IP Library Granted Patent US 12,521,745
Granted Patent B2
US 12,521,745 · App. 17/455,626 · Granted Jan 13, 2026

Method and apparatus for pulse gas delivery with pressure control

Inventors: Junhua Ding (Boxborough, MA); Michael L'Bassi (Sterling, MA)
Assignee: MKS Inc.
B05B12/06H01L21/67017
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Quick Facts
Patent No.
US 12,521,745
App. No.
17/455,626
Granted
Jan 13, 2026
Kind
B2
Abstract

Pulsed gas delivery is obtained with mass flow control using a thermal mass flow sensor and control valve. The controller is augmented for pressure control with a downstream pressure sensor. In separate control modes of operation, the control valve is controlled in response to the flow sensor during pulse gas delivery mode and controlled in response to the downstream pressure sensor during pressure control mode of operation.

Claims (30)

1 . A gas delivery system comprising:

a flow channel;

a flow sensor configured to measure flow rate in the flow channel;

a control valve configured to control flow of gas in the flow channel;

a downstream pressure sensor, downstream of the flow sensor and of the control valve, configured to measure gas pressure in the flow channel; and

a control unit configured to receive signals from the flow sensor and from the downstream pressure sensor and to apply a control signal to the control valve, the control unit configured to operate in separate modes of operation including:

a pulse gas delivery mode in which the control unit is configured to initiate a pulse of gas flow by opening the control valve, to terminate the pulse of gas flow by closing the control valve, and to control mass of gas delivered during the pulse based on flow rate measured by the flow sensor and control of the control valve during the pulse,

a pressure control mode during which the control unit is configured to control pressure at the downstream pressure sensor based on pressure measured by the downstream pressure sensor and control of the control valve; and

an upstream pressure sensor upstream of the control valve.

2 . The gas delivery system of claim 1 wherein, in the pulse gas delivery mode, the number of moles of gas delivered during the pulse is controlled as a function of measured flow rate.

3 . The gas delivery system of claim 1 wherein, in the pulse gas delivery mode, the control unit is configured to provide time-based delivery with control of gas flow to a flow setpoint.

4 . The gas delivery system of claim 1 further comprising an isolation valve downstream from the pressure sensor.

5 . The gas delivery system of claim 4 further comprising a leakage line upstream of the isolation valve.

6 . The gas delivery system of claim 1 wherein the control unit is configured to receive a signal from a host controller to switch between pulse gas delivery and pressure control modes of operation.

7 . The gas delivery system of claim 1 wherein the flow sensor is a thermal flow sensor upstream of the control valve.

8 . The gas delivery system of claim 1 wherein the control unit is configured to use pressure measured with the downstream pressure sensor for diagnosis during the pulse gas delivery mode and to use the measured flow rate for diagnosis during the pressure control mode.

9 . A method of gas delivery comprising:

providing a flow sensor to measure flow rate in a flow channel, a control valve to control flow of gas in the flow channel, and a downstream pressure sensor, downstream of the flow sensor and the control valve, to measure gas pressure in the flow channel; and

with a control unit, controlling gas flow through the control valve in separate modes of operation including:

a pulse gas delivery mode in which a pulse of gas flow is initiated by opening the control valve and terminated by closing the control valve, the mass of gas delivered during the pulse being controlled based on flow rate measured by the flow sensor and control of the control valve during the pulse,

a pressure control mode during which pressure at the downstream pressure sensor is controlled based on pressure measured by the downstream pressure sensor and control of the control valve; and

measuring upstream pressure with an upstream pressure sensor upstream of the control valve and providing pressure sensitive flow control based on the measured upstream pressure.

10 . The method of claim 9 wherein, during the pulse gas delivery mode, the number of moles of gas delivered during the pulse is controlled as a function of measured flow rate.

11 . The method of claim 9 wherein, in the pulse gas delivery mode, the control unit is configured to provide time-based delivery with control of gas flow to a flow setpoint.

12 . The method of claim 9 further comprising opening an isolation valve, downstream of the pressure sensor, during the pulse gas delivery mode.

13 . The method of claim 12 further comprising, during the pressure control mode of operation, closing the isolation valve and leaking gas through a leakage line upstream of the isolation valve.

14 . The method of claim 9 further comprising switching between the pulse gas delivery mode and the pressure mode in response to a signal from a host controller.

15 . The method of claim 9 further comprising switching to the pressure control mode after completion of a sequence of pulses in the pulse delivery mode.

16 . The method of claim 9 further comprising delivering the gas to an ALD tool.

17 . The method of claim 9 wherein measured gas pressure is used for diagnosis in the pulse gas delivery mode and measured flow rate is used for diagnosis in the pressure control mode.

Assignments (8)
CHANGE OF NAME Recorded Sep 26, 2025
From: MKS INSTRUMENTS INC.
To: MKS INC.
Reel/Frame 072962/0754 →
CHANGE OF NAME Recorded Sep 8, 2025
From: MKS INSTRUMENTS, INC.
To: MKS INC.
Reel/Frame 072836/0291 →
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 063009/0001 →
RELEASE OF SECURITY INTEREST Recorded Aug 24, 2022
From: BARCLAYS BANK PLC
To: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
Reel/Frame 062739/0001 →
SECURITY INTEREST Recorded Aug 19, 2022
From: MKS INSTRUMENTS, INC.; NEWPORT CORPORATION; ELECTRO SCIENTIFIC INDUSTRIES, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 061572/0069 →
SECURITY AGREEMENT Recorded Feb 23, 2022
From: MKS INSTRUMENTS, INC.
To: BARCLAYS BANK PLC
Reel/Frame 059220/0637 →
SECURITY AGREEMENT Recorded Feb 23, 2022
From: MKS INSTRUMENTS, INC.
To: BARCLAYS BANK PLC
Reel/Frame 059220/0607 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 18, 2021
From: DING, JUNHUA; L'BASSI, MICHAEL
To: MKS INSTRUMENTS, INC.
Reel/Frame 058156/0320 →
Continuity (2)
Provisional Application 63116599 · Nov 20, 2020
Related Publication 20220161288A1 · May 26, 2022
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