ceramic multilayer on a surface of a fiber preform, the porous ceramic multilayer including low-wettability particles having a high contact angle with molten silicon, an amount of the low-wettability particles in the porous ceramic multilayer varying in a direction normal to the surface;
after forming the porous ceramic multilayer, infiltrating the fiber preform with a melt;
cooling the melt to form a ceramic matrix composite with a surface coating thereon, an outer portion of the surface coating being more readily machinable than an inner portion of the surface coating; and
machining the outer portion to form a ceramic matrix composite having a surface including a predetermined surface finish and/or dimensional tolerance.
10. The method of claim 9 , wherein the low-wettability particles are selected from the group consisting of boron nitride, aluminum nitride and silica.
11. The method of claim 9 , wherein forming the porous ceramic multilayer comprises applying multiple slurry layers to the surface.
12. The method of claim 9 , wherein forming the porous ceramic multilayer comprises applying multiple tape layers to the surface.
13. A gas turbine engine component comprising a ceramic matrix composite having a predetermined surface finish and/or dimensional tolerance formed by the method of claim 1 .